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1. 发明授权

US5821314A Thermosetting compositions and methods of forming a finish coat 失效
标题翻译：热固性组合物和形成精整涂层的方法
公开(公告)号：US5821314A
公开(公告)日：1998-10-13
申请号：US750468
申请日：1996-12-13
申请人： Satoshi Ikushima , Yasumasa Okumura , Osamu Isozaki , Minoru Tsunoda
发明人： Satoshi Ikushima , Yasumasa Okumura , Osamu Isozaki , Minoru Tsunoda
IPC分类号： C08G59/30 , C08G59/32 , C08G59/68 , C09D163/00 , C08G77/00
CPC分类号： C09D163/00 , C08G59/306 , C08G59/3254 , C08G59/68
摘要： This invention provides a thermosetting composition comprising (A) a compound (A-1) containing an epoxy group or groups and a reactive silicon group or groups as essential functional group components in the same molecule, or a mixture (A-2) of an epoxy group-containing compound and a reactive silicon group-containing compound, and (B) an organotin catalyst, a thermosetting composition comprising (A) a compound (A-3) containing (i) an epoxy group or groups, (ii) a reactive silicon group or groups and (iii) a hydroxyl group or groups and/or a carboxyl group or groups as essential functional group components in the same molecule, or a mixture (A-4) of at least two types of compounds, each compound containing at least one member selected from the class consisting of functional group components (i) to (iii), and all of the functional group components (i) to (iii) being present in said mixture, and (B) an organotin catalyst; and methods of forming a finish coat using these thermosetting compositions. The thermosetting compositions of the invention is excellent in storage stability, curable at low temperatures, and capable of producing cured products free of discoloration. The coating methods of the invention can form coating films superior in low-temperature curability, finished appearance, acid resistance, scratch resistance, and weatherability.
摘要翻译： PCT No.PCT / JP95 / 01198 Sec。 371日期1996年12月13日第 102（e）日期1996年12月13日PCT归档1995年6月15日PCT公布。公开号WO95 / 35336 日期1995年12月28日本发明提供了一种热固性组合物，其包含（A）含有环氧基或反应性硅基团的化合物（A-1）和作为同一分子中的必需官能团成分的化合物（A-1）或混合物（A -2）含有环氧基的化合物和含有反应性硅基团的化合物，和（B）有机锡催化剂，包含（A）包含（i）环氧基或基团的化合物（A-3）的热固性组合物，（ii）反应性硅基团和（iii）羟基或基团和/或羧基或基团作为同一分子中的必需官能团组分，或至少两种类型的混合物（A-4）的化合物，每种化合物含有选自官能团组分（i）至（iii）中的至少一种，和所有官能团组分（i）至（iii））存在于所述混合物中，（B ）有机锡催化剂; 以及使用这些热固性组合物形成精整涂层的方法。本发明的热固性组合物的储存稳定性优异，在低温下可固化，并且能够生产没有变色的固化产物。本发明的涂布方法可以形成优异的低温固化性，成品外观，耐酸性，耐擦伤性和耐候性优异的涂膜。

2. 发明授权

US5609918A Method of forming a top coat 失效
标题翻译：形成面漆的方法
公开(公告)号：US5609918A
公开(公告)日：1997-03-11
申请号：US477613
申请日：1995-06-07
申请人： Sachio Yamaguchi, deceased , Akimasa Nakahata , Satoshi Ikushima , Yasumasa Okumura , Haruhiko Aida , Shigeo Nishiguchi , Osamu Isozaki
发明人： Sachio Yamaguchi, deceased , Akimasa Nakahata , Satoshi Ikushima , Yasumasa Okumura , Haruhiko Aida , Shigeo Nishiguchi , Osamu Isozaki
IPC分类号： B05D7/00 , C09D133/06 , C09D163/00 , C09D201/02 , B05D1/36
CPC分类号： B05D7/53 , C09D133/066 , C09D133/068 , C09D163/00 , C09D201/02
摘要： The invention provides a method of forming a top coat by forming in sequence a colored base coat on a substrate and a clear coat, the method being characterized in that at least one of the colored base coat and the clear coat is formed by a curable coating composition consisting essentially of:(a) (a-1) a resin having a hydroxyl group, a carboxyl group and an epoxy group in the same molecule, or (a-2) a mixture of a hydroxyl- and carboxyl-containing resin with a polyepoxide;(b) a silicon compound having, per molecule, at least one silanol group and/or at least one hydrolyzable group directly bound to a silicon atom; and(c) an organic solvent.
摘要翻译：本发明提供一种通过在基材上形成有色底涂层和透明涂层来形成顶涂层的方法，其特征在于，着色底涂层和透明涂层中的至少一个通过可固化涂层形成组合物基本上由以下组成：（a）（a-1）在同一分子中具有羟基，羧基和环氧基的树脂，或（a-2）含羟基和羧基的树脂与聚环氧化物（b）每分子具有至少一个硅烷醇基和/或至少一个与硅原子直接结合的可水解基团的硅化合物; 和（c）有机溶剂。

3. 发明授权

US5719234A High solid coating composition and method for forming topcoat using same 失效
标题翻译：高固体涂料组合物和使用其形成面漆的方法
公开(公告)号：US5719234A
公开(公告)日：1998-02-17
申请号：US747341
申请日：1996-11-12
申请人： Motoshi Yabuta , Masaaki Saika , Satoru Ito , Hiroyuki Okada , Yasumasa Okumura , Hiroshi Igarashi , Satoshi Ikushima
发明人： Motoshi Yabuta , Masaaki Saika , Satoru Ito , Hiroyuki Okada , Yasumasa Okumura , Hiroshi Igarashi , Satoshi Ikushima
IPC分类号： B05D1/36 , B05D7/00 , C08L43/04 , C08L83/04 , C09D133/06 , C09D137/00 , C09D143/04 , C09D163/00 , C09D183/04 , C09D201/08
CPC分类号： B05D7/532 , C09D133/064 , C09D143/04 , C09D201/08 , C08L2205/18 , C08L43/04 , C08L83/04 , Y10T428/2949 , Y10T428/2958 , Y10T428/31663
摘要： An object of the present invention is to provide a heat-curable high solid coating composition capable of forming a coating film which is excellent in both acid resistance and scratch resistance, and a method for forming a topcoat using said composition. The present invention provides a heat-curable high solid coating composition comprising: (A) a carboxyl-containing compound, (B) a vinyl polymer having an epoxy group, a hydroxyl group and a hydrolyzable alkoxysilyl group in one molecule, (C) a reactive organopolysiloxane, and (D) a crosslinked particulate polymer. The present invention also provides a method for forming a topcoat using said composition.
摘要翻译：本发明的目的是提供一种能够形成耐酸性和耐划伤性优异的涂膜的热固性高固体涂料组合物，以及使用该组合物形成面漆的方法。本发明提供一种热固性高固体涂料组合物，其包含：（A）含羧基化合物，（B）一分子中具有环氧基，羟基和可水解烷氧基甲硅烷基的乙烯基聚合物，（C）反应性有机聚硅氧烷，（D）交联的颗粒聚合物。本发明还提供了使用所述组合物形成面漆的方法。

4. 发明授权

US6015848A Coating composition and method for application thereof 失效
标题翻译：涂料组合物及其应用方法
公开(公告)号：US6015848A
公开(公告)日：2000-01-18
申请号：US985907
申请日：1997-12-05
申请人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
发明人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
IPC分类号： C08G59/24 , C08L27/12 , C08L33/06 , C08L33/16 , C08L63/00 , C08L63/02 , C09D133/06 , C09D163/00 , C08J3/28 , C08L83/04
CPC分类号： C08L63/00 , C08G59/24 , C09D133/068 , C09D163/00 , C08L27/12 , C08L33/068 , C08L33/16 , Y10S525/922
摘要： The present invention provides a thermosetting organic solvent type coating capable of forming a cured coating film having a TUKON hardness at 20.degree. C. of 15 or more and the minimum value of dynamic modulus E' at a frequency of 110 Hz in the temperature range of 150-200.degree. C., of 1.times.1O.sup.9 dyn/cm.sup.2 or more. The cured film formed from the coating, as compared with the cured films formed from conventional organic solvent type coatings used as a top coat for automobile (e.g. an organic solvent type coating containing, as main components, a hydroxyl group-containing acrylic resin and a melamine resin, or a carboxylic-epoxy type coating), is at least equivalent in weatherability, finish appearance, acid resistance, etc. and superior in stain resistance.
摘要翻译：本发明提供一种热固性有机溶剂型涂料，其能够在20℃下的TUKON硬度形成15或更高的固化涂膜，并且在110℃的频率下在110Hz的频率下形成动态模量E'的最小值 150-200℃，为1×10 9 dyn / cm 2以上。与由用作汽车面漆的常规有机溶剂型涂料形成的固化膜（例如含有含羟基的丙烯酸树脂的主要成分的有机溶剂型涂料）相比，由涂层形成的固化膜三聚氰胺树脂或羧基环氧型涂料）在耐候性，外观，耐酸性等方面至少相当，并且耐污染性优异。

5. 发明授权

US06319557B1 Coating composition and method for application thereof 失效
标题翻译：涂料组合物及其应用方法
公开(公告)号：US06319557B1
公开(公告)日：2001-11-20
申请号：US09437145
申请日：1999-11-10
申请人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
发明人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
IPC分类号： B05D302
CPC分类号： C08L63/00 , C08G59/24 , C08L27/12 , C08L33/068 , C08L33/16 , C09D133/068 , C09D163/00 , Y10T428/31692 , Y10T428/31699 , C08L2666/04 , C08L2666/06 , C08L2666/14 , C08L2666/54
摘要： The present invention provides a thermosetting organic solvent type coating capable of forming a cured coating film having a TUKON hardness at 20° C. of 15 or more and the minimum value of dynamic modulus E′ at a frequency of 110 Hz in the temperature range of 150-200° C., of 1×109 dyn/cm or more. The cured film formed from the coating, as compared with the cured films formed from conventional organic solvent type coatings used as a top coat for automobile (e.g. an organic solvent type coating containing, as main components, a hydroxyl group-containing acrylic resin and a melamine resin, or a carboxylic-epoxy type coating), is at least equivalent in weatherabiIity, finish appearance, acid resistance, etc. and superior in stain resistance.
摘要翻译：本发明提供一种热固性有机溶剂型涂料，其能够在20℃下形成具有15℃以上的TUKON硬度的固化涂膜，在110Hz的温度范围内形成频率为110Hz的动态模量E'的最小值 150-200℃，1×10 9 dyn / cm以上。与由用作汽车面漆的常规有机溶剂型涂料形成的固化膜（例如含有含羟基的丙烯酸树脂的主要成分的有机溶剂型涂料）相比，由涂层形成的固化膜三聚氰胺树脂或羧基环氧型涂料）在耐候性，外观，耐酸性等方面至少相当，耐污染性优异。

6. 发明授权

US06262147B1 Coating composition and method for application thereof 失效
标题翻译：涂料组合物及其应用方法
公开(公告)号：US06262147B1
公开(公告)日：2001-07-17
申请号：US09384299
申请日：1999-08-26
申请人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
发明人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
IPC分类号： C08L6300
CPC分类号： C08L63/00 , C08G59/24 , C08L27/12 , C08L33/068 , C08L33/16 , C09D133/068 , C09D163/00 , Y10S525/922 , C08L2666/04 , C08L2666/06 , C08L2666/14 , C08L2666/54
摘要： The present invention provides a thermosetting organic solvent type coating capable of forming a cured coating film having a TUKON hardness at 20° C. of 15 or more and the minimum value of dynamic modulus E′ at a frequency of 110 Hz in the temperature range of 150-200° C., of 1×109 dyn/cm2 or more. The cured film formed from the coating, as compared with the cured films formed from conventional organic solvent type coatings used as a top coat for automobile (e.g. an organic solvent type coating containing, as main components, a hydroxyl group-containing acrylic resin and a melamine resin, or a carboxylic-epoxy type coating), is at least equivalent in weatherability, finish appearance, acid resistance, etc. and superior in stain resistance.
摘要翻译：本发明提供一种热固性有机溶剂型涂料，其能够在20℃下形成具有15℃以上的TUKON硬度的固化涂膜，在110Hz的温度范围内形成频率为110Hz的动态模量E'的最小值 150-200℃，1×10 9 dyn / cm 2以上。与由用作汽车面漆的常规有机溶剂型涂料形成的固化膜（例如含有含羟基的丙烯酸树脂的主要成分的有机溶剂型涂料）相比，由涂层形成的固化膜三聚氰胺树脂或羧基环氧型涂料）在耐候性，外观，耐酸性等方面至少相当，并且耐污染性优异。

7. 发明授权

US5929158A Non-aqueous polymer dispersion and curable compositions 失效
标题翻译：非水聚合物分散体和可固化组合物
公开(公告)号：US5929158A
公开(公告)日：1999-07-27
申请号：US72461
申请日：1998-05-05
申请人： Yoshizumi Matsuno , Nobushige Numa , Chihiro Nagano , Satoshi Ikushima , Yasumasa Okumura
发明人： Yoshizumi Matsuno , Nobushige Numa , Chihiro Nagano , Satoshi Ikushima , Yasumasa Okumura
IPC分类号： C08L33/00 , C08F2/08 , C08F20/22 , C08L27/00
CPC分类号： C08F2/08 , C08F20/22
摘要： The invention provides a non-aqueous polymer dispersion wherein a particulate polymer is dispersed in an organic solvent containing a dispersion stabilizer resin, the polymer being insoluble to the organic solvent and containing a fluoroalkyl group-containing (meth)acrylate as a monomer component. The invention further provides a curable composition comprising the non-aqueous polymer dispersion, a hydroxyl group containing resin and at least one crosslinking agent selected from the group consisting of amino resins, tris(alkoxycarbonylamino)triazines, polyisocyanate compounds and blocked polyisocyanate compounds. A highly stain-resistant coating film can be formed using the dispersion or composition of the invention.
摘要翻译：本发明提供一种非水聚合物分散体，其中颗粒状聚合物分散在含有分散稳定剂树脂的有机溶剂中，该聚合物不溶于有机溶剂，并含有含氟烷基的（甲基）丙烯酸酯作为单体组分。本发明还提供了包含非水性聚合物分散体，含羟基树脂和至少一种选自氨基树脂，三（烷氧基羰基氨基）三嗪，多异氰酸酯化合物和封端多异氰酸酯化合物的交联剂的可固化组合物。可以使用本发明的分散体或组合物形成高度耐污染的涂膜。

8. 发明授权

US5641574A Process for forming overcoat 失效
标题翻译：成型外套的工艺
公开(公告)号：US5641574A
公开(公告)日：1997-06-24
申请号：US553399
申请日：1995-11-21
申请人： Akira Kasari , Satoshi Ikushima , Osamu Isozaki , Naoji Matsumoto , John David Nordstrom
发明人： Akira Kasari , Satoshi Ikushima , Osamu Isozaki , Naoji Matsumoto , John David Nordstrom
IPC分类号： B05D1/36 , B05D7/00 , B05D7/24 , C08G59/42 , C09D157/00 , C09D163/00 , C09D167/00 , C09D167/02 , C09D175/00 , C09D175/04 , C09D201/00
CPC分类号： B05D7/532 , C08G59/42 , Y10T428/31511
摘要： A process for forming an overcoat by the two-coat one-bake method wherein a base coat composition and a clear coat composition are applied to a substrate ##STR1## wet-on-wet and thereafter cured at the same time by heating, the process being characterized in that the base coat composition is an aqueous coating composition consisting primarily of: (I) an aqueous dispersion or solution of a polymer containing a crosslinkable functional group, (II) a crosslinking agent, (III) a coloring pigment, and (IV) water, the clear coat composition being a coating composition comprising: (A) at least one resin selected from the group consisting of (i) a resin having at least one epoxy group and at least one hydroxyl group in the molecule, (ii) a resin mixture of (ii-1) a resin having at least two epoxy groups in the molecule and (ii-2) a resin having at least two hydroxyl groups in the molecule, (iii) a resin having at least two epoxy groups in the molecule, and (iv) any mixture thereof, (B) a crosslinking agent comprising a compound having at least two noncyclic acid anhydride groups and represented by formula (1) wherein R is a monovalent hydrocarbon group having 2 to 50 carbon atoms, R' is a bivalent hydrocarbon group having 2 to 50 carbon atoms, the hydrocarbon groups R and R' containing or not containing an ether linkage, urethane linkage or ester linkage, and n is an integer of 1 to 500, and (C) a curing catalyst.
摘要翻译： PCT No.PCT / JP93 / 00678 Sec。 371日期：1995年11月21日 102（e）1995年11月21日日期PCT提交1993年5月24日PCT公布。第WO94 / 27741号公报日期1994年12月8日一种通过双层单烘烤法形成外涂层的方法，其中将底涂层组合物和透明涂层组合物施加到基底上（1）湿润湿润，然后在该方法的特征在于底涂层组合物是主要由以下组成的水性涂料组合物：（I）含有可交联官能团的聚合物的水性分散体或溶液，（II）交联剂，（ III）着色颜料和（IV）水，所述透明涂料组合物为涂料组合物，其包含：（A）至少一种选自以下的树脂：（i）具有至少一个环氧基的树脂和至少一种（ii）分子中具有至少两个环氧基的树脂（ii-1）和（ii-2）分子中具有至少两个羟基的树脂的树脂混合物，（iii）分子中具有至少两个羟基的树脂，分子中具有至少两个环氧基的树脂，和（iv）任何混合物（B）交联剂，其包含具有至少两个非环状酸酐基团并由式（1）表示的化合物，其中R是具有2至50个碳原子的一价烃基，R'是具有2至 50个碳原子，含有或不含醚键的烃基R和R'，氨基甲酸酯键或酯键，n为1〜500的整数，（C）固化催化剂。

9. 发明授权

US5609960A Process for forming overcoat 失效
标题翻译：成型外套的工艺
公开(公告)号：US5609960A
公开(公告)日：1997-03-11
申请号：US553398
申请日：1995-11-21
申请人： Akira Kasari , Satoshi Ikushima , Osamu Isozaki , Naoji Matsumoto , John D. Nordstrom
发明人： Akira Kasari , Satoshi Ikushima , Osamu Isozaki , Naoji Matsumoto , John D. Nordstrom
IPC分类号： B05D1/36 , B05D3/02 , B05D5/00 , B05D7/00 , B05D7/24 , B05D7/26 , C08G59/42 , C08L33/06 , C08L73/02 , C09D133/04 , C09D133/06 , C09D133/14 , C09D161/20 , C09D163/00 , C09D167/00 , C09D167/02 , C09D201/02 , C09D201/06
CPC分类号： B05D7/532 , C08G59/42 , C09D133/068 , C09D163/00 , C08L33/066 , C08L73/02 , Y10T428/31511
摘要： A process for forming an overcoat by the two-coat one-bake method wherein a basecoat composition and a clear coat composition are applied to a substrate wet-on-wet and thereafter cured at the same time by heating, the process being characterized in that the base coat composition is a coating composition consisting primarily of a hydroxyl-containing resin, an amine resin, a pigment and an organic solvent, the clear coat composition being a coating composition comprising:(A) at least one resin selected from the group consisting of (i) a resin having at least one epoxy group and at least one hydroxyl group in the molecue, (ii) a resin mixture of (ii-1) a resin having at least two epoxy groups in the molecule and (ii-2) a resin having at least two hydroxyl groups in the molecule, (iii) a resin having at least two epoxy groups in the molecule, and (iv) any mixture thereof,(B) a crosslinking agent comprising a compound having at least two noncyclic acid anhydride groups and represented by the formula ##STR1## wherein R is a monovalent hydrocarbon group having 2 to 50 carbon atoms, R' is a bivalent hydrocarbon group having 2 to 50 carbon atoms, the hydrocarbon groups R and R' containing or not containing an ether linkage, urethane linkage or ester linkage, and n is an integer of 1 to 500 and (C) a curing catalyst.
摘要翻译： PCT No.PCT / JP93 / 00669 Sec。 371日期：1995年11月21日 102（e）日期1995年11月21日PCT提交1993年5月21日PCT公布。公开号WO94 / 27740 日期1994年12月8日一种通过双层单烘烤法形成外涂层的方法，其中将底涂层组合物和透明涂层组合物施加到湿润基板上，然后通过加热同时固化，方法的特征在于，底涂层组合物是主要由含羟基树脂，胺树脂，颜料和有机溶剂组成的涂料组合物，透明涂料组合物是涂料组合物，其包含：（A）至少一种树脂选自（i）在分子中具有至少一个环氧基和至少一个羟基的树脂，（ii）（ii-1）在分子中具有至少两个环氧基的树脂的树脂混合物和（ii-2）在分子中具有至少两个羟基的树脂，（iii）分子中具有至少两个环氧基的树脂，和（iv）其任何混合物，（B）包含化合物具有至少两个非环酸酐基团a d由下式表示：其中R是具有2至50个碳原子的一价烃基，R'是具有2至50个碳原子的二价烃基，烃基R和R'含有或不含有醚键氨基甲酸酯键或酯键，n为1〜500的整数，（C）固化催化剂。

10. 发明授权

US06395340B1 Coating composition and method for coating therewith 失效
标题翻译：涂料组合物及其涂布方法
公开(公告)号：US06395340B1
公开(公告)日：2002-05-28
申请号：US09529854
申请日：2000-04-20
申请人： Seiji Wada , Satoshi Ikushima , Haruhiko Aida , Hideo Sugai
发明人： Seiji Wada , Satoshi Ikushima , Haruhiko Aida , Hideo Sugai
IPC分类号： B05D136
CPC分类号： C08G59/50 , C09D163/00 , Y10T428/31511 , C08L2666/54
摘要： This invention provides a thermosetting organic solvent paint comprising (A) a compound having at least two alicyclic epoxy groups in one molecule and having a number average molecular weight of less than 2000, (B) a secondary amino group-containing compound and (C) a thermolatent cationically polymerizable catalyst and further, under circumstances, (D) colloidal silica, and capable of forming a rigid coating film which is hard, tough and excellent in stain resistance, and from which pollutants, if adhered, are easily removed. This invention further provides a method to form a multi-layered top coating film which comprises applying, to a material to be coated, one or more species of colored paint and one or more species of clear paint in order, said method being characterized in that the above-mentioned paint is used as a clear paint which is to be applied on the uppermost layer.
摘要翻译：本发明提供一种热固性有机溶剂涂料，其包含（A）在一个分子中具有至少两个脂环族环氧基并且数均分子量小于2000的化合物，（B）含仲氨基的化合物和（C）另外，在（D）胶体二氧化硅的情况下，还可以形成硬质，坚韧，耐污染性优异的刚性涂膜，容易除去附着污染物的情况。本发明还提供一种形成多层顶涂层的方法，该方法包括将一种或多种着色涂料和一种或多种透明涂料应用于待涂覆的材料，所述方法的特征在于：使用上述涂料作为涂布在最上层的透明涂料。

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