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1. 发明授权

US5062966A Process for decomposing solutions of hydroxylammonium salts 失效
标题翻译：分解羟基铵盐溶液的方法
公开(公告)号：US5062966A
公开(公告)日：1991-11-05
申请号：US608416
申请日：1990-11-02
申请人： Ronald L. Dotson , Sanders H. Moore
发明人： Ronald L. Dotson , Sanders H. Moore
IPC分类号： C02F1/58 , C02F1/76 , C02F9/00
CPC分类号： C02F1/76 , C02F1/586 , C02F2101/38 , C02F2209/06 , Y10S210/903
摘要： A process for decomposing a solution of a hydroxylammonium compound includes raising the pH of the solution to about 8 or higher and reacting the alkaline solution with a source of hypohalite ions. The process decomposes solutions of hydroxylammonium salts in a manner which produces benign liquid and gas effluents which can be readily disposed of or discharged.
摘要翻译：用于分解羟基铵化合物溶液的方法包括将溶液的pH提高到约8或更高，并使碱溶液与次卤酸盐离子源反应。该方法以产生良好的液体和气体流出物的方式分解羟基铵盐的溶液，其可以容易地处理或排出。

2. 发明授权

US4470891A Process for removing available halogen from anolyte brine 失效
标题翻译：从阳极电解液盐水中除去可用卤素的方法
公开(公告)号：US4470891A
公开(公告)日：1984-09-11
申请号：US600678
申请日：1984-04-16
申请人： Sanders H. Moore , Ronald L. Dotson
发明人： Sanders H. Moore , Ronald L. Dotson
IPC分类号： C01D3/14 , C25B1/46 , C25B15/08 , C25B1/02 , C25B1/26
CPC分类号： C01D3/145 , C01D3/14 , C25B1/46 , C25B15/08
摘要： A process is disclosed for substantially reducing the dissolved halogen and hypohalite ion concentration in a recycled brine from a membrane electrolytic cell with a closed loop brine system comprising the addition of a non-sulfate generating reducing agent to the brine in a less than conventional stoichiometric molar quantity in relation to each mole of available halogen and hypohalite present in the brine after the steps of dehalogenation, precipitation and pH adjustment.
摘要翻译：公开了一种用于大大降低来自具有闭环盐水系统的膜电解池的再循环盐水中的溶解卤素和次卤酸盐离子浓度的方法，该系统包括在少于常规化学计量摩尔浓度的盐水中加入不产生硫酸盐的还原剂在脱卤，沉淀和pH调节步骤后，存在于盐水中的每摩尔可用卤素和次卤酸盐的量。

3. 发明授权

US4405465A Process for the removal of chlorate and hypochlorite from spent alkali metal chloride brines 失效
标题翻译：从废碱金属氯化物盐水中除去氯酸盐和次氯酸盐的方法
公开(公告)号：US4405465A
公开(公告)日：1983-09-20
申请号：US393578
申请日：1982-06-30
申请人： Sanders H. Moore , Ronald L. Dotson
发明人： Sanders H. Moore , Ronald L. Dotson
IPC分类号： C25B15/08 , C25B1/34
CPC分类号： C25B15/08
摘要： A process is described for reducing the concentration of oxyhalogen impurities in an alkali metal halide brine recovered from an electrolytic cell which comprises circulating the alkali metal halide brine to a treatment zone outside of the electrolytic cell. Within the treatment zone, the alkali metal halide brine is reacted with oxalic acid while maintaining the alkali metal halide brine at a pH of less than about 4.5. A purified brine having a substantially reduced concentration of oxyhalogen impurities is recovered from the treatment zone. The process may be employed in treating brines recovered from mercury cells and membrane cells for the production of chlorine and alkali metal hydroxides and its employment results in a substantial reduction in the amount of concentrated acid required in brine treatment and a reduction in energy costs for brine purification.
摘要翻译：描述了一种用于降低从电解池回收的碱金属卤化物盐水中的卤代卤素杂质的浓度的方法，该方法包括将碱金属卤化物盐水循环到电解池外部的处理区。在处理区内，碱金属卤化物盐水与草酸反应，同时保持碱金属卤化物盐水的pH低于约4.5。从处理区回收具有显着降低的卤代卤素杂质浓度的纯化盐水。该方法可用于处理从汞电池和膜电池回收的用于生产氯和碱金属氢氧化物的盐水，并且其使用导致盐水处理中所需的浓缩酸的量的显着减少以及盐水能量成本的降低纯化。

4. 发明授权

US5651951A Hydroxylammonium nitrate free of ammonium nitrate 失效
标题翻译：硝酸铵不含硝酸铵
公开(公告)号：US5651951A
公开(公告)日：1997-07-29
申请号：US445480
申请日：1995-05-22
申请人： David W. Cawlfield , Ronald L. Dotson , Harry J. Loftis , Sanders H. Moore , Robert T. Brooker , Jay S. Stirrat
发明人： David W. Cawlfield , Ronald L. Dotson , Harry J. Loftis , Sanders H. Moore , Robert T. Brooker , Jay S. Stirrat
IPC分类号： C01B21/14 , C01B21/20
CPC分类号： C01B21/1454
摘要： The present invention relates to a multi-step process for producing HAN that is free of ammonium nitrate. The process comprises the steps of: (a) stripping ammonia from an ammonia-containing, aqueous hydroxylamine solution having a hydroxylamine concentration of at least 10% by weight based upon the weight of the hydroxylamine solution, by contacting the ammonia-containing hydroxylamine solution with a stripping agent selected from the group consisting of inert gases and steam to provide an ammonia-free, aqueous hydroxylamine solution, and (b) reacting the ammonia-free, aqueous hydroxylamine solution with aqueous nitric acid having an acid concentration of at least about 0.1%, preferably at least about 20%, based upon the weight of the aqueous nitric acid, to produce ammonium nitrate-free HAN. In another process embodiment of the invention, the above-described ammonia stripping step is not required, and the hydroxylamine concentration is at least about 0.5%, based upon the weight of the reaction mixture employed. Also disclosed is the ammonium nitrate-free HAN product produced by the process of this invention.
摘要翻译：本发明涉及一种不含硝酸铵的生产HAN的多步法。该方法包括以下步骤：（a）通过使含氨的羟胺溶液与含羟胺的羟胺溶液接触，从基于羟胺溶液重量的羟胺浓度至少为10重量％的含氨基羟胺溶液中除去氨选自惰性气体和蒸汽的汽提剂，以提供无氨的羟胺水溶液，和（b）使无氨水羟胺溶液与酸浓度为至少约0.1的硝酸水溶液反应％，优选至少约20％，基于硝酸水溶液的重量，以产生不含硝酸铵的HAN。在本发明的另一方法实施方案中，不需要上述氨汽提步骤，并且基于所用反应混合物的重量，羟胺浓度为至少约0.5％。还公开了通过本发明的方法生产的不含硝酸铵的HAN产物。

5. 发明授权

US5510097A Hydroxylammonium nitrate free of ammonium nitrate 失效
标题翻译：硝酸铵不含硝酸铵
公开(公告)号：US5510097A
公开(公告)日：1996-04-23
申请号：US245928
申请日：1994-05-19
申请人： David W. Cawlfield , Ronald L. Dotson , Harry J. Loftis , Sanders H. Moore , Robert T. Brooker , Jay S. Stirrat
发明人： David W. Cawlfield , Ronald L. Dotson , Harry J. Loftis , Sanders H. Moore , Robert T. Brooker , Jay S. Stirrat
IPC分类号： C01B21/14 , C01B21/20
CPC分类号： C01B21/1454
摘要： The present invention relates to a multi-step process for producing HAN that is free of ammonium nitrate. The process comprises the steps of: (a) stripping ammonia from an ammonia-containing, aqueous hydroxylamine solution having a hydroxylamine concentration of at least 10% by weight based upon the weight of the hydroxylamine solution, by contacting the ammonia-containing hydroxylamine solution with a stripping agent selected from the group consisting of inert gases and steam to provide an ammonia-free, aqueous hydroxylamine solution, and (b) reacting the ammonia-free, aqueous hydroxylamine solution with aqueous nitric acid having an acid concentration of at least about 0.1%, preferably at least about 20%, based upon the weight of the aqueous nitric acid, to produce ammonium nitrate-free HAN. In another process embodiment of the invention, the above-described ammonia stripping step is not required, and the hydroxylamine concentration is at least about 0.5%, based upon the weight of the reaction mixture employed. Also disclosed is the ammonium nitrate-free HAN product produced by the process of this invention.
摘要翻译：本发明涉及一种不含硝酸铵的生产HAN的多步法。该方法包括以下步骤：（a）通过使含氨的羟胺溶液与含羟胺的羟胺溶液接触，从基于羟胺溶液重量的羟胺浓度至少为10重量％的含氨基羟胺溶液中除去氨选自惰性气体和蒸汽的汽提剂，以提供无氨的羟胺水溶液，和（b）使无氨水羟胺溶液与酸浓度为至少约0.1的硝酸水溶液反应％，优选至少约20％，基于硝酸水溶液的重量，以产生不含硝酸铵的HAN。在本发明的另一方法实施方案中，不需要上述氨汽提步骤，并且基于所用反应混合物的重量，羟胺浓度为至少约0.5％。还公开了通过本发明的方法生产的不含硝酸铵的HAN产物。

6. 发明授权

US4481088A Removal of chlorate from electrolyte cell brine 失效
标题翻译：从电解池盐水中去除氯酸盐
公开(公告)号：US4481088A
公开(公告)日：1984-11-06
申请号：US395753
申请日：1982-07-06
申请人： Sanders H. Moore , Ronald L. Dotson
发明人： Sanders H. Moore , Ronald L. Dotson
IPC分类号： C25B1/46 , C25B15/08 , C25B1/16
CPC分类号： C25B15/08
摘要： A process for removing chlorate ions from a recirculating anolyte brine as typically used in membrane chlor-alkali cells is disclosed. In this, a portion of the circulating brine after dechlorination and resaturation with additional alkali metal chloride is diverted and treated with a stoichiometric amount of hydrochloric acid to convert substantially all of the chlorate to chlorine gas and chloride ion. When performed in this manner, substantially lower quantities of acid are required as compared to prior art processes and the problems with the generation of ClO.sub.2 are minimized.
摘要翻译：公开了通常用于膜氯碱电池中的从再循环阳极电解液盐水中除去氯酸根离子的方法。在此，一部分循环盐水在脱氯并用另外的碱金属氯化物再饱和之后转移并用化学计量的盐酸处理以将基本上所有的氯酸盐转化为氯气和氯离子。当以这种方式进行时，与现有技术的方法相比，需要相当少量的酸，并且使产生ClO 2的问题最小化。

7. 发明授权

US5294417A Process for removal of mercury from hydroxyl-ammonium nitrate solutions 失效
标题翻译：从硝酸铵溶液中除去汞的方法
公开(公告)号：US5294417A
公开(公告)日：1994-03-15
申请号：US864244
申请日：1992-04-06
申请人： Sanders H. Moore , James F. Pickering , Ronald L. Dotson , Carey O. Burger , Jeffery D. Casteel , Phillip J. Reed , Richard E. Mellor
发明人： Sanders H. Moore , James F. Pickering , Ronald L. Dotson , Carey O. Burger , Jeffery D. Casteel , Phillip J. Reed , Richard E. Mellor
IPC分类号： C01G13/00 , C02F1/70 , C02F9/00 , C02F1/76
CPC分类号： C02F9/00 , C01G13/00 , C02F1/70 , C02F2101/20
摘要： A process for the removal of mercury from industrial waste streams is disclosed wherein the waste stream is a nitrate based solution that has been decomposed by the addition of hypochlorite. The method involves adding a reducing agent to reduce the hypochlorite and/or adjusting the pH by the use of a strong acid to less than about 2.0, converting any residual chlorine to a soluble unreactive salt, adding a soluble precipitating agent, such as sodium sulfide, to the solution in a ratio to the mercury present of greater than 1:1 to about 2:1 to precipitate out the mercury as a mercury compound. The solution is then filtered to remove the precipitated mercury compound.
摘要翻译：公开了从工业废物流中除去汞的方法，其中废物流是通过加入次氯酸盐分解的基于硝酸盐的溶液。该方法包括加入还原剂以减少次氯酸盐和/或通过使用强酸调节pH至小于约2.0，将任何残留的氯转化为可溶性非反应性盐，加入可溶性沉淀剂如硫化钠以与汞存在的比例大于1:1至约2:1的溶液沉淀出汞作为汞化合物。然后过滤溶液以除去沉淀的汞化合物。

8. 发明授权

US4578195A Process for the purification of effluents and purge streams containing trace elements 失效
标题翻译：净化含微量元素的污水和净化流的方法
公开(公告)号：US4578195A
公开(公告)日：1986-03-25
申请号：US634837
申请日：1984-07-26
申请人： Sanders H. Moore , Maurice R. Smith , Harvey B. Cochran
发明人： Sanders H. Moore , Maurice R. Smith , Harvey B. Cochran
IPC分类号： C02F1/28
CPC分类号： C02F1/285 , C22B3/24 , Y02P10/234 , Y10S210/906 , Y10S210/911 , Y10S210/912 , Y10S210/913 , Y10S210/914
摘要： An improved process for treating aqueous effluents and purge streams to selectively remove polluting elements such as iron, copper, lead and mercury therefrom is described. The procedure comprises contacting the effluent with a poly(dithiocarbamate) chelating agent whereby the polluting elements are absorbed. The resin is extracted with an acidic aqueous solution having a pH of from about 4 to about 6; and removing the resin. When this is done, the residual content of these polluting elements in the effluent is reduced to a level below EPA required levels so that the effluent can safely be discharged into the surrounding ecosystem. The poly(dithiocarbamate) resin containing the polluting elements can be disposed of, for example, by being deposited in an unsecured landfill.
摘要翻译：描述了一种用于处理含水排出物和吹扫流以从其中选择性地去除污染元素如铁，铜，铅和汞的改进方法。该方法包括使流出物与聚（二硫代氨基甲酸盐）螯合剂接触，从而吸收污染元素。树脂用pH为约4至约6的酸性水溶液萃取; 并除去树脂。当这样做时，污水中这些污染物质的残留含量降低到低于EPA所需水平的水平，以便流出物可以安全地排放到周围的生态系统中。含有污染元素的聚（二硫代氨基甲酸酯）树脂可以例如通过沉积在不安全的填埋场中来处理。

9. 发明授权

US5779269A Propellant module assembly 失效
标题翻译：推进剂组件
公开(公告)号：US5779269A
公开(公告)日：1998-07-14
申请号：US761296
申请日：1996-12-06
申请人： Sanders H. Moore , Brian D. Sharpe
发明人： Sanders H. Moore , Brian D. Sharpe
IPC分类号： B60R21/263 , B60R21/264 , C06B31/00 , B60R21/26
CPC分类号： B60R21/264 , C06B31/00 , B60R2021/2633
摘要： A propellant module assembly is adapted for containing a liquid propellant which is used to inflate a vehicular air bag. The module assembly includes an igniter; a liquid propellant; a propellant and igniter capsule; and a rupturable closure member. The capsule and rupturable member are compatible with, and will not deteriorate as a result of contact with the liquid propellant. The liquid propellant, when ignited, will not produce toxic gases, and will not subject vehicle occupants to the possibility of chemical burns, as can occur with solid propellants.
摘要翻译：推进剂模块组件适于容纳用于使车辆气囊膨胀的液体推进剂。模块组件包括点火器; 液体推进剂; 推进剂和点火器胶囊; 和可破裂的封闭构件。胶囊和可破裂构件与液体推进剂的接触相容并且不会劣化。液体推进剂在点燃时不会产生有毒气体，并且不会使车辆乘客发生化学燃烧的可能性，如固体推进剂可能发生的那样。

10. 发明授权

US4397720A Removal of chlorate and hypochlorite from electrolyte cell brine 失效
标题翻译：从电解质盐水中去除氯酸盐和次氯酸盐
公开(公告)号：US4397720A
公开(公告)日：1983-08-09
申请号：US426336
申请日：1982-09-29
申请人： Sanders H. Moore , Maurice R. Smith
发明人： Sanders H. Moore , Maurice R. Smith
IPC分类号： C25B15/08 , C25B1/34
CPC分类号： C25B15/08
摘要： A process for removing chlorate ions from a recirculating anolyte brine as typically used in membrane chlor-alkali cells is disclosed. In this, a portion of the circulating brine after dechlorination and resaturation with additional alkali metal chloride is diverted and treated with an acidified aliphatic aldehyde to convert substantially all of the hypochlorite and chlorate to chlorine dioxide, chlorine gas and chloride ion. When performed in this manner, substantially lower quantities of acid are required as compared to prior art processes and the problems with the generation of excessive quantities of ClO.sub.2 are minimized.
摘要翻译：公开了通常用于膜氯碱电池中的从再循环阳极电解液盐水中除去氯酸根离子的方法。在此，一部分循环盐水在脱氯并用另外的碱金属氯化物再饱和后被转移并用酸化的脂族醛处理，以将基本上所有的次氯酸盐和氯酸盐转化成二氧化氯，氯气和氯离子。当以这种方式进行时，与现有技术方法相比，需要相当少量的酸，并且产生过量ClO 2的问题被最小化。

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