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1. 发明授权

US07276573B2 Method for producing monoesters and diesters of polytetrahydrofuran and of tetrahydrofuran copolymers 有权
标题翻译：聚四氢呋喃和四氢呋喃共聚物的单酯和二酯的制备方法
公开(公告)号：US07276573B2
公开(公告)日：2007-10-02
申请号：US10527583
申请日：2003-09-04
申请人： Rolf Pinkos , Achim Gerstlauer , Martin Haubner , Stephan Schlitter , Stefan Käshammer , Klaus-Peter Pfaff
发明人： Rolf Pinkos , Achim Gerstlauer , Martin Haubner , Stephan Schlitter , Stefan Käshammer , Klaus-Peter Pfaff
IPC分类号： C08G65/04 , C07D307/00 , C07C67/24
CPC分类号： C08G65/20
摘要： The present invention provides a process for preparing mono- or diesters of polytetrahydrofuran or of tetrahydrofuran copolymers by polymerizing tetrahydrofuran in the presence of at least one telogen and/or of a comonomer over an acidic catalyst, wherein the polymerization reactor is started up using a mixture of polytetrahydrofuran, the mono- or diesters of polytetrahydrofuran and/or of the THF copolymers, tetrahydrofuran, any comonomer and at least one carboxylic acid and/or one carboxylic anhydride.
摘要翻译：本发明提供了一种通过在酸性催化剂上在至少一种环糊精和/或共聚单体存在下使四氢呋喃聚合来制备聚四氢呋喃或四氢呋喃共聚物的单酯或二酯的方法，其中聚合反应器使用混合物的聚四氢呋喃，聚四氢呋喃和/或THF共聚物，四氢呋喃，任何共聚单体和至少一种羧酸和/或一种羧酸酐的单酯或二酯。

2. 发明授权

US07098349B2 Method for producing tetrahydrofuran 有权
公开(公告)号：US07098349B2
公开(公告)日：2006-08-29
申请号：US10524851
申请日：2003-07-30
申请人： Rolf Pinkos , Stefan Käshammer , Volkmar Menger , Martin Haubner , Peter Groll , Stephan Schlitter , Klaus-Peter Pfaff
发明人： Rolf Pinkos , Stefan Käshammer , Volkmar Menger , Martin Haubner , Peter Groll , Stephan Schlitter , Klaus-Peter Pfaff
IPC分类号： C07D307/02
CPC分类号： C08G65/20 , C07D307/08 , C08G65/2666
摘要： The invention relates to a process for the continuous preparation of THF by reaction of a 1,4-butanediol-containing reaction mixture over a heteropolyacid catalyst which has not been predried, wherein the reaction mixture comprises 2-(4-hydroxybutoxy)tetrahydrofuran.

3. 发明申请

US20060122365A1 Method for producing tetrahydrofuran 有权
标题翻译：生产四氢呋喃的方法
公开(公告)号：US20060122365A1
公开(公告)日：2006-06-08
申请号：US10524851
申请日：2003-07-30
申请人： Rolf Pinkos , Stefan Kashammer , Volkmar Menger , Martin Haubner , Peter Groll , Stephan Schlitter , Klaus-Peter Pfaff
发明人： Rolf Pinkos , Stefan Kashammer , Volkmar Menger , Martin Haubner , Peter Groll , Stephan Schlitter , Klaus-Peter Pfaff
IPC分类号： C08G65/00 , C07D307/02
CPC分类号： C08G65/20 , C07D307/08 , C08G65/2666
摘要： The invention relates to a process for the continuous preparation of THF by reaction of a 1,4-butanediol-containing reaction mixture over a heteropolyacid catalyst which has not been predried, wherein the reaction mixture comprises 2-(4-hydroxybutoxy)tetrahydrofuran.
摘要翻译：本发明涉及通过在未预干燥的杂多酸催化剂上使含1,4-丁二醇的反应混合物反应连续制备THF的方法，其中反应混合物包含2-（4-羟基丁氧基）四氢呋喃。

4. 发明申请

US20060266635A1 Method for obtaining oligomers of polytetrahydofurane or tetrahydrofurane 有权
标题翻译：获得聚四氢呋喃或四氢呋喃的低聚物的方法
公开(公告)号：US20060266635A1
公开(公告)日：2006-11-30
申请号：US10563421
申请日：2004-06-19
申请人： Volkmar Menger , Michael Schwarztrauber , Martin Haubner , Klaus-Peter Pfaff
发明人： Volkmar Menger , Michael Schwarztrauber , Martin Haubner , Klaus-Peter Pfaff
IPC分类号： B01D3/00
CPC分类号： C08G65/20 , C08G65/30 , C08G65/3311 , Y10S203/24
摘要： A process for obtaining oligomers of polytetrahydrofuran or of tetrahydrofuran copolymers from a methanolic crude product which contains polytetrahydrofuran or tetrahydrofuran copolymers and is obtained in the transesterification of the mono- and/or diesters of polytetrahydrofuran or tetrahydrofuran copolymers with methanol, which comprises a) removing the majority of the methanol from the crude product in a first distillation stage, b) separating the resulting bottom product by distillation into a top fraction comprising the oligomers of polytetrahydrofuran or of tetrahydrofuran copolymers, and polytetrahydrofuran or tetrahydrofuran copolymer, c) condensing the oligomers of polytetrahydrofuran or of tetrahydrofuran copolymers out of the top fraction from stage b).
摘要翻译：从含有四氢呋喃或四氢呋喃共聚物的甲醇粗产物中获得聚四氢呋喃或四氢呋喃共聚物的低聚物的方法，是在聚四氢呋喃或四氢呋喃共聚物与甲醇的单酯和/或二酯的酯交换反应中获得的，该方法包括：a）大部分来自粗产物的甲醇在第一蒸馏阶段，b）通过蒸馏将所得底部产物分离成包含聚四氢呋喃或四氢呋喃共聚物的低聚物的顶级馏分和聚四氢呋喃或四氢呋喃共聚物，c）将聚四氢呋喃的低聚物或来自阶段b）的最高级分的四氢呋喃共聚物。

5. 发明授权

US07718041B2 Method for obtaining oligomers of polytetrahydofurane or tetrahydrofurane 有权
标题翻译：获得聚四氢呋喃或四氢呋喃的低聚物的方法
公开(公告)号：US07718041B2
公开(公告)日：2010-05-18
申请号：US10563421
申请日：2004-06-19
申请人： Volkmar Menger , Michael Schwarztrauber , Martin Haubner , Klaus-Peter Pfaff
发明人： Volkmar Menger , Michael Schwarztrauber , Martin Haubner , Klaus-Peter Pfaff
IPC分类号： B01D3/10 , C07C29/80 , C07D307/08
CPC分类号： C08G65/20 , C08G65/30 , C08G65/3311 , Y10S203/24
摘要： A process for obtaining oligomers of polytetrahydrofuran or of tetrahydrofuran copolymers from a methanolic crude product which contains polytetrahydrofuran or tetrahydrofuran copolymers and is obtained in the transesterification of the mono- and/or diesters of polytetrahydrofuran or tetrahydrofuran copolymers with methanol, which includes a) removing the majority of the methanol from the crude product in a first distillation stage, b) separating the resulting bottom product by distillation into a top fraction containing the oligomers of polytetrahydrofuran or of tetrahydrofuran copolymers, and polytetrahydrofuran or tetrahydrofuran copolymer, and c) condensing the oligomers of polytetrahydrofuran or of tetrahydrofuran copolymers out of the top fraction from stage b).
摘要翻译：从含有聚四氢呋喃或四氢呋喃共聚物的甲醇粗产物中获得聚四氢呋喃或四氢呋喃共聚物的低聚物的方法，是在聚四氢呋喃或四氢呋喃共聚物与甲醇的单酯和/或二酯的酯交换反应中获得的，其包括a）大部分来自粗产物的甲醇在第一蒸馏阶段中，b）通过蒸馏将所得的底部产物分离成含有聚四氢呋喃或四氢呋喃共聚物的低聚物和四氢呋喃或四氢呋喃共聚物的顶级馏分，和c）将聚四氢呋喃或来自阶段b）的顶级馏分中的四氢呋喃共聚物。

6. 发明申请

US20100222606A1 METHOD FOR PRODUCING BISABOLOL WHICH IS FARNESOL FREE OR IS LOW IN FARNESOL 审中-公开
标题翻译：无机化学物质的双酚A的生产方法
公开(公告)号：US20100222606A1
公开(公告)日：2010-09-02
申请号：US12160918
申请日：2007-01-12
申请人： Hansgeorg Ernst , Klaus-Peter Pfaff , Karl Beck , Jürgen Schubert , Günther Gottwald , Wolfgang Krause
发明人： Hansgeorg Ernst , Klaus-Peter Pfaff , Karl Beck , Jürgen Schubert , Günther Gottwald , Wolfgang Krause
IPC分类号： C07C35/18 , C11C1/00
CPC分类号： C07C29/1285 , C07C29/095 , C07C67/02 , C07C67/03 , C07C403/08 , C07C2601/16 , C07C33/14 , C07C69/007 , C07C69/78 , C07C69/06 , C07C69/145
摘要： The present invention relates to a method of producing pure or enriched bisabolol by separating substance mixtures comprising bisabolol and farnesol by selective esterification of farnesol and subsequent distillative separation. The invention relates specifically to a method as specified above comprising the selective transesterification of mixtures comprising formyl-bisabolol and formyl-farnesol and subsequent distillative separation.The present invention furthermore relates to a method of producing farnesol esters.
摘要翻译：本发明涉及通过用法呢醇的选择性酯化和随后的蒸馏分离来分离包含红没药醇和法呢醇的物质混合物来生产纯的或富含的赤铁矿的方法。本发明具体涉及如上所述的方法，其包括含有甲酰基 - 对映体和甲酰法尼醇的混合物的选择性酯交换和随后的蒸馏分离。本发明还涉及一种生产法呢醇酯的方法。

7. 发明授权

US07622617B2 Method for producing α-bisabolol from farnesol 失效
标题翻译：从法呢醇生产α-红没药醇的方法
公开(公告)号：US07622617B2
公开(公告)日：2009-11-24
申请号：US12092731
申请日：2006-10-26
申请人： Klemens Massonne , Klaus-Peter Pfaff , Juergen Schubert , Guenther Gottwald
发明人： Klemens Massonne , Klaus-Peter Pfaff , Juergen Schubert , Guenther Gottwald
IPC分类号： C07C29/56
CPC分类号： C07C403/08 , C07B2200/09 , C07C2601/16
摘要： The present invention relates to a process for preparing α-bisabolol, comprising the reaction of farnesol in the presence of a ketone, of a sulfonic acid and of a further strong acid.
摘要翻译：本发明涉及一种制备α-红没药醇的方法，包括法呢醇在酮存在下，磺酸和另外的强酸的反应。

8. 发明申请

US20080269530A1 Method for Producing Alpha-Bisabolol from Farnesol 失效
标题翻译：从法呢醇生产α-对映体的方法
公开(公告)号：US20080269530A1
公开(公告)日：2008-10-30
申请号：US12092731
申请日：2006-10-26
申请人： Klemens Massonne , Klaus-Peter Pfaff , Juergen Schubert , Guenther Gottwald
发明人： Klemens Massonne , Klaus-Peter Pfaff , Juergen Schubert , Guenther Gottwald
IPC分类号： C07C29/56
CPC分类号： C07C403/08 , C07B2200/09 , C07C2601/16
摘要： The present invention relates to a process for preparing α-bisabolol, comprising the reaction of farnesol in the presence of a ketone, of a sulfonic acid and of a further strong acid.
摘要翻译：本发明涉及一种制备α-红没药醇的方法，包括法呢醇在酮存在下，磺酸和另外的强酸的反应。

9. 发明申请

US20100311988A1 METHOD FOR PRODUCING CIS-ROSE OXIDE 有权
标题翻译：生产环氧丙烷的方法
公开(公告)号：US20100311988A1
公开(公告)日：2010-12-09
申请号：US12809356
申请日：2008-12-17
申请人： Lucia Koenigsmann , Juergen Schubert , Andreas Walch , Guenther Gottwald , Martin Kamasz , Ekkehard Schwab , Klaus-Peter Pfaff , Michael Slany
发明人： Lucia Koenigsmann , Juergen Schubert , Andreas Walch , Guenther Gottwald , Martin Kamasz , Ekkehard Schwab , Klaus-Peter Pfaff , Michael Slany
IPC分类号： C07D309/04
CPC分类号： C07D309/04
摘要： The present invention relates to a process for the preparation of cis-2-(2-methylprop-1-enyl)-4-methyltetrahydropyran comprising the catalytic hydrogenation of 2-(2-methylprop-1-enyl)-4-methylenetetrahydropyran in the presence of hydrogen and a heterogeneous catalyst comprising ruthenium on a support and subsequently bringing the compounds obtained in this way into contact with a strongly acidic cation exchanger.
摘要翻译：本发明涉及一种制备顺式-2-（2-甲基丙-1-烯基）-4-甲基四氢吡喃的方法，其包括2-（2-甲基丙-1-烯基）-4-亚甲基四氢吡喃的催化氢化在载体上存在氢和包含钌的非均相催化剂，随后将以这种方式获得的化合物与强酸性阳离子交换剂接触。

10. 发明授权

US4681936A Preparation of sugar ketals 失效
标题翻译：糖缩酮的制备
公开(公告)号：US4681936A
公开(公告)日：1987-07-21
申请号：US826317
申请日：1986-02-05
申请人： Klaus-Peter Pfaff , Joachim Paust , Horst Hartmann
发明人： Klaus-Peter Pfaff , Joachim Paust , Horst Hartmann
IPC分类号： C07H1/00 , B01J31/00 , C07B61/00 , C07H9/04
CPC分类号： C07H9/04
摘要： Sugar ketals are prepared by reacting a sugar with a ketone in the presence of an acid catalyst by a process in whichA. a molecular boron trifluoride compound or trifluoromethanesulfonic acid is used in an amount of only from 0.01 to 10% by weight, based on the sugar used,B. up to a 30-fold molar excess of the ketone is used andC. the water formed during the reaction is removed continuously from the reaction mixture.In a particularly advantageous embodiment of the process, the boron trifluoride is used in the form of boron trifluoride etherate and, when the reaction is complete, this compound or the trifluoromethanesulfonic acid is rendered ineffective under non-aqueous conditions, after which the ketone is evaporated off and the reaction mixture is then subjected to fractional distillation. The process is particularly important for the reaction of L-sorbose with acetone to obtain 2,3:4,6-di-O-isopropylidene-L-sorbofuranose, which is required for the synthesis of ascorbic acid.
摘要翻译：糖缩成物是通过在酸催化剂存在下使糖与酮反应的方法制备的，其中A为分子三氟化硼化合物或三氟甲磺酸的用量，其量仅为0.01至10重量％，基于使用的糖，B.使用高达30倍摩尔过量的酮，并且C.从反应混合物中连续除去反应期间形成的水。在该方法的特别有利的实施方案中，三氟化硼以三氟化硼醚合物的形式使用，当反应完成时，该化合物或三氟甲磺酸在非水性条件下变得无效，之后酮蒸发然后将反应混合物进行分馏。该方法对于L-山梨糖与丙酮的反应特别重要，得到合成抗坏血酸所需的2,3：4,6-二-O-异亚丙基-L-山梨糖。

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