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1. 发明授权

US4193851A Silica gels and their formation by electrolysis of silicate solutions 失效
标题翻译：二氧化硅凝胶及其通过电解硅酸盐溶液的形成
公开(公告)号：US4193851A
公开(公告)日：1980-03-18
申请号：US927269
申请日：1978-07-21
申请人： Roger A. Crawford , Howard H. Hoekje
发明人： Roger A. Crawford , Howard H. Hoekje
IPC分类号： C25B1/00
CPC分类号： C25B1/00
摘要： Novel silica gels are disclosed, as well as their formation from aqueous sodium silicate solutions by neutralizing the hydroxyl ion by electrolysis at a rate whereby the concentration of hydroxide ion is maintained within the range wherein silica gel forms.
摘要翻译：公开了新型硅胶，以及它们由硅酸钠水溶液形成，通过以氢氧化物离子的浓度保持在硅胶形成的范围内通过电解中和羟基离子形成。

2. 发明授权

US4894241A Halophor composition 失效
标题翻译：卤虫组成
公开(公告)号：US4894241A
公开(公告)日：1990-01-16
申请号：US819443
申请日：1986-01-16
申请人： Paritosh M. Chakrabarti , Roger A. Crawford , Robert H. Juda
发明人： Paritosh M. Chakrabarti , Roger A. Crawford , Robert H. Juda
IPC分类号： A01N59/00 , A01N59/12
CPC分类号： A01N59/12 , A01N59/00
摘要： Halophors of a complex of bromine or iodine, a tertiary amide, e.g., dialkylformamide or dialkyl acetamide, and a halide, e.g., alkali metal or alkaline earth metal bromide or iodide, are described. The alkyl groups of the tertiary amide are typically lower alkyl groups, i.e., groups containing from 1 to 4 carbon atoms. Also described are solid biocidal compositions, e.g., fumigants, of particulate, free-flowing inert amorphous siliceous carrier having at least a biocidal amount of halophor admixed with said carrier.
摘要翻译：描述了溴或碘络合物的卤化物，叔酰胺，例如二烷基甲酰胺或二烷基乙酰胺，以及卤化物，例如碱金属或碱土金属的溴化物或碘化物。叔酰胺的烷基通常是低级烷基，即含有1至4个碳原子的基团。还描述了具有与所述载体混合的至少具有杀生物剂量的卤代物的颗粒状，自由流动的惰性无定形硅质载体的固体杀生物组合物，例如熏蒸剂。

3. 发明授权

US4328200A Process for producing calcium hypochlorite 失效
标题翻译：生产次氯酸钙的方法
公开(公告)号：US4328200A
公开(公告)日：1982-05-04
申请号：US269241
申请日：1981-06-01
申请人： Cletus N. Welch , Clifford E. Loehr , Roger A. Crawford , John E. Carbaugh
发明人： Cletus N. Welch , Clifford E. Loehr , Roger A. Crawford , John E. Carbaugh
IPC分类号： C01B11/06
CPC分类号： C01B11/064 , Y02P20/125
摘要： A continuous integrated process for the production of calcium hypochlorite in which crystals of by-product sodium chloride are more easily separated for the calcium hypochlorite product is described. The process includes: (a) introducing with agitation into a vessel an aqueous slurry of dibasic calcium hypochlorite, sodium hydroxide, and aqueous salt solution saturated with calcium ion and sodium chloride in amounts at least sufficient to substantially dilute the sodium hydroxide; (b) forwarding the resulting aqueous mixture of step (a) to a chlorination zone containing a seed bed of calcium hypochlorite and sodium chloride crystals; (c) introducing chlorine into the chlorination zone, thereby producing an aqueous suspension containing further quantities of calcium hypochlorite crystals and readily separable significantly larger sodium chloride crystals; and (d) removing aqueous suspension containing such calcium hypochlorite and sodium chloride crystals from the chlorination zone to a classification zone. Calcium hypochlorite crystals are maintained in suspension in and removed from the upper portion of the classification zone; while the larger and more dense crystals of sodium chloride settle and are removed from the lower portion of said classification zone.
摘要翻译：描述了一种用于生产次氯酸钙的连续一体化方法，其中副产物氯化钠的晶体更容易分离用于次氯酸钙产物。该方法包括：（a）在搅拌下将至少足以基本上稀释氢氧化钠的量的钙离子和氯化钠饱和的二价次氯酸钙，氢氧化钠和盐水溶液的水性浆料搅拌引入容器中; （b）将得到的步骤（a）的水性混合物转移到含有次氯酸钙和氯化钠晶体的种子床的氯化区; （c）将氯引入氯化区，从而产生含有更多量的次氯酸钙晶体和容易分离的显着较大氯化钠晶体的水性悬浮液; 和（d）将含有这种次氯酸钙和氯化钠晶体的含水悬浮液从氯化区移除到分级区。将次氯酸钙晶体保持在分级区上部的悬浮液中并从分离区的上部除去; 而较大和更致密的氯化钠晶体沉淀并从分级区的下部除去。

4. 发明授权

US4297333A Method of decomposing hypochlorite ion in a basic solution 失效
标题翻译：在碱性溶液中分解次氯酸根离子的方法
公开(公告)号：US4297333A
公开(公告)日：1981-10-27
申请号：US166020
申请日：1980-07-07
申请人： Roger A. Crawford , Robert B. Simmons
发明人： Roger A. Crawford , Robert B. Simmons
IPC分类号： B01J23/00 , B01J23/755 , C02F1/76 , B01D53/34 , C01B13/02 , C01D3/08 , C02F1/72
CPC分类号： C02F1/705 , B01J23/005 , B01J23/755 , C02F2303/185 , Y10S502/524
摘要： Disclosed is a hypochlorite decomposition catalyst of nickel (II) oxide and NiCo.sub.2 O.sub.4 spinel, a hypochlorite destruction process using the catalyst, and a method of synthesizing the catalyst on a porous support.
摘要翻译：公开了使用该催化剂的次氯酸盐破坏方法和在多孔载体上合成催化剂的方法，使用氧化镍（II）和NiCo2O4尖晶石的次氯酸盐分解催化剂。

5. 发明授权

US5673470A Extended jacket end, double expansion hydroforming 失效
标题翻译：延长护套端，双膨胀液压成型
公开(公告)号：US5673470A
公开(公告)日：1997-10-07
申请号：US522172
申请日：1995-08-31
申请人： James R. Dehlinger , Roger A. Crawford , Wallace J. Poole , Robert A. Shaffer , Donald R. VandePolder
发明人： James R. Dehlinger , Roger A. Crawford , Wallace J. Poole , Robert A. Shaffer , Donald R. VandePolder
IPC分类号： F01N13/08 , B21D26/045 , B21D39/08 , B21D39/04 , B21D26/02
CPC分类号： B21D26/045 , Y10T29/49398 , Y10T29/49805 , Y10T29/49879 , Y10T29/5199
摘要： Hydroforming double wall tubular stock into an air gap tubular element comprising providing a plural wall tubular workpiece having at least an inner wall liner and an outer wall jacket having adjacent open axial ends, causing at least one of the jacket ends to extend axially beyond the adjacent liner end and to be flared outwardly, placing the workpiece into a first mold cavity of a size and configuration to result in the desired size and configuration of the liner, sealing the open ends of said liner, injecting hydroforming fluid into said liner to fill it and applying pressure thereto to expand the liner and jacket in the first mold cavity, releasing the pressure, placing the workpiece in a second mold cavity of a size and configuration desired for the jacket on a resulting air gap tubular element, providing hydroforming end closures to seal off the jacket ends, at least one of the end closures having an annular shoulder aligned with the flared extended jacket end radially outwardly offset from the adjacent liner end, pressing the annular shoulder directly against the flared jacket end to seal the flared jacket end between the shoulder and an anvil surface, injecting fluid into the workpiece to fill it and applying pressure to expand only the jacket.
摘要翻译：将双壁管状原料液压成气隙管状元件，包括提供具有至少内壁衬套和具有相邻开口轴向端部的外壁套管的多壁管状工件，使得至少一个护套端部轴向延伸超过相邻衬里端部并向外张开，将工件放置在尺寸和构造的第一模腔中，以产生所需衬套的所需尺寸和构造，密封所述衬套的开口端，将液压成形流体注入所述衬套以填充并向其施加压力以使第一模腔中的衬套和护套膨胀，释放压力，将工件放置在所形成的空气间隙管状元件上用于套管所需的尺寸和构造的第二模腔中，从而提供液压成形端盖封闭护套端部，至少一个封闭件具有与扩张的扩展护套对准的环形肩部径向向外偏离相邻的衬垫端，将环形肩部直接压靠在扩口护套端部上，以密封肩部和砧座表面之间的喇叭形护套端部，将流体注入工件以填充其并施加压力以仅膨胀护套。

6. 发明授权

US4818532A Bromophor composition 失效
标题翻译：溴素组成
公开(公告)号：US4818532A
公开(公告)日：1989-04-04
申请号：US922375
申请日：1986-10-23
申请人： Paritosh M. Chakrabarti , Roger A. Crawford , Robert H. Juda
发明人： Paritosh M. Chakrabarti , Roger A. Crawford , Robert H. Juda
IPC分类号： A01N59/00 , A01N59/12 , A61K33/18
CPC分类号： A01N59/00 , A01N59/12
摘要： Described are free-flowing particulate bromophor compositions of a siliceous carrier having absorbed therein from 1 to 80 weight percent of a bromophor that is a complex of (a) bromine, (b) alkali metal halide and (c) nonionic, anionic or cationic surfactant-type organic material.
摘要翻译：描述了自由流动的硅质载体的自由流动的颗粒状溴代烃组合物，其中已经从其中吸收了1至80重量％的溴代醇，其是（a）溴，（b）碱金属卤化物和（c）非离子，阴离子或阳离子表面活性剂型有机材料。

7. 发明授权

US4390512A Process for producing calcium hypochlorite 失效
标题翻译：生产次氯酸钙的方法
公开(公告)号：US4390512A
公开(公告)日：1983-06-28
申请号：US350653
申请日：1982-02-22
申请人： Clifford E. Loehr , Roger A. Crawford , John E. Carbaugh , Cletus N. Welch
发明人： Clifford E. Loehr , Roger A. Crawford , John E. Carbaugh , Cletus N. Welch
IPC分类号： C01B11/06
CPC分类号： C01B11/064 , Y02P20/125
摘要： A continuous integrated process for the production of neutral calcium hypochlorite in which crystals of by-product sodium chloride are more easily separated from the calcium hypochlorite product is described. The process includes diluting an aqueous slurry of sodium hydroxide, lime and bleach mother liquor with aqueous salt solution saturated with calcium ion and sodium chloride and chlorinating the resulting aqueous admixture in the presence of a seed bed of sodium chloride crystals and calcium hypochlorite crystals at temperatures less than 35.degree. C., e.g., 15.degree.-20.degree. C. A suspension of readily separable, sodium chloride crystals and calcium hypochlorite crystals in chlorinator liquor is conveyed to a classification zone where the sodium chloride and calcium hypochlorite crystals are separated.
摘要翻译：描述了用于生产中性次氯酸钙的连续一体化方法，其中副产物氯化钠的晶体更容易从次氯酸钙产物中分离出来。该方法包括用氯化钠和氯化钠饱和的盐水溶液稀释氢氧化钠，石灰和漂白母液的含水浆液，并在温度下氯化钠晶体和次氯酸钙晶体的种子床存在下氯化得到的水混合物低于35℃，例如15-20℃。氯化钠溶液中容易分离的氯化钠晶体和次氯酸钙晶体的悬浮液被输送到氯化钠和次氯酸钙晶体分离的分级区域。

8. 发明授权

US5030286A High solids aqueous silica slurry 失效
标题翻译：高固体含水二氧化硅浆液
公开(公告)号：US5030286A
公开(公告)日：1991-07-09
申请号：US396402
申请日：1989-08-14
申请人： Roger A. Crawford , Thomas G. Krivak , Patrick G. Malloy , Da-Hung Yang
发明人： Roger A. Crawford , Thomas G. Krivak , Patrick G. Malloy , Da-Hung Yang
IPC分类号： C01B33/14 , C01B33/141 , C01B33/187 , C08K3/36 , C08L33/04 , C08L33/06 , D21H19/40
CPC分类号： C01B33/1417 , D21H19/40 , Y10S423/15
摘要： Described are high solids aqueous slurries of amorphous precipitated hydrated silica, which slurries are of relatively low viscosity. The slurry typically contains from about 40 to about 60 weight percent of hydrated precipitated high structure silica. The viscosity of the high solids slurry is less than about 1000 centipoises. Processes for producing the aqueous high solids silica slurry are disclosed. In one embodiment, a wet cake of amorphous precipitated hydrated silica is liquified and the liquified wet cake charged to a high intensity mill wherein the silica is wet milled until the median agglomerate particle size of the silica is between about 0.3 and about 3 microns. In a further embodiment, finely-divided dry amorphous precipitated silica is slurried in a dispersion mill to the desired solids level and this slurry charged to a high-intensity mill and wet milled therein until the aforesaid agglomerate particle size range is attained. The resulting high solids slurry can be shipped in bulk with only mild agitation to prevent setting. A dispersant may also be added to the slurry prior to milling to retard settling of the silica.
摘要翻译：描述了无定形沉淀的水合二氧化硅的高固体含水浆料，其中浆料的粘度相对较低。浆料通常含有约40至约60重量％的水合沉淀高结构二氧化硅。高固体浆料的粘度小于约1000厘泊。公开了用于生产含水高固体二氧化硅浆料的方法。在一个实施方案中，将无定形沉淀的水合二氧化硅的湿滤饼液化并将液化的湿滤饼装入高强度研磨机中，其中二氧化硅被湿磨，直到二氧化硅的中值附聚物粒度在约0.3至约3微米之间。在另一个实施方案中，将细碎的干无定形沉淀二氧化硅在分散研磨机中浆化至所需的固体含量，并将该浆料装入高强度研磨机中并在其中湿磨，直到达到上述附聚物粒度范围。所得到的高固体浆料可以散装运输，只需轻微的搅拌即可防止固化。在研磨之前还可以将分散剂加入到浆料中以阻止二氧化硅沉降。

9. 发明授权

US4844899A Halophor composition 失效
标题翻译：卤虫组成
公开(公告)号：US4844899A
公开(公告)日：1989-07-04
申请号：US819452
申请日：1986-01-16
申请人： Robert H. Juda , Paritosh M. Chakrabarti , Roger A. Crawford
发明人： Robert H. Juda , Paritosh M. Chakrabarti , Roger A. Crawford
IPC分类号： A01N59/00 , A01N59/12
CPC分类号： A01N59/00 , A01N59/12
摘要： Halophors, e.g., bromophors, comprising a complex of sulfone, e.g., sulfolane, halide ion, e.g., sodium bromide, and halogen, e.g., bromine, are described. Solid, free-flowing halophor compositions of the aforesaid complex and an amorphous siliceous carrier are also described.
摘要翻译：描述了包含砜的复合物，例如环丁砜，卤化物离子，例如溴化钠和卤素例如溴的卤素，例如溴代烃。还描述了上述复合物和无定形硅质载体的固体，自由流动的卤代组合物。

10. 发明授权

US4782078A Halophor biocidal compositions 失效
标题翻译： Halophor杀生物组合物
公开(公告)号：US4782078A
公开(公告)日：1988-11-01
申请号：US819453
申请日：1986-01-16
申请人： Roger A. Crawford , Robert H. Juda , Paritosh M. Chakrabarti
发明人： Roger A. Crawford , Robert H. Juda , Paritosh M. Chakrabarti
IPC分类号： A01N59/12 , A01N43/36
CPC分类号： A01N59/12
摘要： Halophor biocidal compositions, e.g., bromophors, comprising a complex of N-alkyl substituted-2-pyrrolidone, e.g., N-methyl pyrrolidone, halide ion, e.g., sodium bromide, and halogen, e.g., bromine, are described.
摘要翻译：描述了包含N-烷基取代-2-吡咯烷酮如N-甲基吡咯烷酮，卤化物离子，例如溴化钠和卤素如溴的络合物杀生物组合物，例如溴代物。

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