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1. 发明授权

US3952125A Electrically insulating material 失效
标题翻译：电绝缘材料
公开(公告)号：US3952125A
公开(公告)日：1976-04-20
申请号：US500502
申请日：1974-08-26
申请人： Takatoshi Kuratsuji , Hiroo Shima , Takeo Shima , Shoji Kawase , Sakae Shimotsuma , Masahiro Hosoi
发明人： Takatoshi Kuratsuji , Hiroo Shima , Takeo Shima , Shoji Kawase , Sakae Shimotsuma , Masahiro Hosoi
IPC分类号： H01B3/42 , C08G63/12
CPC分类号： H01B3/423 , Y10T428/266
摘要： An electrically insulating material composed of an unstretched film of a substantially linear polyester at least 85 mol% of the recurring units of which consist of a hexamethylene naphthalene-2,6-dicarboxylate unit and which has an intrinsic viscosity, as measured on its ortho-chlorophenol solution at 35.degree.C., of at least 0.3.
摘要翻译：由绝缘材料构成的电绝缘材料，其基本线性聚酯的至少85摩尔％的重复单元的未拉伸膜由六亚甲基萘-2,6-二甲酸酯单元组成，并且其特性粘度为其邻位 - 氯酚溶液在35℃，至少0.3。

2. 发明授权

US3963844A Extrusion-molded article having good thermal stability 失效
标题翻译：具有良好热稳定性的挤压成型品
公开(公告)号：US3963844A
公开(公告)日：1976-06-15
申请号：US478101
申请日：1974-06-10
申请人： Sakae Shimotsuma , Masahiro Hosoi , Takatoshi Kuratsuji , Shoji Kawase , Takeo Shima
发明人： Sakae Shimotsuma , Masahiro Hosoi , Takatoshi Kuratsuji , Shoji Kawase , Takeo Shima
IPC分类号： B29C47/00 , B29C47/78 , B29C47/88 , B29D7/01 , C08L67/02 , F16L9/12
CPC分类号： C08J7/08 , B29C47/00 , B29C47/0021 , B29C47/0026 , B29C47/786 , B29C47/862 , B29C47/88 , B29C47/8815 , B29C47/8845 , B29C47/8875 , B29C47/8895 , C08J2367/00 , C08J2367/02 , Y10T428/139 , Y10T428/261 , Y10T428/268 , Y10T428/269 , Y10T428/31786
摘要： A thermally stable extrusion-molded article characterized by (1) consisting of a substantially linear polyester in which at least 90 mol% of the total recurring units consist of tetramethylene 2,6-naphthalate units, (2) having a density not in excess of 1.318, and (3) being in the unstretched state.This article is prepared by extruding a melt of a substantially linear polyester in which at least 90 mol% of the total recurring units consist of tetramethylene 2,6-naphthalate units into the form of a molded structure, and cooling the extruded molded structure to room temperature, wherein during the period in which the extruded molded structure is cooled from at least 75%C. to room temperature, the cooling of the molded structure is performed rapidly so that the density of the molded structure does not exceed 1.318.
摘要翻译：一种热稳定的挤出模塑制品，其特征在于（1）由基本上线性的聚酯组成，其中至少90摩尔％的总重复单元由2,6-萘二甲酸丁二烯酯单元组成，（2）密度不超过 1.318，（3）处于未拉伸状态。

3. 发明授权

US3961008A Process for preparing polyester shaped articles 失效
标题翻译：聚酯成型制品的制备方法
公开(公告)号：US3961008A
公开(公告)日：1976-06-01
申请号：US500503
申请日：1974-08-26
申请人： Takatoshi Kuratsuji , Shoji Kawase , Takeo Shima , Sakae Shimotsuma , Masahiro Hosoi
发明人： Takatoshi Kuratsuji , Shoji Kawase , Takeo Shima , Sakae Shimotsuma , Masahiro Hosoi
IPC分类号： B29C61/00 , B29C47/00 , B29C47/78 , B29C47/88 , B29D7/01 , B29C25/00 , B29D23/04
CPC分类号： C08J7/08 , B29C47/00 , B29C47/0021 , B29C47/0023 , B29C47/0026 , B29C47/862 , B29C47/88 , B29C47/8805 , B29C47/8815 , B29C47/8845 , B29C47/8895 , B29C47/0019 , C08J2367/00 , C08J2367/02
摘要： A process for preparing a shaped article by melt-extruding a polyester containing tetramethylene naphthalene-2,6-dicarboxylate or hexamethylene naphthalene-2,6-dicarboxylate as a main recurring unit, wherein the extrudate is exposed to a temperature of 75.degree. to 450.degree.C. for 1 to 180 seconds immediately after extrusion.
摘要翻译：通过熔融挤出含有2,6-萘二甲酸2,6-二甲酯或六亚甲基萘-2,6-二羧酸六亚甲酯的聚酯作为主要重复单元制备成型制品的方法，其中将挤出物暴露于75℃至450℃的温度在挤出后立即进行1至180秒。

4. 发明授权

US4066624A Polyesters of naphthalene carboxylic acids and hydroxy alkoxydiphenyl sulfones 失效
标题翻译：萘二羧酸和羟基烷基二苯基磺酸酯的聚酯
公开(公告)号：US4066624A
公开(公告)日：1978-01-03
申请号：US542793
申请日：1975-01-21
申请人： Shoji Kawase , Takatoshi Kuratsuji , Hiroo Inata , Kazuyoshi Suzuki , Takeo Shima
发明人： Shoji Kawase , Takatoshi Kuratsuji , Hiroo Inata , Kazuyoshi Suzuki , Takeo Shima
IPC分类号： C08G63/00 , C08G63/688 , C08G63/18 , C08G63/66 , C08G63/68
CPC分类号： C08G63/6886
摘要： A process for preparing polyesters, which comprises reacting (A) a difunctional carboxylic acid component containing at least 50 mol% of a naphthalene dicarboxylic acid and/or its ester-forming derivative, (B) a diol component containing an aromatic group and at least 50 mol% of a 4,4'-bis-(.omega.-hydroxyalkoxy)diphenylsulfone and (C) an aliphatic or alicyclic diol component, the molar ratio of component (B) to component (A) being 0.05-1, and the molar ratio of the sum of components (B) and (C) to component (A) being 1.1-3.0; and then polymerizing the resulting reaction product in the presence of a catalyst while distilling off the excess of the component (C) out of the reaction system, thereby to form a polymer having a reduced viscosity of at least 0.5.

5. 发明授权

US4060516A Naphthalate polyester filaments 失效
标题翻译：萘二甲酸酯聚酯长丝
公开(公告)号：US4060516A
公开(公告)日：1977-11-29
申请号：US646645
申请日：1976-01-05
申请人： Takatoshi Kuratsuji , Shoji Kawase , Takeo Shima
发明人： Takatoshi Kuratsuji , Shoji Kawase , Takeo Shima
IPC分类号： C08G63/189 , D01F6/62 , C08G63/18 , C08G63/70
CPC分类号： C08G63/189 , D01F6/62
摘要： Naphthalate polyester filaments, yarns or fibers consisting essentially of a naphthalate polyester which has an intrinsic viscosity of 0.3 to 3.5 and a softening point of at least 200.degree. C, and in which at least 85 mol% of the total recurring units consist of units of the formula ##STR1## wherein n is 4 or 6, and having at least one diffraction peak at a Bragg scattering angle 2.theta. = 16.3.degree. -- 16.7.degree. and/or 2.theta. = 25.3.degree. - 25.8.degree. in their X-ray diffraction. These filaments, yarns or fibers are useful especially as an electrically insulating material, an elastomeric reinforcing material, a fluid filter material, a paper-making canvas and a fastener component material.Of these, filaments, yarns or fibers of poly(tetramethylene 2,6-naphthalate) are prepared by melt-spinning the polymer thereby to form undrawn filaments having a birefringence of at lest 0.01 and a density of not more than 1.300, drawing the undrawn filaments in at least one step at a temperature of at least 60.degree. C. at a total draw ratio of at least 1.8, and then heat-treating the drawn filaments at a temperature higher than the temperature employed in the drawing step and within a range of 100.degree. to 240.degree. C. at constant length, under a restricted shrinkage of not more than 15%, or under a stretch of not more than 15%.
摘要翻译：萘二甲酸酯聚酯长丝，基本上由萘甲酸酯聚酯组成的纱线或纤维，其特性粘度为0.3-3.5，软化点为至少200℃，其中至少85mol％的总重复单元由其中n为4或6，并且在其X射线衍射中在布喇格散射角2θ= 16.3°-16.7°和/或2θ= 25.3°-25.8°处具有至少一个衍射峰的式。这些长丝，纱线或纤维特别用作电绝缘材料，弹性体增强材料，流体过滤材料，造纸帆布和紧固件组件材料。

6. 发明授权

US4026973A Process for preparing heat-resistant aromatic polyester filaments 失效
标题翻译：制备耐热芳香聚酯长丝的方法
公开(公告)号：US4026973A
公开(公告)日：1977-05-31
申请号：US601232
申请日：1975-08-01
申请人： Takeo Shima , Seiichi Yamashiro , Masao Yoshimura , Takayuki Kobayashi , Takatoshi Kuratsuji , Hiroo Inata
发明人： Takeo Shima , Seiichi Yamashiro , Masao Yoshimura , Takayuki Kobayashi , Takatoshi Kuratsuji , Hiroo Inata
IPC分类号： D01F6/62 , B29C25/00
CPC分类号： D01F6/62
摘要： Heat-resistant aromatic polyester filaments having heretofore unknown physical properties and a combination of excellent heat resistance and mechanical strength, which (1) is composed of an aromatic polyester in which at least 90 mole % of the structural units are ethylene-2,6-naphthalate units, (2) has a melting point at a constant length (Tm;.degree.C.) of at least 287.degree. C., (3) has a density (d)(g/cm.sup.3) of at least 1.370, (4) is insoluble in a phenol/orthodichlorobenzene mixed solvent (mixing ratio = 6/4 on the weight basis) at 160.degree. C. and (5) meets the requirements expressed by the following formulaeL(Tm - 280) = 400 (I).DELTA. n(d - 1.350) = 70 .times. 10.sup.-.sup.3 (II)L = .lambda.K/(B-b)cos .theta. (III)and the process for the preparation thereof.
摘要翻译：耐热芳香族聚酯长丝具有迄今未知的物理性能和优异的耐热性和机械强度的组合，（1）由芳族聚酯组成，其中至少90摩尔％的结构单元是乙烯 - （2）具有至少287℃的恒定长度（Tm;℃）的熔点，（3）密度（d）（g / cm 3）至少为1.370，（4））在160℃下不溶于苯酚/邻二氯苯混合溶剂（混合比为6/4），（5）满足下式L（Tm-280）= 400（I）表示的要求， DELTA n（d-1.350）= 70×10 -3（II）L =λK /（Bb）cosθ（III）及其制备方法。

7. 发明授权

US4042571A Fire-retardant polyamides from naphthalene dicarboxylic reactant and halogenated carboxylic reactant 失效
标题翻译：萘二羧酸反应物和卤代羧酸反应物的阻燃聚酰胺
公开(公告)号：US4042571A
公开(公告)日：1977-08-16
申请号：US495417
申请日：1974-08-07
申请人： Shoji Kawase , Takeo Shima , Keiichi Moriyama
发明人： Shoji Kawase , Takeo Shima , Keiichi Moriyama
IPC分类号： C08G69/42 , C08G69/26
CPC分类号： C08G69/42
摘要： A process for preparing a fired-retardant polyamide, which comprises polymerizing a carboxylic acid component consisting essentially of at least one naphthalene-dicarboxylic acid selected from the group consisting of naphthalene-2,7-dicarboxylic acid and naphthalene-2,6-dicarboxylic acid and/or its amide-forming derivative, and a halogen substituted-carboxylic acid and/or its amide-forming derivative, and an aliphatic diamine, the amount of said naphthalene dicarboxylic acid and/or its derivative being at least 40 mol% of the total acid component, and the amount of said halogen-substituted carboxylic acid being such that the halogen atom content of the polyamide is at least 0.13% by weight.
摘要翻译：一种制备阻燃聚酰胺的方法，其包括将基本上由至少一种选自萘-2,7-二羧酸和萘-2,6-二羧酸的萘 - 二羧酸组成的羧酸组分聚合和/或其酰胺形成衍生物和卤素取代的羧酸和/或其酰胺形成衍生物和脂族二胺，所述萘二甲酸和/或其衍生物的量为至少40摩尔％总酸成分和所述卤素取代羧酸的量使得聚酰胺的卤素原子含量为至少0.13重量％。

8. 发明授权

US3972852A Process for preparing aromatic polyesters from diphenols 失效
标题翻译：从二酚制备芳族聚酯的方法
公开(公告)号：US3972852A
公开(公告)日：1976-08-03
申请号：US494870
申请日：1974-08-05
申请人： Hiroo Inata , Shoji Kawase , Takeo Shima
发明人： Hiroo Inata , Shoji Kawase , Takeo Shima
IPC分类号： C08G63/195 , C08G63/199 , C08G63/64 , C08G63/672 , C08G63/688 , C08G63/80 , C08G63/18 , C08G63/26
CPC分类号： C08G63/6884 , C08G63/195 , C08G63/199 , C08G63/64 , C08G63/672 , C08G63/6886 , C08G63/80
摘要： In a process of preparing aromatic polyesters from (A) aromatic dicarboxylic acids and (B) diphenols by the solid phase polymerization method, the speed of the solid phase polymerization reaction can be enhanced to a marked degree by copolymerizing (C) an aliphatic dihydroxy compound, and in this case the amounts in which the components (B) and (C) are used, based on (A), being 70 - 105 mol % of (B) and 1 - 50 mol % of (C), with the total amount of (B) and (C) corresponding to 100 - 130 mol % of (A).
摘要翻译：在通过固相聚合法从（A）芳族二羧酸和（B）二酚制备芳族聚酯的方法中，通过共聚（C）脂族二羟基化合物，可以显着提高固相聚合反应的速度，在这种情况下，使用（A）成分（B）和（C）的量为（B）为70〜105摩尔％，（C）为1-50摩尔％，其中（B）和（C）的总量相当于（A）的100-130mol％。

9. 发明授权

US4012365A Fiber-forming polyamides from naphthalene-2,7-dicarboxylic acid and aliphatic diamine 失效
标题翻译：来自萘-2,7-二羧酸和脂族二胺的成纤聚酰胺
公开(公告)号：US4012365A
公开(公告)日：1977-03-15
申请号：US515048
申请日：1974-10-15
申请人： Keiichi Moriyama , Shoji Kawase , Takeo Shima
发明人： Keiichi Moriyama , Shoji Kawase , Takeo Shima
IPC分类号： C08G69/00 , C08G69/26 , C08G69/36
CPC分类号： C08G69/265 , C08G69/36
摘要： Fiber-forming polyamides are prepared by poly-condensing naphthalene-2,7-dicarboxylic acid and a straight-chain aliphatic diamine containing 4 to 13 carbon atoms and 15 to 50 mol% of another carboxylic acid and/or another diamine as a copolymerizing component.
摘要翻译：通过将萘-2,7-二羧酸和含有4至13个碳原子的直链脂族二胺和15至50摩尔％的另一种羧酸和/或其它二胺作为共聚组分聚缩合制备纤维形成聚酰胺。

10. 发明授权

US3989664A Stabilized polyester composition and method for stabilizing polyester 失效
标题翻译：稳定聚酯组合物和聚酯稳定方法
公开(公告)号：US3989664A
公开(公告)日：1976-11-02
申请号：US569687
申请日：1975-04-21
申请人： Shoji Kawase , Hiroo Inata , Takeo Shima
发明人： Shoji Kawase , Hiroo Inata , Takeo Shima
IPC分类号： C08K5/134 , C08K5/13
CPC分类号： C08K5/1345
摘要： A method for stabilizing a polyester at least 80% of the recurring units of which in terms of number consist of tetramethylene terephthalate units or tetramethylene-2,6-naphthalate units, by incorporating into said polyester 0.001 to 10% by weight, based on the weight of the polyester, of at least one compound of the following formula (I) ##SPC1##This application is a continuation-in-part of application Ser. No. 548,988, filed Feb. 10, 1975, which in turn is a divisional application of Ser. No. 417,918 filed Nov. 21, 1973, now U.S. Pat. No. 3,904,578.
摘要翻译：一种稳定聚酯的方法，其中至少80％的重复单元数目以对苯二甲酸丁二醇酯单元或四亚甲基-2,6-萘二甲酸酯单元组成，通过将0.001至10重量％的所述聚酯掺入所述聚酯中，基于聚酯的重量，至少一种下式（I）的化合物+ Q，10本申请是申请序列号的部分继续申请。 1975年2月10日提交的第548,988号，其又是Ser的分案申请。 1973年11月21日提交的美国专利第417,918号。 3,904,578。

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