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1. 发明授权

US4108781A Production of polyester tire yarn 失效
标题翻译：生产聚酯轮胎纱线
公开(公告)号：US4108781A
公开(公告)日：1978-08-22
申请号：US770124
申请日：1977-02-18
申请人： Robert Moore Marshall , Kimon Constantine Dardoufas
发明人： Robert Moore Marshall , Kimon Constantine Dardoufas
IPC分类号： D06M13/50 , D01F11/08 , D02G3/48 , D06M13/02 , D06M13/165 , D06M13/17 , D06M13/51 , D06M13/513 , D06M101/00 , D06M101/16 , D06M101/30 , D06M101/32 , D06M13/18
CPC分类号： D06M13/165 , D06M13/513 , Y10S156/91 , Y10T428/2962 , Y10T428/2967 , Y10T428/2969
摘要： In a process for producing polyethylene terephthalate yarn wherein a liquid finish is applied to the yarn, said process involving spinning and drawing steps, the improvement comprising first applying to the yarn prior to said drawing step a liquid finish composition consisting essentially of a polyalkylene glycol compound which is a mixed polyoxyethylated-polyoxypropylated monoether prepared in accordance with the equation: ##STR1## where R is an alkyl group having 1 to 8 carbon atoms, x and y are the number of moles of propylene oxide and ethylene oxide respectively and wherein ethylene oxide comprises 40 to 60 percent by weight of the combined total of ethylene oxide and propylene oxide and x+y has a value to produce a molecular weight of from 300 to 1,000, and then applying to said yarn after said drawing step a liquid finish composition consisting essentially of about 70 to 95 parts by weight of said mixed polyoxyethylated-polyoxypropylated monoether, about 5 to 30 parts by weight of a silane having the structural formula: ##STR2## wherein n =2 to 5, and a sufficient amount of a water-soluble alkaline catalyst to adjust the pH of the finish composition to 8-10.
摘要翻译：在生产聚对苯二甲酸乙二醇酯纱线的方法中，其中对纱线施加液体整理剂，所述方法涉及纺丝和拉伸步骤，其改进包括首先在所述拉伸步骤之前向纱线施加基本上由聚亚烷基二醇化合物其是根据以下等式制备的混合的聚氧乙烯 - 聚氧丙基化单醚：其中R是具有1至8个碳原子的烷基，x和y分别是环氧丙烷和环氧乙烷的摩尔数，并且其中环氧乙烷占环氧乙烷和环氧丙烷的总和的40〜60重量％，x + y的分子量为300〜1000的值，然后在拉伸工序后对所述纱线施加组成的液体组合物组合物基本上约70至95重量份的所述混合的聚氧乙基化聚氧丙基化单醚，约5至30重量份的o f具有以下结构式的硅烷：其中n = 2至5，和足量的水溶性碱性催化剂，以将整理剂组合物的pH调节至8-10。

2. 发明授权

US3940544A Production of polyester yarn 失效
标题翻译：生产聚酯纱线
公开(公告)号：US3940544A
公开(公告)日：1976-02-24
申请号：US484055
申请日：1974-06-28
申请人： Robert Moore Marshall , Kimon Constantine Dardoufas
发明人： Robert Moore Marshall , Kimon Constantine Dardoufas
IPC分类号： B29C67/24 , B29C70/20 , C08J5/06 , D06M13/364 , B29H9/02 , B32B25/02 , B32B27/02
CPC分类号： D06M13/364 , B29D30/40 , C08J5/06 , D06M7/00 , B29D2030/383 , B29K2021/00 , C08J2321/00 , D06M2200/40 , Y10S156/91 , Y10T428/2938 , Y10T428/2942 , Y10T428/2945 , Y10T428/2947 , Y10T428/2969
摘要： An improved polyethylene terephthalate tire yarn is prepared by applying to the yarn a finish composition comprising a polyalkylene glycol compound having the formulaR--(O--R.sub.1 --O--R.sub.2).sub.n --OHin which R.sub.1 and R.sub.2 are the same or different lower alkylene units such as ethylene, propylene and so forth up to 5 carbon atoms, R is an alkyl group containing 1 to 8 carbon atoms, and n has a value to produce a molecular weight of at least about 300; and about 5 to 35 parts per 100 parts, by weight, of said polyalkylene glycol compound of a triol compound having the formula: ##EQU1## WHEREIN R and R' are independently at each occurrence hydrogen, methyl or ethyl and r, s, and t are integers from 1 to about 20. This method of finishing the tire yarn results in an improved adhesion of the fiber to rubber.
摘要翻译：通过向纱线施加包含具有式R-（O-R 1 -O-R 2）n -OH的聚亚烷基二醇化合物的精整组合物，其中R1和R2是相同或不同的低级亚烷基单元如乙烯，丙烯等至多5个碳原子，R是含有1至8个碳原子的烷基，n具有产生至少约300的分子量的值; 和约5至35份/ 100份（重量）的所述聚亚烷基二醇化合物的具有下式的三醇化合物：O并行烷基H OCHCH2 -O-CHCH2-NN-CH2CHO-CH2CHO -H |||||| R'RRO = CC = ORR的ANGLE | CH 2 CHO-CH 2 CHO -H || RR't其中R和R'在每次出现时独立地为氢，甲基或乙基，并且r，s和t为1至约20的整数。整理轮胎纱线的方法导致纤维与橡胶的粘合性提高。

3. 发明授权

US4054634A Production of polyester tire yarn 失效
标题翻译：生产聚酯轮胎纱线
公开(公告)号：US4054634A
公开(公告)日：1977-10-18
申请号：US617547
申请日：1975-09-29
申请人： Robert Moore Marshall , Kimon Constantine Dardoufas
发明人： Robert Moore Marshall , Kimon Constantine Dardoufas
IPC分类号： D06M13/50 , D01F11/08 , D02G3/48 , D06M13/02 , D06M13/165 , D06M13/17 , D06M13/51 , D06M13/513 , D06M101/00 , D06M101/16 , D06M101/30 , D06M101/32 , B05D1/38 , B05D3/12
CPC分类号： D06M13/165 , D06M13/513 , Y10S156/91 , Y10T428/2962 , Y10T428/2967 , Y10T428/2969
摘要： In a process for producing polyethylene terephthalate yarn, particularly for tire cords, wherein a liquid finish is applied to the yarn, said process involving spinning and drawing steps, the improvement comprising: (a) first applying to the yarn prior to said drawing step a liquid finish composition consisting essentially of a polyalkylene glycol compound which is a mixed polyoxyethylated-polyoxypropylated monoether prepared in accordance with the equation: ##STR1## where R is an alkyl group having 1 to 8 carbon atoms, x and y are the number of moles of propylene oxide and ethylene oxide respectively and wherein ethylene oxide comprises 40 to 60 percent by weight of the combined total of ethylene oxide and propylene oxide and x+y has a value to produce a molecular weight of from 300 to 1,000; and then (b) applying to said yarn after said drawing step a liquid finish composition consisting essentially of about 70 to 95 parts by weight of said mixed polyoxyethylated-polyoxypropylated monoether, about 5 to 30 parts by weight of a silane having the structural formula: ##STR2## wherein n = 2 to 5, and a sufficient amount of a water-soluble alkaline catalyst to adjust the pH of the finish composition to 8-10.
摘要翻译：在制造聚对苯二甲酸乙二醇酯纱线的方法中，特别是用于轮胎帘线的方法，其中对纱线施加液体精加工，所述方法涉及纺丝和拉伸步骤，其改进包括：（a）在所述拉伸步骤a之前首先施加到纱线上基本上由聚亚烷基二醇化合物组成的液体组合物组合物，其是根据以下等式制备的混合的聚氧乙基化 - 聚氧丙基化单醚：其中R是具有1至8个碳原子的烷基，其中R 2是（C 2 H 4 O，C 3 H 6 O）x + x和y分别是环氧丙烷和环氧乙烷的摩尔数，其中环氧乙烷占环氧乙烷和环氧丙烷总量的40-60％（重量），x + y具有产生分子量为 300至1,000; 然后（b）在所述拉伸步骤之后向所述纱线施加基本上由约70至95重量份的所述混合的聚氧乙基化聚氧丙基化单醚组成的液体涂料组合物，约5至30重量份的具有以下结构式的硅烷：＆lt; IMAGE＆gt;其中n = 2至5，以及足量的水溶性碱性催化剂，以将整理剂组合物的pH调节至8-10。

4. 发明授权

US4019990A Production of polyester tire yarn polyglycol ether spin finish composition 失效
标题翻译：生产聚酯轮胎纱聚乙二醇醚旋涂组合物
公开(公告)号：US4019990A
公开(公告)日：1977-04-26
申请号：US598465
申请日：1975-07-23
申请人： Robert Moore Marshall , Kimon Constantine Dardoufas
发明人： Robert Moore Marshall , Kimon Constantine Dardoufas
IPC分类号： D06M13/165 , D06M15/53 , D06M15/10
CPC分类号： D06M15/53 , D06M13/165 , D06M7/00 , D06M2200/40 , Y10S264/84
摘要： It has been suggested that certain polyglycol ethers, in particular mixed polyoxyethylated-polyoxypropylated monoethers, are useful as spin finishes in the production of polyester tire yarns. Polyglycol ethers having a relatively low molecular weight of about 300 to 1,000 make the best lubricants; however, their effectiveness is significantly diminished by volatilization loss during high temperature processing of the tire yarn. It has now been found that said volatilization loss is greatly decreased by including in the finish a small percentage of certain antioxidant compounds. The particular antioxidant compound used has been found to be very critical.
摘要翻译：已经提出某些聚乙二醇醚，特别是混合的聚氧乙基化聚氧丙基化单醚，可用作生产聚酯轮胎纱线中的纺丝整理剂。具有约300至1,000分子量相对较低的聚乙二醇醚是最好的润滑剂; 然而，其轮胎纱线的高温加工期间的挥发损失显着降低了它们的效果。现在已经发现，通过在完成中包含少量的某些抗氧化剂化合物，所述挥发损失大大降低。已经发现使用的特定抗氧化剂化合物非常关键。

5. 发明授权

US4103068A Polyester filamentary yarns 失效
标题翻译：聚酯长丝纱
公开(公告)号：US4103068A
公开(公告)日：1978-07-25
申请号：US781913
申请日：1977-03-28
申请人： Robert Moore Marshall , Kimon Constantine Dardoufas
发明人： Robert Moore Marshall , Kimon Constantine Dardoufas
IPC分类号： D02G3/00 , D06M13/148 , D06M13/224 , B32B27/00
CPC分类号： D06M13/224 , D06M13/148 , D06M7/00 , D06M2200/40 , Y10S57/902 , Y10T428/2933 , Y10T428/2938 , Y10T428/2969
摘要： Synthetic filamentary yarn comprised of polyethylene terephthalate filaments which are first treated with a liquid composition consisting essentially of refined coconut oil, about 10 to 20 weight percent of said composition of a stearic acid ester of a branched chain alcohol having 14-15 carbon atoms, ethoxylated tallow amine, ethoxylated lauryl alcohol, sodium salt of alkylarylsulfonate, dinonyl-sodium-sulfosuccinate, and white mineral oil having a boiling point of between 510.degree. and 620.degree. F., and then treated with a liquid composition consisting essentially of a compound selected from the group consisting of glycerol monooleate and decaglycerol tetraoleate with ethoxylated tall oil fatty acids, a compound selected from the group consisting of sulfated glycerol trioleate and ethoxylated tallow amine, and a stearic acid ester of a branched chain alcohol having 14-15 carbon atoms.
摘要翻译：由聚对苯二甲酸乙二醇酯长丝组成的合成长丝纱，其首先用基本上由精制椰子油组成的液体组合物，约10-20重量％的所述组合物，具有14-15个碳原子的支链醇的硬脂酸酯，乙氧基化牛脂胺，乙氧基化月桂醇，烷基芳基磺酸钠盐，二壬基磺基琥珀酸钠和沸点为510至620°F的白色矿物油，然后用基本上由以下化合物组成的液体组合物处理：由甘油单油酸酯和十聚甘油四油酸酯与乙氧基化妥尔油脂肪酸组成的组，选自硫酸甘油三油酸酯和乙氧基化牛脂胺的化合物和具有14-15个碳原子的支链醇的硬脂酸酯组成的组。

6. 发明授权

US3962516A Production of polyester tire yarn 失效
标题翻译：生产聚酯轮胎纱线
公开(公告)号：US3962516A
公开(公告)日：1976-06-08
申请号：US583826
申请日：1975-06-04
申请人： Robert Moore Marshall , Kimon Constantine Dardoufas
发明人： Robert Moore Marshall , Kimon Constantine Dardoufas
IPC分类号： C08J5/06 , D06M15/53 , B32B27/04
CPC分类号： C08J5/06 , D06M15/53 , C08J2321/00 , Y10S156/91 , Y10T428/2967
摘要： An improved polyethylene terephthalate tire yarn is prepared by applying to the yarn a finish composition consisting essentially of a polyalkylene glycol compound having the formulaR--(O--R.sub.1 --O-- R.sub.2 ).sub.n --OHin which R.sub.1 and R.sub.2 are the same or different lower alkylene units such as ethylene, propylene and so forth up to 5 carbon atoms, R is an alkyl group containing 1 to 8 carbon atoms, and n has a value to produce a molecular weight of at least about 300. Preferably, the yarn is thereafter heated for 10 to 160 seconds at a temperature of from about 215.degree. to 230.degree.C. This method of finishing the tire yarn results in an improved compression-extension durability of the fiber in rubber.
摘要翻译：通过向纱线施加基本上由具有式R-（O-R 1 -O-R 2）n -OH的聚亚烷基二醇化合物组成的组合物制备改进的聚对苯二甲酸乙二醇酯轮胎纱线，其中R1和R2相同或不同低级亚烷基单元如乙烯，丙烯等至多5个碳原子，R是含有1至8个碳原子的烷基，n具有至少约300的分子量的值。优选地，纱线是然后在约215〜230℃的温度下加热10〜160秒。对轮胎纱线进行精加工的这种方法导致橡胶中的纤维的压缩延伸耐久性得到改善。

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