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1. 发明申请

US20140081041A1 COPPER-PROMOTED SHELL CATALYST FOR PRODUCING ALKENYL CARBOXYLIC ACID ESTERS 有权
标题翻译：用于生产烷基羧酸酯的铜促销壳催化剂
公开(公告)号：US20140081041A1
公开(公告)日：2014-03-20
申请号：US14031587
申请日：2013-09-19
申请人： Roman Bobka , Gerhard Mestl , Peter Scheck , Carolin Fischer , Martin Schoenfelder
发明人： Roman Bobka , Gerhard Mestl , Peter Scheck , Carolin Fischer , Martin Schoenfelder
IPC分类号： C07C67/055 , B01J23/66 , B01J23/89
CPC分类号： C07C67/055 , B01J23/626 , B01J23/66 , B01J23/8926 , B01J23/8946 , B01J35/002 , B01J35/008 , B01J35/108 , B01J37/0242 , B01J37/0244 , B01J37/18 , Y02P20/582 , C07C69/15
摘要： A method for producing a shell catalyst which is suitable for the synthesis of alkenyl carboxylic acid esters, in particular for producing vinyl acetate monomer (VAM) from ethylene or allyl acetate monomer from propylene by means of oxy-acetylation. Also, a shell catalyst that can be obtained by the method according to the invention, as well as the use of the shell catalyst produced using the method for producing alkenyl carboxylic acid esters, in particular vinyl acetate monomer (VAM) and allyl acetate monomer.
摘要翻译：一种适用于合成链烯基羧酸酯的壳催化剂的制备方法，特别是通过氧乙酰化由乙烯或乙酸烯丙酯单体由丙烯生产乙酸乙烯酯单体（VAM）的方法。此外，可以通过本发明的方法获得的壳催化剂以及使用制备烯基羧酸酯，特别是乙酸乙烯酯单体（VAM）和乙酸烯丙酯单体的方法制备的壳催化剂的用途。

2. 发明申请

US20150031911A1 Post-Gilding of PD-AU-Coated Shell Catalysts 有权
标题翻译： PD-AU涂层壳催化剂后镀金
公开(公告)号：US20150031911A1
公开(公告)日：2015-01-29
申请号：US14379262
申请日：2013-02-19
申请人： Gerhard Mestl , Peter Scheck , Alfred Hagemeyer , Carolin Fischer , Roman Bobka
发明人： Gerhard Mestl , Peter Scheck , Alfred Hagemeyer , Carolin Fischer , Roman Bobka
IPC分类号： B01J31/28 , C07C67/05 , B01J31/38
CPC分类号： B01J31/28 , B01J23/52 , B01J23/58 , B01J31/38 , B01J35/008 , B01J37/0205 , B01J37/18 , B01J2231/49 , C07C67/05 , C07C67/055 , C07C69/15
摘要： The invention relates to a method for producing a shell catalyst that is suitable for producing vinyl acetate monomer (VAM). The invention further relates to a shell catalyst that is obtainable by the method according to the invention and to the use of the shell catalyst according to the invention for producing VAM.
摘要翻译：本发明涉及适用于生产乙酸乙烯酯单体（VAM）的壳催化剂的制备方法。本发明还涉及通过根据本发明的方法获得的壳催化剂以及根据本发明的壳催化剂用于生产VAM的用途。

3. 发明授权

US09873114B2 Post-gilding of PD-AU-coated shell catalysts 有权
公开(公告)号：US09873114B2
公开(公告)日：2018-01-23
申请号：US14379262
申请日：2013-02-19
申请人： Gerhard Mestl , Peter Scheck , Alfred Hagemeyer , Carolin Fischer , Roman Bobka
发明人： Gerhard Mestl , Peter Scheck , Alfred Hagemeyer , Carolin Fischer , Roman Bobka
IPC分类号： B01J31/28 , B01J37/18 , B01J37/02 , B01J23/52 , B01J23/58 , B01J35/00 , C07C67/055 , B01J31/38 , C07C67/05
CPC分类号： B01J31/28 , B01J23/52 , B01J23/58 , B01J31/38 , B01J35/008 , B01J37/0205 , B01J37/18 , B01J2231/49 , C07C67/05 , C07C67/055 , C07C69/15
摘要： The invention relates to a method for producing a shell catalyst that is suitable for producing vinyl acetate monomer (VAM). The invention further relates to a shell catalyst that is obtainable by the method according to the invention and to the use of the shell catalyst according to the invention for producing VAM.

4. 发明授权

US09849442B2 Method for producing a metal-containing shell catalyst without intermediate calcining 有权
公开(公告)号：US09849442B2
公开(公告)日：2017-12-26
申请号：US13468442
申请日：2012-05-10
申请人： Alfred Hagemeyer , Peter Scheck , Gerhard Mestl , Alice Kyriopoulos , Carolin Fischer
发明人： Alfred Hagemeyer , Peter Scheck , Gerhard Mestl , Alice Kyriopoulos , Carolin Fischer
IPC分类号： B01J37/02 , B01J37/08 , B01J37/16 , B01J37/18 , B01J23/42 , B01J23/44 , B01J23/50 , B01J23/66 , B01J35/00 , B01J23/52 , B01J23/58 , C07C67/055 , B01J21/04 , B01J21/08
CPC分类号： B01J23/42 , B01J21/04 , B01J21/08 , B01J23/44 , B01J23/50 , B01J23/52 , B01J23/58 , B01J23/66 , B01J35/008 , B01J37/0221 , B01J37/08 , B01J37/16 , C07C67/055 , Y02P20/582 , C07C69/15
摘要： A method for producing a shell catalyst which comprises, in the outer shell, one or more of the following metals: Pd, Pt, Ag and Au. Also the use of the shell catalyst produced using the method according to the invention for the production of vinyl acetate monomer, in the hydrogenation of hydrocarbons, in particular the selective hydrogenation of polyunsaturated hydrocarbon compounds, or in the oxidation of alcohols to ketones/aldehydes/carboxylic acids.

5. 发明申请

US20130172603A1 METHOD FOR PRODUCING A SHELL CATALYST AND SHELL CATALYST 审中-公开
标题翻译：制备壳催化剂和壳催化剂的方法
公开(公告)号：US20130172603A1
公开(公告)日：2013-07-04
申请号：US13808712
申请日：2011-07-07
申请人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck , Alice Kyriopoulos , Carolin Fischer
发明人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck , Alice Kyriopoulos , Carolin Fischer
IPC分类号： B01J21/16
CPC分类号： B01J21/16 , B01J21/066 , B01J21/08 , B01J23/52 , B01J23/58 , B01J35/002 , B01J35/008 , B01J35/08 , B01J37/0221 , B01J37/024 , B01J37/035 , B01J37/06 , B01J37/18 , B01J2219/00247 , C07C67/04 , C07C69/15
摘要： A method for producing a shell catalyst is provided which comprises a porous catalyst support shaped body with an outer shell in which at least one transition metal in metal form is contained, comprising: providing catalyst support shaped bodies; applying a transition-metal precursor compound to an outer shell of the catalyst support shaped bodies; and converting the metal component of the transition-metal precursor compound into the metal form by reduction in a process gas at a temperature of from 50 to 500° C., wherein the temperature and the duration of the reduction are chosen such that the product of reduction temperature in ° C. and reduction time in hours lies in a range of from 50 to 5000, more preferably 80 to 2500, further preferably 80 to 2000, and more preferably 100 to 1500.
摘要翻译：提供一种制备壳催化剂的方法，其包括具有外壳的多孔催化剂载体成形体，其中包含至少一种金属形式的过渡金属，其包括：提供催化剂载体成形体; 将过渡金属前体化合物施加到催化剂载体成形体的外壳上; 并且通过在50-500℃的温度下还原处理气体将过渡金属前体化合物的金属组分转化为金属形式，其中选择温度和还原的持续时间使得产物还原温度以℃为单位，还原时间以小时为50-5000倍，更优选为80-2,500，进一步优选为80-2000，更优选为100-1500。

6. 发明授权

US08586780B2 Doped Pd/Au shell catalyst, method for producing the same and use thereof 失效
标题翻译：掺杂Pd / Au壳催化剂及其制备方法及其用途
公开(公告)号：US08586780B2
公开(公告)日：2013-11-19
申请号：US12601419
申请日：2008-05-30
申请人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
发明人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
IPC分类号： C07C67/04 , B01J23/00 , B01J21/00
CPC分类号： B01J23/66 , B01J21/16 , B01J23/56 , B01J23/8906 , B01J23/8946 , B01J35/002 , B01J35/008 , B01J35/08 , B01J35/10 , B01J35/1014 , B01J35/1019 , B01J35/1038 , B01J35/1042 , B01J35/1061 , B01J35/108 , B01J37/0018 , B01J37/0205 , B01J37/0207 , B01J37/0221 , C07C67/055 , C07C69/01 , C07C69/15
摘要： A shell catalyst for producing vinyl acetate monomer (VAM), comprising an oxidic porous catalyst support, formed as a shaped body, with an outer shell in which metallic Pd and Au are contained. To provide a shell catalyst for producing VAM which has a relatively high activity and can be obtained at relatively low cost, the catalyst support is doped with at least one oxide of an element selected from the group consisting of Li, P, Ca, V, Cr, Mn, Fe, Sr, Nb, Ta, W, La and the rare-earth metals.
摘要翻译：一种用于生产乙酸乙烯酯单体（VAM）的壳催化剂，其包含形成为成形体的氧化多孔催化剂载体，其中包含金属Pd和Au的外壳。为了提供具有较高活性并可以相对低成本获得的VAM的壳催化剂，催化剂载体上掺杂有选自Li，P，Ca，V， Cr，Mn，Fe，Sr，Nb，Ta，W，La和稀土金属。

7. 发明授权

US08466082B2 PD/AU shell catalyst containing HFO2, processes for the preparation and use thereof 失效
标题翻译：含有HFO2的PD / AU壳催化剂，其制备方法和用途
公开(公告)号：US08466082B2
公开(公告)日：2013-06-18
申请号：US12601399
申请日：2008-05-30
申请人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
发明人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
IPC分类号： B01J20/00 , B01J21/00 , B01J21/04 , B01J23/00 , B01J23/02 , B01J23/04 , B01J23/08 , B01J23/40 , B01J23/42 , B01J23/44 , B01J23/56 , B01J23/58
CPC分类号： B01J21/16 , B01J21/06 , B01J21/066 , B01J23/66 , B01J35/0006 , B01J35/002 , B01J35/008 , B01J35/08 , B01J35/1019 , B01J35/1038 , B01J35/1061 , B01J37/0036 , B01J37/0221 , B01J37/0242 , B01J37/0248 , B01J37/04 , C07C67/055 , C07C69/01 , C07C69/15
摘要： A shell catalyst for the preparation of vinyl acetate monomer, comprising an oxidic porous catalyst support with an outer shell, containing metallic Pd and Au, wherein the framework structure of the porous catalyst support contains hafnium oxide units. This shell catalyst is suitable for the preparation of VAM and is characterized by a relatively high activity and VAM selectivity and maintains this activity and selectivity over relatively long service lives. Also, processes for the preparation and use of the shell catalyst.
摘要翻译：一种用于制备乙酸乙烯酯单体的壳催化剂，其包含含有金属Pd和Au的外壳的氧化多孔催化剂载体，其中多孔催化剂载体的骨架结构含有氧化铪单元。该壳催化剂适用于制备VAM，其特征在于相对较高的活性和VAM选择性，并且在相对较长的使用寿命中保持该活性和选择性。另外，壳催化剂的制备和使用方法。

8. 发明申请

US20140113806A1 BASIC CATALYST SUPPORT BODY HAVING A LOW SURFACE AREA 审中-公开
标题翻译：基础催化剂支撑体具有低表面积
公开(公告)号：US20140113806A1
公开(公告)日：2014-04-24
申请号：US14113684
申请日：2012-04-25
申请人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck , Peter Bauer , Andreas Pritzl
发明人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck , Peter Bauer , Andreas Pritzl
IPC分类号： B01J23/66
CPC分类号： B01J23/66 , B01J21/066 , B01J21/08 , B01J23/44 , B01J23/52 , B01J35/002 , B01J35/0026 , B01J35/026 , B01J35/08 , B01J35/1014 , B01J35/1019 , B01J35/1038 , B01J35/1042 , B01J35/1061 , B01J37/0205 , B01J37/0207 , C07C67/055 , C07C69/15
摘要： A catalyst support body containing an SiO2-containing material and a metal selected from the group consisting of alkali metals, alkaline earth metals, rare earth metals and mixtures thereof, wherein the total metal content lies in the range of from 0.5 to 10 wt.-%, relative to the total weight of the catalyst support. Also, a catalyst that comprises a catalyst support body according to the invention and a catalytically active metal, in particular palladium and/or gold. Also, a method for producing a catalyst support, wherein an SiO2-containing material is treated with a metal-containing compound, dried and then calcined. Also, a method for producing a catalyst, in which a solution having a precursor compound of a catalytically active metal is applied to a catalyst support body.
摘要翻译：一种催化剂载体，其含有含SiO 2的材料和选自碱金属，碱土金属，稀土金属及其混合物的金属，其中总金属含量在0.5-10重量％的范围内，％，相对于催化剂载体的总重量。而且，包含根据本发明的催化剂载体和催化活性金属，特别是钯和/或金的催化剂。另外，制备催化剂载体的方法，其中含金属的材料用含金属的化合物处理，干燥然后煅烧。另外，在催化剂载体上涂布具有催化活性金属的前体化合物的溶液的催化剂的制造方法。

9. 发明申请

US20100261603A1 METHOD FOR THE PRODUCTION OF A SHELL CATALYST LOADED WITH PD AND/OR AU 审中-公开
标题翻译：用PD和/或AU加载壳体催化剂的方法
公开(公告)号：US20100261603A1
公开(公告)日：2010-10-14
申请号：US12601900
申请日：2008-05-30
申请人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
发明人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
IPC分类号： B01J23/44 , B01J23/52
CPC分类号： B01J37/031 , B01J23/44 , B01J23/52 , B01J23/66 , B01J35/008 , B01J35/026 , B01J37/0221 , B01J37/024
摘要： The present invention relates to a process for the production of a shell catalyst which comprises a catalyst support shaped body with an outer shell in which metallic Pd and/or Au is contained. In order to provide a process by means of which shell catalysts can be obtained, in the outer shell of which relatively high metallic Pd and/or Au contents are contained, a process is proposed comprising the steps of a) providing a porous catalyst support shaped body; b) providing a first solution in which a Pd and/or an Au precursor compound is contained; c) providing a second solution in which a Pd and/or a Au precursor compound is contained, wherein the first solution brings about a precipitation of the noble-metal component(s) of the second solution and the second solution a precipitation of the noble-metal component(s) of the first solution; d) loading the catalyst support shaped body with the first and with the second solution; e) converting the noble-metal component(s) precipitated on the catalyst support body into the metal form.
摘要翻译：本发明涉及一种壳催化剂的制备方法，其包括具有外壳的催化剂载体成形体，其中包含金属Pd和/或Au。为了提供可以获得壳催化剂的方法，在其包含相对高的金属Pd和/或Au含量的外壳中，提出了一种方法，包括以下步骤：a）提供多孔催化剂载体，其形状身体; b）提供其中包含Pd和/或Au前体化合物的第一溶液; c）提供其中包含Pd和/或Au前体化合物的第二溶液，其中第一溶液导致第二溶液的贵金属组分的沉淀和第二溶液沉淀贵金属 - 第一溶液的金属组分; d）用第一和第二溶液装载催化剂载体成形体; e）将催化剂载体上沉淀的贵金属组分转化为金属形式。

10. 发明申请

US20100190638A1 Method For Producing A Shell Catalyst and Corresponding Shell Catalyst 审中-公开
标题翻译：生产壳催化剂和相应壳催化剂的方法
公开(公告)号：US20100190638A1
公开(公告)日：2010-07-29
申请号：US12602026
申请日：2008-05-30
申请人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck , Silvia Neumann
发明人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck , Silvia Neumann
IPC分类号： B01J23/66 , B01J23/00 , B01J21/08 , B01J21/04 , B01J21/06 , B01J23/20 , B01J23/40 , B01J23/48 , B01J23/44 , B01J23/50 , B01J23/755 , B01J23/72 , B01J31/20 , B01J23/30 , B01J23/58 , B01J23/745 , B01J8/08
CPC分类号： B01J35/008 , B01J23/42 , B01J23/44 , B01J23/50 , B01J23/52 , B01J23/58 , B01J23/72 , B01J23/75 , B01J23/755 , B01J35/002 , B01J35/0066 , B01J35/08 , B01J35/10 , B01J35/1014 , B01J35/1038 , B01J35/1042 , B01J35/1061 , B01J35/108 , B01J37/0221 , B01J37/16
摘要： A method for producing a shell catalyst comprising a porous catalyst support shaped body with an outer shell containing at least one transition metal in metal form. To provide a shell catalyst with a relatively small shell thickness, a device is set up to circulate the catalyst support shaped bodies by means of process gases with a reductive effect. The device is charged with catalyst support shaped bodies that are circulated by means of a process gas with a reductive effect, an outer shell of the catalyst support shaped bodies is impregnated with a transition-metal precursor compound by spraying the circulating catalyst support shaped bodies with a solution containing the transition-metal precursor compound, the metal component of the transition-metal precursor compound is converted into the metal form by reduction by means of the process gas, and the catalyst support shaped bodies sprayed with the solution are dried.
摘要翻译：一种壳催化剂的制备方法，其包括多孔催化剂载体成型体，其外壳含有至少一种金属形式的过渡金属。为了提供具有相对小的壳厚度的壳催化剂，设置了一种通过具有还原效应的工艺气体循环催化剂载体成形体的装置。该装置装有催化剂载体成型体，其通过具有还原作用的工艺气体循环，催化剂载体成形体的外壳用过渡金属前体化合物浸渍，通过将循环催化剂载体成形体喷涂将过渡金属前体化合物的溶液，过渡金属前体化合物的金属成分通过用工艺气体还原而转变为金属形式，并且将溶液喷射的催化剂载体成形体干燥。

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