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    • 3. 发明授权
    • Crystalline mixture solid composition and process for preparation thereof
    • 结晶混合物固体组合物及其制备方法
    • US06746541B2
    • 2004-06-08
    • US09958666
    • 2001-10-12
    • Ryuzo UenoAkihiko TabataJunya HondaYojiro FurukawaSho Arai
    • Ryuzo UenoAkihiko TabataJunya HondaYojiro FurukawaSho Arai
    • C13F300
    • C07H1/08A23L27/34C40B40/00
    • A crystalline mixture solid composition which has almost no hygroscopicity, is easy to handle and dissolve and hardly worn by abrasion, and comprises &agr;-D-glucopyranosyl-1,1-mannitol and &agr;-D-glucopyranosyl-1,6-sorbitol and may further comprise &agr;-D-glucopyranosyl-1,1-sorbitol in a certain case is obtained in an extremely short period of time by a power-saving and labor-saving process with a small-scale apparatus. A composition which comprises 20 to 75 wt % of &agr;-D-glucopyranosyl-1,1-mannitol, 23 to 70 wt % of &agr;-D-glucopyranosyl-1,6-sorbitol and 2 to 25 wt % of &agr;-D-glucopyranosyl-1,1-sorbitol and is in a crystalline mixture solid state or has a specific surface area of 0.07 to 0.1 m2/g, and a composition which comprises 30 to 75 wt % of &agr;-D-glucopyranosyl-l,1-mannitol, 25 to 70 wt % of &agr;-D-glucopyranosyl-1,6-sorbitol and has a specific surface area of 0.07 to 0.1 m2/g. The above compositions are produced by a process comprising supplying a raw material, which is obtained by optionally removing trehalulose from a mixture containing isomaltulose and trehalulose produced from cane sugar through an isomerization reaction and hydrogenating into a kneader having a thin and long cooling zone together with seed crystals and discharging the obtained composition from an outlet continuously.
    • 具有几乎没有吸湿性的结晶混合物固体组合物易于处理和溶解并且几乎不被磨损磨损,并且包括α-D-吡喃葡萄糖基-1,1-甘露醇和α-D-吡喃葡萄糖基-1,6-山梨糖醇,并且还可以包含α 通过小型装置的省电省力的方法,在极短的时间内可以获得一定的D-吡喃葡萄糖基-1,1-山梨醇.1。一种组合物,其含有20〜75重量% α-D-吡喃葡萄糖基-1,1-甘露醇,23〜70重量%的α-D-吡喃葡萄糖基-1,6-山梨醇和2〜25重量%的α-D-吡喃葡萄糖基-1,1-山梨醇, 结晶混合物固态或比表面积为0.07〜0.1m 2 / g,组成为30〜75重量%的α-D-吡喃葡萄糖基-1,1-甘露糖醇,25〜70重量% 的α-D-吡喃葡萄糖基-1,6-山梨糖醇,其比表面积为0.07〜0.1m 2 / g。上述组合物通过包括供给原料的方法制备, 通过任选地通过异构化反应从蔗糖产生的异麦芽酮糖和海藻糖醇的混合物中任选除去海藻糖糖,并将其与晶种一起氢化成具有薄而长的冷却区的捏合机,并连续从出口排出所得组合物。
    • 5. 发明申请
    • Process for producing crystalline maltitol
    • 生产结晶麦芽糖醇的方法
    • US20050220959A1
    • 2005-10-06
    • US10517451
    • 2003-06-16
    • Ryuzo UenoJunya HondaYojiro Furukawa
    • Ryuzo UenoJunya HondaYojiro Furukawa
    • A23L1/236C07H1/00C07H15/04C13B30/02
    • C07H15/04A23L27/34A23V2002/00C07H1/00C13B30/02A23V2250/6416
    • There is provided methods for producing crystalline maltitol without using seed crystals, with good workability, at low costs, and with efficiency in a short time. One of the methods comprises the steps of feeding a first maltitol aqueous solution to a kneader so as to knead and cool it, then feeding a second maltitol aqueous solution having a high solid content in place of the first maltitol aqueous solution and further kneading and cooling the resulting mixture so as to produce a plastic mass, cooling the plastic mass so as to solidify it, and pulverizing the solidified mass. The other method comprises the steps of feeding a maltitol aqueous solution to a kneader so as to knead and cool it, then adding water and further kneading and cooling the mixture so as to produce a plastic mass, cooling the plastic mass so as to solidify it, and pulverizing the solidified mass.
    • 提供了不使用晶种生产结晶麦芽糖醇的方法,具有良好的可加工性,低成本和短时间的效率。 其中一种方法包括以下步骤:将第一麦芽糖醇水溶液加入到捏和机中进行混炼和冷却,然后加入固体含量高的第二麦芽糖醇水溶液代替第一麦芽糖醇水溶液,并进一步混炼和冷却 得到的混合物,以产生塑料块,冷却塑料块使其固化,并粉碎固化的物料。 另一种方法是将麦芽糖醇水溶液进料到捏合机中进行混合和冷却,然后加水并进一步混炼和冷却混合物以产生塑料块,冷却塑料块使其固化 ,并粉碎固化物。