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1. 发明申请

US20140113806A1 BASIC CATALYST SUPPORT BODY HAVING A LOW SURFACE AREA 审中-公开
标题翻译：基础催化剂支撑体具有低表面积
公开(公告)号：US20140113806A1
公开(公告)日：2014-04-24
申请号：US14113684
申请日：2012-04-25
申请人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck , Peter Bauer , Andreas Pritzl
发明人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck , Peter Bauer , Andreas Pritzl
IPC分类号： B01J23/66
CPC分类号： B01J23/66 , B01J21/066 , B01J21/08 , B01J23/44 , B01J23/52 , B01J35/002 , B01J35/0026 , B01J35/026 , B01J35/08 , B01J35/1014 , B01J35/1019 , B01J35/1038 , B01J35/1042 , B01J35/1061 , B01J37/0205 , B01J37/0207 , C07C67/055 , C07C69/15
摘要： A catalyst support body containing an SiO2-containing material and a metal selected from the group consisting of alkali metals, alkaline earth metals, rare earth metals and mixtures thereof, wherein the total metal content lies in the range of from 0.5 to 10 wt.-%, relative to the total weight of the catalyst support. Also, a catalyst that comprises a catalyst support body according to the invention and a catalytically active metal, in particular palladium and/or gold. Also, a method for producing a catalyst support, wherein an SiO2-containing material is treated with a metal-containing compound, dried and then calcined. Also, a method for producing a catalyst, in which a solution having a precursor compound of a catalytically active metal is applied to a catalyst support body.
摘要翻译：一种催化剂载体，其含有含SiO 2的材料和选自碱金属，碱土金属，稀土金属及其混合物的金属，其中总金属含量在0.5-10重量％的范围内，％，相对于催化剂载体的总重量。而且，包含根据本发明的催化剂载体和催化活性金属，特别是钯和/或金的催化剂。另外，制备催化剂载体的方法，其中含金属的材料用含金属的化合物处理，干燥然后煅烧。另外，在催化剂载体上涂布具有催化活性金属的前体化合物的溶液的催化剂的制造方法。

2. 发明授权

US08586780B2 Doped Pd/Au shell catalyst, method for producing the same and use thereof 失效
标题翻译：掺杂Pd / Au壳催化剂及其制备方法及其用途
公开(公告)号：US08586780B2
公开(公告)日：2013-11-19
申请号：US12601419
申请日：2008-05-30
申请人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
发明人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
IPC分类号： C07C67/04 , B01J23/00 , B01J21/00
CPC分类号： B01J23/66 , B01J21/16 , B01J23/56 , B01J23/8906 , B01J23/8946 , B01J35/002 , B01J35/008 , B01J35/08 , B01J35/10 , B01J35/1014 , B01J35/1019 , B01J35/1038 , B01J35/1042 , B01J35/1061 , B01J35/108 , B01J37/0018 , B01J37/0205 , B01J37/0207 , B01J37/0221 , C07C67/055 , C07C69/01 , C07C69/15
摘要： A shell catalyst for producing vinyl acetate monomer (VAM), comprising an oxidic porous catalyst support, formed as a shaped body, with an outer shell in which metallic Pd and Au are contained. To provide a shell catalyst for producing VAM which has a relatively high activity and can be obtained at relatively low cost, the catalyst support is doped with at least one oxide of an element selected from the group consisting of Li, P, Ca, V, Cr, Mn, Fe, Sr, Nb, Ta, W, La and the rare-earth metals.
摘要翻译：一种用于生产乙酸乙烯酯单体（VAM）的壳催化剂，其包含形成为成形体的氧化多孔催化剂载体，其中包含金属Pd和Au的外壳。为了提供具有较高活性并可以相对低成本获得的VAM的壳催化剂，催化剂载体上掺杂有选自Li，P，Ca，V， Cr，Mn，Fe，Sr，Nb，Ta，W，La和稀土金属。

3. 发明授权

US08466082B2 PD/AU shell catalyst containing HFO2, processes for the preparation and use thereof 失效
标题翻译：含有HFO2的PD / AU壳催化剂，其制备方法和用途
公开(公告)号：US08466082B2
公开(公告)日：2013-06-18
申请号：US12601399
申请日：2008-05-30
申请人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
发明人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
IPC分类号： B01J20/00 , B01J21/00 , B01J21/04 , B01J23/00 , B01J23/02 , B01J23/04 , B01J23/08 , B01J23/40 , B01J23/42 , B01J23/44 , B01J23/56 , B01J23/58
CPC分类号： B01J21/16 , B01J21/06 , B01J21/066 , B01J23/66 , B01J35/0006 , B01J35/002 , B01J35/008 , B01J35/08 , B01J35/1019 , B01J35/1038 , B01J35/1061 , B01J37/0036 , B01J37/0221 , B01J37/0242 , B01J37/0248 , B01J37/04 , C07C67/055 , C07C69/01 , C07C69/15
摘要： A shell catalyst for the preparation of vinyl acetate monomer, comprising an oxidic porous catalyst support with an outer shell, containing metallic Pd and Au, wherein the framework structure of the porous catalyst support contains hafnium oxide units. This shell catalyst is suitable for the preparation of VAM and is characterized by a relatively high activity and VAM selectivity and maintains this activity and selectivity over relatively long service lives. Also, processes for the preparation and use of the shell catalyst.
摘要翻译：一种用于制备乙酸乙烯酯单体的壳催化剂，其包含含有金属Pd和Au的外壳的氧化多孔催化剂载体，其中多孔催化剂载体的骨架结构含有氧化铪单元。该壳催化剂适用于制备VAM，其特征在于相对较高的活性和VAM选择性，并且在相对较长的使用寿命中保持该活性和选择性。另外，壳催化剂的制备和使用方法。

4. 发明申请

US20100261603A1 METHOD FOR THE PRODUCTION OF A SHELL CATALYST LOADED WITH PD AND/OR AU 审中-公开
标题翻译：用PD和/或AU加载壳体催化剂的方法
公开(公告)号：US20100261603A1
公开(公告)日：2010-10-14
申请号：US12601900
申请日：2008-05-30
申请人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
发明人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
IPC分类号： B01J23/44 , B01J23/52
CPC分类号： B01J37/031 , B01J23/44 , B01J23/52 , B01J23/66 , B01J35/008 , B01J35/026 , B01J37/0221 , B01J37/024
摘要： The present invention relates to a process for the production of a shell catalyst which comprises a catalyst support shaped body with an outer shell in which metallic Pd and/or Au is contained. In order to provide a process by means of which shell catalysts can be obtained, in the outer shell of which relatively high metallic Pd and/or Au contents are contained, a process is proposed comprising the steps of a) providing a porous catalyst support shaped body; b) providing a first solution in which a Pd and/or an Au precursor compound is contained; c) providing a second solution in which a Pd and/or a Au precursor compound is contained, wherein the first solution brings about a precipitation of the noble-metal component(s) of the second solution and the second solution a precipitation of the noble-metal component(s) of the first solution; d) loading the catalyst support shaped body with the first and with the second solution; e) converting the noble-metal component(s) precipitated on the catalyst support body into the metal form.
摘要翻译：本发明涉及一种壳催化剂的制备方法，其包括具有外壳的催化剂载体成形体，其中包含金属Pd和/或Au。为了提供可以获得壳催化剂的方法，在其包含相对高的金属Pd和/或Au含量的外壳中，提出了一种方法，包括以下步骤：a）提供多孔催化剂载体，其形状身体; b）提供其中包含Pd和/或Au前体化合物的第一溶液; c）提供其中包含Pd和/或Au前体化合物的第二溶液，其中第一溶液导致第二溶液的贵金属组分的沉淀和第二溶液沉淀贵金属 - 第一溶液的金属组分; d）用第一和第二溶液装载催化剂载体成形体; e）将催化剂载体上沉淀的贵金属组分转化为金属形式。

5. 发明申请

US20100190638A1 Method For Producing A Shell Catalyst and Corresponding Shell Catalyst 审中-公开
标题翻译：生产壳催化剂和相应壳催化剂的方法
公开(公告)号：US20100190638A1
公开(公告)日：2010-07-29
申请号：US12602026
申请日：2008-05-30
申请人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck , Silvia Neumann
发明人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck , Silvia Neumann
IPC分类号： B01J23/66 , B01J23/00 , B01J21/08 , B01J21/04 , B01J21/06 , B01J23/20 , B01J23/40 , B01J23/48 , B01J23/44 , B01J23/50 , B01J23/755 , B01J23/72 , B01J31/20 , B01J23/30 , B01J23/58 , B01J23/745 , B01J8/08
CPC分类号： B01J35/008 , B01J23/42 , B01J23/44 , B01J23/50 , B01J23/52 , B01J23/58 , B01J23/72 , B01J23/75 , B01J23/755 , B01J35/002 , B01J35/0066 , B01J35/08 , B01J35/10 , B01J35/1014 , B01J35/1038 , B01J35/1042 , B01J35/1061 , B01J35/108 , B01J37/0221 , B01J37/16
摘要： A method for producing a shell catalyst comprising a porous catalyst support shaped body with an outer shell containing at least one transition metal in metal form. To provide a shell catalyst with a relatively small shell thickness, a device is set up to circulate the catalyst support shaped bodies by means of process gases with a reductive effect. The device is charged with catalyst support shaped bodies that are circulated by means of a process gas with a reductive effect, an outer shell of the catalyst support shaped bodies is impregnated with a transition-metal precursor compound by spraying the circulating catalyst support shaped bodies with a solution containing the transition-metal precursor compound, the metal component of the transition-metal precursor compound is converted into the metal form by reduction by means of the process gas, and the catalyst support shaped bodies sprayed with the solution are dried.
摘要翻译：一种壳催化剂的制备方法，其包括多孔催化剂载体成型体，其外壳含有至少一种金属形式的过渡金属。为了提供具有相对小的壳厚度的壳催化剂，设置了一种通过具有还原效应的工艺气体循环催化剂载体成形体的装置。该装置装有催化剂载体成型体，其通过具有还原作用的工艺气体循环，催化剂载体成形体的外壳用过渡金属前体化合物浸渍，通过将循环催化剂载体成形体喷涂将过渡金属前体化合物的溶液，过渡金属前体化合物的金属成分通过用工艺气体还原而转变为金属形式，并且将溶液喷射的催化剂载体成形体干燥。

6. 发明授权

US10150099B2 Zirconium oxide-doped catalyst support, method for producing the same and catalyst containing a zirconium oxide-doped catalyst support 有权
公开(公告)号：US10150099B2
公开(公告)日：2018-12-11
申请号：US12601420
申请日：2008-05-30
申请人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
发明人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
IPC分类号： C07C67/05 , B01J21/06 , B01J21/16 , B01J23/66 , B01J35/08 , B01J37/02 , B01J37/04 , C07C67/055 , B01J23/10 , B01J35/00 , B01J35/10 , B01J37/00 , B01J37/16 , B01J37/28
摘要： The present invention relates to a porous catalyst support, consisting of a material comprising a natural sheet silicate, containing ZrO2 dispersed throughout the material. The present invention also relates to a method for the production of the catalyst support according to the invention and to a shell catalyst containing the catalyst support according to the invention and also the use of the catalyst according to the invention in particular for the production of vinyl acetate monomer (VAM).

7. 发明申请

US20100273644A1 DOPED Pd/Au SHELL CATALYST, METHOD FOR PRODUCING THE SAME AND USE THEREOF 失效
标题翻译： DOPED Pd / Au壳体催化剂，其制备方法和用途
公开(公告)号：US20100273644A1
公开(公告)日：2010-10-28
申请号：US12601419
申请日：2008-05-30
申请人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
发明人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
IPC分类号： B01J21/08
CPC分类号： B01J23/66 , B01J21/16 , B01J23/56 , B01J23/8906 , B01J23/8946 , B01J35/002 , B01J35/008 , B01J35/08 , B01J35/10 , B01J35/1014 , B01J35/1019 , B01J35/1038 , B01J35/1042 , B01J35/1061 , B01J35/108 , B01J37/0018 , B01J37/0205 , B01J37/0207 , B01J37/0221 , C07C67/055 , C07C69/01 , C07C69/15
摘要： A shell catalyst for producing vinyl acetate monomer (VAM), comprising an oxidic porous catalyst support, formed as a shaped body, with an outer shell in which metallic Pd and Au are contained. To provide a shell catalyst for producing VAM which has a relatively high activity and can be obtained at relatively low cost, the catalyst support is doped with at least one oxide of an element selected from the group consisting of Li, P, Ca, V, Cr, Mn, Fe, Sr, Nb, Ta, W, La and the rare-earth metals.
摘要翻译：一种用于生产乙酸乙烯酯单体（VAM）的壳催化剂，其包含形成为成形体的氧化多孔催化剂载体，其中包含金属Pd和Au的外壳。为了提供具有较高活性并可以相对低成本获得的VAM的壳催化剂，催化剂载体上掺杂有选自Li，P，Ca，V， Cr，Mn，Fe，Sr，Nb，Ta，W，La和稀土金属。

8. 发明申请

US20100197488A1 METHOD FOR PRODUCING A SHELL CATALYST AND CORRESPONDING SHELL CATALYST 有权
标题翻译：制备壳催化剂的方法和相应的壳催化剂
公开(公告)号：US20100197488A1
公开(公告)日：2010-08-05
申请号：US12601777
申请日：2008-05-30
申请人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck , Sybille Ungar
发明人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck , Sybille Ungar
IPC分类号： B01J23/66 , B01J21/08 , B01J21/06 , B01J23/72 , B01J23/44 , B01J23/02
CPC分类号： B01J35/008 , B01J2/16 , B01J23/66 , B01J37/0221 , C07C67/055 , C07C69/01 , C07C69/15
摘要： The present invention relates to a method for producing a shell catalyst which comprises a porous shaped catalyst support body with an outer shell in which at least one catalytically active species is present. In order to provide a shell catalyst production method by means of which shell catalysts can be produced, said shell catalysts having, over a comparatively large region of their shell thickness, a substantially uniform concentration of catalytically active species and having a substantially uniform shell thickness, what is proposed is a method using an device which is designed to generate, by means of a process gas, a fluid bed of shaped catalyst support bodies in which the shaped catalyst support bodies circulate elliptically or toroidally, preferably toroidally, comprising the steps of charging the device with shaped catalyst support bodies and generating a shaped catalyst support body fluid bed by means of a process gas, the shaped catalyst support bodies circulating elliptically or toroidally in the fluid bed, preferably toroidally; impregnating an outer shell of the shaped catalyst support body with a catalytically active species or precursor thereof by spraying the shaped catalyst support bodies circulating elliptically or toroidally in the fluid bed with a solution comprising a catalytically active species or a precursor thereof; drying the shaped catalyst support bodies sprayed with the solution.
摘要翻译：本发明涉及一种壳催化剂的制备方法，其包括具有至少一种催化活性物质的具有外壳的多孔成形催化剂载体。为了提供壳催化剂制备方法，通过该方法可以制备壳催化剂，所述壳催化剂在其厚度比较大的较大区域上具有基本上均匀的催化活性物质浓度并具有基本均匀的壳厚度，提出的是一种使用设备的方法，该装置被设计成通过工艺气体产生成形催化剂载体的流化床，其中成形催化剂载体以椭圆或环形的方式循环，优选环形，其包括以下步骤：所述装置具有成形的催化剂支撑体并且通过处理气体产生成形的催化剂载体体液床，所述成形催化剂载体在流化床中循环或环状地循环，优选环形; 通过用包含催化活性物质或其前体的溶液在流化床中喷射椭圆形或环形的成形催化剂载体，浸渍具有催化活性物质或其前体的成型催化剂载体的外壳; 干燥用溶液喷涂的成型催化剂载体。

9. 发明申请

US20100185010A1 ZIRCONIUM OXIDE-DOPED CATALYST SUPPORT, PROCESS FOR ITS PREPARATION AND CATALYST CONTAINING A ZIRCONIUM OXIDE-DOPED CATALYST SUPPORT 审中-公开
标题翻译：氧化锆催化剂支持，其制备方法和含氧化锆催化剂支持的催化剂
公开(公告)号：US20100185010A1
公开(公告)日：2010-07-22
申请号：US12601420
申请日：2008-05-30
申请人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
发明人： Alfred Hagemeyer , Gerhard Mestl , Peter Scheck
IPC分类号： C07C67/05 , B01J21/06 , B01J23/36 , B01J27/135 , B01J31/20 , B01J23/44 , B01J23/52
CPC分类号： B01J21/16 , B01J21/06 , B01J21/066 , B01J23/10 , B01J23/66 , B01J35/0006 , B01J35/002 , B01J35/008 , B01J35/08 , B01J35/1019 , B01J35/1038 , B01J35/1061 , B01J37/0036 , B01J37/0221 , B01J37/0242 , B01J37/0248 , B01J37/04 , B01J37/16 , B01J37/28 , C07C67/055 , Y02P20/582 , C07C69/01 , C07C69/15
摘要： The present invention relates to a porous catalyst support, consisting of a material comprising a natural sheet silicate, wherein ZrO2 is contained distributed in the material. The present invention also relates to a process for the preparation of the catalyst support according to the invention and to a shell catalyst containing the catalyst support according to the invention and also the use of the catalyst according to the invention in particular for the preparation of vinyl acetate monomer (VAM).
摘要翻译：本发明涉及一种多孔催化剂载体，由包含天然片状硅酸盐的材料组成，其中ZrO 2分布在材料中。本发明还涉及制备根据本发明的催化剂载体和含有本发明的催化剂载体的壳催化剂的方法，还涉及根据本发明的催化剂的用途，特别是用于制备乙烯基乙酸酯单体（VAM）。

10. 发明申请

US20150031911A1 Post-Gilding of PD-AU-Coated Shell Catalysts 有权
标题翻译： PD-AU涂层壳催化剂后镀金
公开(公告)号：US20150031911A1
公开(公告)日：2015-01-29
申请号：US14379262
申请日：2013-02-19
申请人： Gerhard Mestl , Peter Scheck , Alfred Hagemeyer , Carolin Fischer , Roman Bobka
发明人： Gerhard Mestl , Peter Scheck , Alfred Hagemeyer , Carolin Fischer , Roman Bobka
IPC分类号： B01J31/28 , C07C67/05 , B01J31/38
CPC分类号： B01J31/28 , B01J23/52 , B01J23/58 , B01J31/38 , B01J35/008 , B01J37/0205 , B01J37/18 , B01J2231/49 , C07C67/05 , C07C67/055 , C07C69/15
摘要： The invention relates to a method for producing a shell catalyst that is suitable for producing vinyl acetate monomer (VAM). The invention further relates to a shell catalyst that is obtainable by the method according to the invention and to the use of the shell catalyst according to the invention for producing VAM.
摘要翻译：本发明涉及适用于生产乙酸乙烯酯单体（VAM）的壳催化剂的制备方法。本发明还涉及通过根据本发明的方法获得的壳催化剂以及根据本发明的壳催化剂用于生产VAM的用途。

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