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1. 发明授权

US5112783A Conductive copper oxide ceramics and process for producing same 失效
标题翻译：导电铜氧化物陶瓷及其制造方法
公开(公告)号：US5112783A
公开(公告)日：1992-05-12
申请号：US639931
申请日：1991-01-14
申请人： Ryoji Sugise , Hiroshi Daimon , Itsuhiro Fujii , Hideo Ihara , Norio Terada , Masatoshi Jo , Masayuki Hirabayashi
发明人： Ryoji Sugise , Hiroshi Daimon , Itsuhiro Fujii , Hideo Ihara , Norio Terada , Masatoshi Jo , Masayuki Hirabayashi
IPC分类号： C01G3/00 , C01G15/00 , C04B35/45 , H01B1/08 , H01M4/90
CPC分类号： H01M4/9016 , C01G15/006 , C01G3/006 , C04B35/45 , H01B1/08 , C01P2002/72 , C01P2002/76 , C01P2002/82
摘要： Cubic conductive copper oxide ceramics which are represented by the following formula I:(M.sub.x Cu.sub.y).sub.7 O.sub.z A.sub.w Iwherein M represents at least one element selected from the group consisting of In, Sc, Y, Tl, and Ga, A represents Cl, NO.sub.3, or Cl and NO.sub.3, x+Y is a value of 1, x/y is a number of 0 to 10, z is a number of from 6 to 8, and w is a number of from 1 to 9, and processes for producing same by mixing at least one nitrate and/or chloride of a metal selected from the group consisting of In, Sc, Y, Tl, and Ga, with copper nitrate and/or copper chloride, and firing the mixture at from 200.degree. to 600.degree. C. The copper oxide ceramics are preferably used as electrodes in various fields, heat emiters and also as a material for producing superconductors.
摘要翻译：由下式I表示的立方导电铜氧化物陶瓷：（MxCuy）7OzAw I其中M表示选自In，Sc，Y，Tl和Ga中的至少一种元素，A表示Cl，NO 3或 Cl和NO 3，x + Y为1，x / y为0〜10的数，z为6〜8的数，w为1〜9的数，其制造方法通过将选自In，Sc，Y，Tl和Ga的金属的至少一种硝酸盐和/或氯化物与硝酸铜和/或氯化铜混合，并将混合物在200〜600℃ 铜氧化物陶瓷优选用作各种领域的电极，发热体以及用作制造超导体的材料。

2. 发明申请

US20050038282A1 Process for producing alkyl nitrite 有权
标题翻译：亚硝酸烷基酯的制备方法
公开(公告)号：US20050038282A1
公开(公告)日：2005-02-17
申请号：US10946475
申请日：2004-09-21
申请人： Ryoji Sugise , Shuji Tanaka , Hirofumi Ii , Kazuaki Mii
发明人： Ryoji Sugise , Shuji Tanaka , Hirofumi Ii , Kazuaki Mii
IPC分类号： C07C201/04 , C07C203/00 , C07C23/02
CPC分类号： C07C201/04 , C07C203/00
摘要： An alkyl nitrite is produced with high efficiency by bringing a nitrogen monoxide gas into contact with an aqueous solution of an alkyl alcohol and nitric acid in a reactor 2, which aqueous solution may be a liquid fraction generated in an alkyl nitrite-production process in which an alkyl alcohol is reacted with nitrogen monoxide and oxygen in a reaction column 1.
摘要翻译：通过在反应器2中使一氧化氮气体与烷基醇和硝酸的水溶液接触，可以高效率地生产亚硝酸烷基酯，该水溶液可以是在亚硝酸烷基酯制备方法中产生的液体馏分，其中在反应塔1中使烷基醇与一氧化氮和氧气反应。

3. 发明授权

US6143917A Process for producing aryl carbamates 失效
标题翻译：制备芳基氨基甲酸酯的方法
公开(公告)号：US6143917A
公开(公告)日：2000-11-07
申请号：US171076
申请日：1998-10-13
申请人： Katsumasa Harada , Ryoji Sugise , Kohichi Kashiwagi , Tsunao Matsuura
发明人： Katsumasa Harada , Ryoji Sugise , Kohichi Kashiwagi , Tsunao Matsuura
IPC分类号： C07C269/04 , C07D295/205
CPC分类号： C07D295/205 , C07C269/04
摘要： A process for producing an aryl carbamate of a high purity at a high yield by reacting a diaryl carbonate with an amine compound having one or more hydrogen atoms bonded to the N position in the presence of carboxylic acid(s) of the following general formulae (I): R.sup.1 --COOH and/or (II): R.sup.2 --COOH (wherein R.sup.1 represents an alkyl or cycloalkyl group having an .alpha.-positioned carbon atom bonded to only one hydrogen atom, an alkyl group having an .alpha.-positioned carbon atom bonded to no hydrogen atom, or an aryl or heterocyclic group, and R.sup.2 represents an alkyl group having an .alpha.-positioned carbon atom bonded to two or more hydrogen atoms).
摘要翻译： PCT No.PCT / JP98 / 00592 Sec。 371日期：1998年10月13日 102（e）1998年10月13日日期PCT提交1998年2月13日PCT公布。出版物WO98 / 35936 日期：1998年8月20日一种通过使碳酸二芳基酯与具有一个或多个氢原子的胺化合物在羧酸存在下与N位相结合的方法，以高收率制备高纯度氨基甲酸芳基酯的方法以下通式（I）：R 1 -COOH和/或（II）：R 2 -COOH（其中R 1表示具有仅与一个氢原子键合的α-位置碳原子的烷基或环烷基，具有α 与无氢原子结合的位置碳原子，或芳基或杂环基，R2表示具有与两个或多个氢原子结合的α位碳原子的烷基）。

4. 发明授权

US5648510A Process for preparation of diaryl carbonate 失效
标题翻译：碳酸二芳基酯的制备方法
公开(公告)号：US5648510A
公开(公告)日：1997-07-15
申请号：US627897
申请日：1996-04-03
申请人： Katsumasa Harada , Yoichi Imbe , Keigo Nishihira , Shuji Tanaka , Satoru Fujitsu , Ryoji Sugise , Koichi Kashiwagi , Toshihiko Sumida
发明人： Katsumasa Harada , Yoichi Imbe , Keigo Nishihira , Shuji Tanaka , Satoru Fujitsu , Ryoji Sugise , Koichi Kashiwagi , Toshihiko Sumida
IPC分类号： C07C67/333 , C07C68/00 , C07D307/68 , C07D333/38 , C07C69/96
CPC分类号： C07C67/333 , C07C68/00 , C07D307/68 , C07D333/38
摘要： A diaryl carbonate is prepared at a high yield and a high selectivity by heating a diaryl oxalate in the presence of an organic phosphorous compound to release carbon monoxide therefrom. A halogen atom-containing compound can be employed in combination with the organic phosphorous compound.
摘要翻译：通过在有机磷化合物的存在下加热草酸二芳基酯从而释放一氧化碳，以高产率和高选择性制备碳酸二芳基酯。含卤原子的化合物可以与有机磷化合物组合使用。

5. 发明授权

US06417404B1 Process for continuously producing a cyclododecanone compound 有权
公开(公告)号：US06417404B1
公开(公告)日：2002-07-09
申请号：US09879067
申请日：2001-06-13
申请人： Ryoji Sugise , Shuji Tanaka , Takashi Doi , Masayuki Nishio , Sadao Niida , Tsunao Matsuura
发明人： Ryoji Sugise , Shuji Tanaka , Takashi Doi , Masayuki Nishio , Sadao Niida , Tsunao Matsuura
IPC分类号： C07C4500
CPC分类号： C07C45/58 , C07C49/607 , C07C49/413
摘要： A cyclododecanone compound is continuously produced by feeding a liquid feed containing a corresponding epoxycyclododecane compound and LiBr and/or LiI into a frontmost reaction region of a plurality of reaction regions connected to each other in series; successively passing the liquid feed through the series of reaction regions to catalytically isomerize the epoxycyclododecane compound into a corresponding cyclododecanone compound; and collecting the resultant reaction mixture containing the target cyclododecanone compound from a rearmost reaction region of the series of reaction regions.

6. 发明授权

US5922827A Process for producing a polycarbonate 失效
标题翻译：聚碳酸酯的制造方法
公开(公告)号：US5922827A
公开(公告)日：1999-07-13
申请号：US936666
申请日：1997-09-24
申请人： Keigo Nishihira , Shuji Tanaka , Katsumasa Harada , Ryoji Sugise , Akinori Shiotani , Katsutoshi Washio
发明人： Keigo Nishihira , Shuji Tanaka , Katsumasa Harada , Ryoji Sugise , Akinori Shiotani , Katsutoshi Washio
IPC分类号： C08G64/30 , C08G64/00
CPC分类号： C08G64/307
摘要： A diaryl carbonate is produced by decarbonylating a diaryl oxalate, which can be prepared by transesterification of a dialkyl oxalate with a hydroxyaryl compound, in the presence of a catalyst, while removing the resultant carbon monoxide as a by-product, and then optionally refined by an evaporation and/or distillation, and then the resultant diaryl carbonate is condensation-polymerized with a polyhydroxyl compound, while recovering a resultant hydroxyaryl compound from the reaction system, to produce a polycarbonate.
摘要翻译：碳酸二芳基酯是通过将草酸二芳基酯脱碳化而制得的，该草酸二芳基酯可以在催化剂存在下通过草酸二烷基酯与羟基芳基化合物的酯交换制备，同时除去作为副产物的所得一氧化碳，然后任选地通过蒸发和/或蒸馏，然后将所得碳酸二芳基酯与多羟基化合物缩聚，同时从反应体系中回收得到的羟基芳基化合物，以制备聚碳酸酯。

7. 发明授权

US5731453A Process for producing a diaryl carbonate 失效
标题翻译：制备碳酸二芳基酯的方法
公开(公告)号：US5731453A
公开(公告)日：1998-03-24
申请号：US814089
申请日：1997-03-10
申请人： Keigo Nishihira , Shuji Tanaka , Yuki Nishida , Hirofumi Ii , Satoru Fujitsu , Katsumasa Harada , Ryoji Sugise , Koichi Kashiwagi , Takashi Doi
发明人： Keigo Nishihira , Shuji Tanaka , Yuki Nishida , Hirofumi Ii , Satoru Fujitsu , Katsumasa Harada , Ryoji Sugise , Koichi Kashiwagi , Takashi Doi
IPC分类号： C07C67/02 , C07C67/03 , C07C68/00 , C07C69/36 , C07C69/96
CPC分类号： C07C67/03 , C07C68/00 , Y02P20/127
摘要： A diaryl carbonate with a high degree of purity is produced at a high yield by (A) subjecting (a) a diaryl oxalate and a phenol compound or (b) an alkylaryl oxalate to transesterification reaction in one or two stages in the presence of a catalyst to prepare a diaryl oxalate, while removing a by-product from the reaction system; (B) collecting the diaryl oxalate from the resultant reaction product mixture of the step (A); (C) subjecting the diaryl oxalate to a decarbonylation reaction, preferably in the presence of a phosphorous compound-containing catalyst, to convert the diaryl oxalate to a corresponding diaryl carbonate, while removing a reaction by-product comprising carbon monoxide from the reaction system; and (D) collecting the diaryl carbonate from the reaction product mixture of the step (C).
摘要翻译：通过（A）在（a）草酸二芳基酯和酚化合物或（b）草酸烷基芳基酯在一个或两个阶段中存在下进行酯交换反应，以高产率生产具有高纯度的碳酸二芳基酯催化剂，以制备草酸二芳基酯，同时从反应体系中除去副产物; （B）从所得步骤（A）的反应产物混合物中收集草酸二芳基酯; （C）优选在含磷化合物的催化剂存在下使草酸二芳基酯进行脱羰反应，将草酸二芳基酯转化为相应的碳酸二芳基酯，同时从反应体系中除去包含一氧化碳的反应副产物; 和（D）从步骤（C）的反应产物混合物中收集碳酸二芳基酯。

8. 发明授权

US5466858A Method of producing straight-chain acrylonitrile dimers 失效
标题翻译：制备直链丙烯腈二聚体的方法
公开(公告)号：US5466858A
公开(公告)日：1995-11-14
申请号：US298113
申请日：1994-08-30
申请人： Ryoji Sugise , Kouichi Kashiwagi , Masashi Shirai , Toshihiro Shimakawa
发明人： Ryoji Sugise , Kouichi Kashiwagi , Masashi Shirai , Toshihiro Shimakawa
IPC分类号： C07C63/70 , C07C65/32 , C07C65/34 , C07C253/30
CPC分类号： C07C65/32 , C07C253/30 , C07C65/34 , Y02P20/52
摘要： Straight-chain acrylonitrile dimers including 1,4-dicyanobutene, 1,4-dicyanobutadiene and adiponitrile are produced at a high selectivity by dimerizing acrylonitrile in the presence of a ruthenium catalyst, and in the presence of a straight-chain dimer selectivity-enhancing agent comprising at least one member selected from(A) substituted benzoic acids, except for monoalkylbenzoic acids, having at least one substituent and preferably exhibiting a pKa of 1.50 to 6.0 determined in water at an ionic strength of 0 to 0.1 mole/liter at 25.degree. C.;(B) hetero atom-containing acyclic carboxylic acids having at least one substituent having a sulfur or nitrogen atom attached to a carbon atom located in an .alpha.- on .beta.-position with respect to a carboxyl group in a main hydrocarbon structure; and(C) 5 to 12 membered heterocyclic carboxylic acids having an oxygen, sulfur or nitrogen atom included in a 5 to 12 membered heterocyclic structure and a carboxyl or carboxymethyl group attached to a carbon atom located in an .alpha.-position with respect to the hetero atom.
摘要翻译：通过在钌催化剂的存在下使丙烯腈二聚，并且在直链二聚体选择性增强剂的存在下，以高选择性制备包括1,4-二氰基，1,4-二氰基丁二烯和己二腈的直链丙烯腈二聚体包括至少一种选自（A）取代的苯甲酸，除了单烷基苯甲酸，具有至少一个取代基，并且优选表现出在25℃下在离子强度为0至0.1摩尔/升的水中测定的pKa为1.50至6.0。 C。; （B）具有至少一个具有硫原子或氮原子的取代基的含杂原子的非环状羧酸与位于主烃结构中的羧基上位于β-位上的α-位上的碳原子连接; 和（C）5至12元杂环结构中包含的具有氧，硫或氮原子的5至12元杂环羧酸和连接于位于相对于杂原子的α位的碳原子上的羧基或羧甲基原子。

9. 发明授权

US4625025A Process for producing a 2H-1,3-thiazolidine, 2H-tetrahydro-1,3-thiazine, or 2H-hexahydro-1,3-thiazepine derivative substituted at the 2 position by a nitromethylene group derivative 失效
标题翻译：制备在2位被硝基亚甲基衍生物取代的2H-1,3-噻唑烷，2H-四氢-1,3-噻嗪或2H-六氢-1,3-硫氮杂衍生物的方法
公开(公告)号：US4625025A
公开(公告)日：1986-11-25
申请号：US639919
申请日：1984-08-10
申请人： Fumio Iwata , Katsumasa Harada , Ryoji Sugise
发明人： Fumio Iwata , Katsumasa Harada , Ryoji Sugise
IPC分类号： C07D277/08 , C07D277/10 , C07D279/06 , C07D281/02
CPC分类号： C07D277/10 , C07D279/06 , C07D281/02
摘要： Disclosed is a process for producing a heterocyclic compound having a nitromethylene group as the side chain, of the formula ##STR1## wherein Y represents a hydrogen atom, a halogen atom or a lower alkyl group, R represents a hydrogen atom, an alkyl group, a cycloalkyl group, an aralkyl group, an alkenyl group, an alkynyl group or an acyl group, and n represents an integer of 2, 3 or 4,which comprises reacting a 2,2,2-trihalo-1-nitroethane compound with a 1-aminoalkanethiol compound or a 1-N-substituted derivative thereof.
摘要翻译：本发明公开了一种制备具有硝基亚甲基作为侧链的杂环化合物的方法，其中Y表示氢原子，卤素原子或低级烷基，R表示氢原子，烷基，环烷基，芳烷基，烯基，炔基或酰基，n表示2,3或4的整数，其包括使2,2,2-三卤代-1-硝基乙烷化合物与 1-氨基烷硫醇化合物或其1-N-取代的衍生物。

10. 发明授权

US06861563B2 Process for preparation of cyclododecanone 失效
标题翻译：环十二酮的制备方法
公开(公告)号：US06861563B2
公开(公告)日：2005-03-01
申请号：US10486735
申请日：2002-08-09
申请人： Ryoji Sugise , Shuji Tanaka , Takashi Doi , Masayuki Nishio , Sadao Niida , Tsunao Matsuura
发明人： Ryoji Sugise , Shuji Tanaka , Takashi Doi , Masayuki Nishio , Sadao Niida , Tsunao Matsuura
IPC分类号： C07C45/58 , C07C45/67
CPC分类号： C07C45/58 , C07C49/413
摘要： In the process for producing a cyclododecanone by isomerizing an epoxycyclododecane-containing starting material in the presence of an isomerization reaction catalyst containing lithium bromide and/or lithium iodide, in order to perform the reaction with high efficiency (high reaction rate) and high selectivity and stably produce a high-purity cyclododecanone in industry while maintaining a high-level reaction rate, the epoxycyclododecane-containing starting material is produced by contacting an epoxycyclododecadiene with hydrogen in the presence of a hydrogen-reduction catalyst and has a content of the hydroxyl group-containing cyclododecane compounds contained in the epoxycyclododecane-containing starting material controlled to 5 mol % or less.
摘要翻译：在通过在含有溴化锂和/或碘化锂的异构化反应催化剂的存在下异构化含环氧环十二烷的原料来制备环十二酮的方法中，为了以高效率（高反应速率）和高选择性进行反应，以及在保持高反应速率的同时稳定地生产高纯度环十二烷酮，含环氧环十二烷的原料是通过在氢还原催化剂存在下使环氧环十二烷与氢接触而制得的，含有环氧十二烷的原料中含有的环十二烷化合物控制在5摩尔％以下。

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