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1. 发明授权

US5578652A Method of producing rigid foams and products produced therefrom 失效
标题翻译：生产硬质泡沫的产品及由其生产的产品的方法
公开(公告)号：US5578652A
公开(公告)日：1996-11-26
申请号：US498276
申请日：1995-07-03
申请人： Robert H. Blanpied , James D. Thornsberry
发明人： Robert H. Blanpied , James D. Thornsberry
IPC分类号： C07C13/10 , C08G18/00 , C08G18/08 , C08G18/40 , C08G18/42 , C08G18/76 , C08G101/00 , C08J9/00 , C08J9/14
CPC分类号： C08J9/149 , C07C13/10 , C08G18/0852 , C08G18/4018 , C08G18/42 , C08J9/0038 , C08J9/141 , C07C2101/08 , C08G2101/0025 , C08G2101/005 , C08J2375/04
摘要： A thermosetting plastic foam solid is obtained using a blowing agent comprised at least partially from depolymerization of dicyclopentadiene into essentially pure cyclopentane. This unique hydrocarbon is miscible in polyester polyols, where others, such as extracted cyclopentane, are not. In a blend of 15 parts of liquid flame retardant per hundred parts polyester polyol, the mixture is both stable and has a suitably low viscosity.
摘要翻译：使用至少部分地将二环戊二烯解聚成基本上纯的环戊烷的发泡剂获得热固性塑料泡沫固体。这种独特的烃在聚酯多元醇中是可混溶的，其他的，如提取的环戊烷不是。在每100份聚酯多元醇混合15份液体阻燃剂的混合物中，混合物既稳定又具有适当的低粘度。

2. 发明授权

US06866923B2 Thermosetting plastic foams and methods of production thereof using adhesion additives 失效
标题翻译：热固塑料泡沫及其使用粘合添加剂的生产方法
公开(公告)号：US06866923B2
公开(公告)日：2005-03-15
申请号：US09987693
申请日：2001-11-15
申请人： James D. Thornsberry , Gregory Islas , Robert H. Blanpied
发明人： James D. Thornsberry , Gregory Islas , Robert H. Blanpied
IPC分类号： B32B5/18 , B32B27/40 , B32B3/26 , B32B9/00 , B32B27/00
CPC分类号： B32B5/18 , B32B27/40 , Y10T428/249953 , Y10T428/249976 , Y10T428/249987 , Y10T428/249988 , Y10T428/249991 , Y10T428/249992
摘要： A rigid closed cell polyisocyanate-based foams is created by reacting at least one organic polyisocyanate with compounds having at least two active hydrogen atoms in the presence of an n-pentane blowing agent. When the foam is formed into a laminated board with facers, the foam formulation includes a sufficient amount of a common blend of cleaning solvent chemicals to cause a noticeable improvement in facer adhesion. The chemicals used to improve facer adhesion are a standard blend of industrial cleaning solvents called “Di-Basic Esters” or DBE. The actual chemical compounds in one mode of this mixture are the methyl esters of about 59% glutaric acid, about 20% succinic acid, and about 21% adipic acid. The minimum rate of addition of the Di-Basic Esters”[DBE] thought to be effective may be less than about 0.5 parts per hundred parts of polyol (pphpp). The currently preferred embodiments use add-on rates within the range of about 0.5 to about 5.0 pphpp, with the currently most preferred range being from about 1.0 to about 3.0 pphpp. The blend of cleaning chemicals employed by the present invention surprisingly enhance the adhesion between the foam and the facer.
摘要翻译：通过在正戊烷发泡剂的存在下使至少一种有机聚异氰酸酯与具有至少两个活性氢原子的化合物反应来产生刚性的闭孔聚异氰酸酯基泡沫。当泡沫形成具有平板的层压板时，泡沫配方包括足够量的清洁溶剂化学品的共同混合物，以引起表面附着力的明显改善。用于改善表面粘附性的化学品是称为“Di-Basic Esters”或DBE的工业清洁溶剂的标准混合物。该混合物的一种模式中的实际化合物是约59％戊二酸，约20％琥珀酸和约21％己二酸的甲基酯。认为有效的二碱基酯“DBE”的最小添加量可能少于每百份多元醇约0.5份（pphpp）。目前优选的实施方案使用附加率在约0.5 至约5.0pphpp，目前最优选的范围为约1.0至约3.0pphpp。本发明使用的清洁化学品的共混物令人惊奇地增强了泡沫与表面之间的粘合性。

3. 发明申请

US20090023350A1 Building construction felt paper with biocide/anti-microbial treatment 审中-公开
标题翻译：建筑施工用杀菌剂/抗微生物处理毡纸
公开(公告)号：US20090023350A1
公开(公告)日：2009-01-22
申请号：US12216711
申请日：2008-07-09
申请人： Robert H. Blanpied , Freddie Lee Murphy
发明人： Robert H. Blanpied , Freddie Lee Murphy
IPC分类号： B32B5/02
CPC分类号： D21H11/14 , D21H21/36 , Y10T442/20 , Y10T442/2525
摘要： A nonwoven web has a weight sufficient for construction industry use and comprises at least forty percent (40%) recycled waste paper. At least one surface of the web bears a biocide, e.g., has a biocide applied thereto. Preferably the weight of the web is greater than fifteen pounds per thousand square feet (15-lbs/MSF). Preferably the biocide is zinc pyrithione. The web preferably bears at least 50-grams of biocide per thousand square feet per side of said web. One example use of the web is as builders felt, with other uses including as a facer for a laminate board and for asphalt-impregnated webs. The biocide-bearing nonwoven web is specifically directed to use in building construction. One example use of the web is as builders felt, with other uses including as a facer for a laminate board and for asphalt-impregnated webs. Because building construction products must be tough, but priced as low as possible, this web is made largely from recycled waste paper (as opposed to virgin cellulose fiber, as a cost-reducing measure), and optionally clarifier sludge.
摘要翻译：非织造纤维网具有足以用于建筑工业使用的重量，并且包含至少40％（40％）的再生废纸。纤维网的至少一个表面带有杀生物剂，例如具有施加于其上的杀生物剂。优选地，幅材的重量大于十五磅/千平方英尺（15磅/ MSF）。优选地，杀生物剂是吡啶硫酮锌。纤维网优选地在所述纤维网的每侧每千平方英尺承载至少50克的杀生物剂。网的一个示例使用是感觉到的建筑者，其他用途包括作为层压板的面和沥青浸渍的网。具有杀菌剂的非织造纤维网专门用于建筑施工。网的一个示例使用是感觉到的建筑者，其他用途包括作为层压板的面和沥青浸渍的网。由于建筑施工产品必须坚固，但价格尽可能低，因此这种纤维网主要由回收废纸制成（与原始纤维素纤维相反，作为降低成本的措施），以及任选的澄清污泥。

4. 发明授权

US5294647A Method of producing rigid foams and products produced therefrom 失效
标题翻译：生产硬质泡沫的产品及由其生产的产品的方法
公开(公告)号：US5294647A
公开(公告)日：1994-03-15
申请号：US18304
申请日：1993-02-16
申请人： Robert H. Blanpied , Robert J. Butkus , Andy I. McLaughlin , Richard L. Donald
发明人： Robert H. Blanpied , Robert J. Butkus , Andy I. McLaughlin , Richard L. Donald
IPC分类号： C08G18/16 , C08G18/76 , C08J9/14 , C08J9/30
CPC分类号： C08J9/30 , C08G18/163 , C08G18/7664 , C08J9/144 , C08G2101/0025 , C08G2101/005 , C08G2105/02 , C08J2375/04 , Y10S521/902
摘要： In a method of producing a thermosetting foam, a first of two foam forming blends ("A-Blend") is prepared using a multi-functional isocyanate such as polymeric polymethylene polyphenylisocyanate ("PMDI"). A second of two foam forming blends ("B-Blend") is prepared by mixing together a polyol; water; a tertiary amine catalyst having at least two hydrogen bonding sites for one molecule; and, an alkali metal organo-salt catalyst. The tertiary amine catalyst is of a type wherein both the hydrogen segment and the hydroxyl segment of water are attracted by both of the hydrogen bonding cites on the catalyst molecule essentially simultaneously. A first blowing agent is included with one of the two foam forming blends. When the first and second foam forming blends are mixed together, the tertiary amine catalyst quickly initiates a reaction predominately of the polymeric polymethylene polyphenylisocyanate with water (as opposed to a reaction with the polyol). The quick reaction of the PMDI with water causes, prior to a gel point of the foam, both (1) the production of a second blowing agent for forming cells in the blends and for causing expansion in the liquid blends; and (2) sufficient exothermic heat to initiate boiling of the first blowing agent. Relatively large amounts of alkali metal organo-salt catalyst induce rapid vaporizing of the first blowing agent due to a high level of exothermic heat, whereby expansion of the mixed blends is substantially completed prior to the effective conversion of the mixed liquid blends to a solid. According to the method, a degree of completion of expansion of the foam at any point in time exceeds a degree of completion of chemical reactions of the foam. In another mode of the invention, a frothing agent is also employed.
摘要翻译：在制备热固性泡沫的方法中，使用多官能异氰酸酯如聚合多亚甲基多苯基异氰酸酯（“PMDI”）制备两种泡沫形成共混物中的第一种（“A-Blend”）。通过将多元醇混合在一起制备两种泡沫形成共混物（“B-Blend”）中的第二种; 水; 一个分子具有至少两个氢键位置的叔胺催化剂; 和碱金属有机盐催化剂。叔胺催化剂是一种类型，其中氢链段和水的羟基部分基本上同时地被催化剂分子上的氢键引物吸引。第一发泡剂包括在两种泡沫形成共混物之一中。当第一和第二泡沫形成共混物混合在一起时，叔胺催化剂迅速引发聚合物多亚甲基多苯基异氰酸酯与水的反应（与与多元醇的反应相反）。 PMDI与水的快速反应在泡沫的凝胶点之前导致（1）生产用于在共混物中形成细胞并引起液体共混物膨胀的第二发泡剂; 和（2）充分的放热以引发第一发泡剂的沸腾。相对大量的碱金属有机盐催化剂由于高水平的放热导致第一发泡剂的快速蒸发，从而在将混合液体共混物有效转化为固体之前基本上完成了混合共混物的膨胀。根据该方法，泡沫在任何时间点的膨胀完成程度都超过了泡沫化学反应的完成程度。在本发明的另一方式中，也采用发泡剂。

5. 发明授权

US07867927B2 Method and composition for coating mat and articles produced therewith 有权
标题翻译：用于涂覆垫和用其制造的制品的方法和组合物
公开(公告)号：US07867927B2
公开(公告)日：2011-01-11
申请号：US11508338
申请日：2006-08-23
申请人： Philip Bush , Robert H. Blanpied , Freddie Lee Murphy , Jimmy Rogers Dubose
发明人： Philip Bush , Robert H. Blanpied , Freddie Lee Murphy , Jimmy Rogers Dubose
IPC分类号： B32B3/00 , B32B17/02 , A61F13/15
CPC分类号： D06N3/0022 , B05C1/12 , B05C11/04 , B28B19/0092 , B28B23/0006 , B32B17/10018 , B32B27/36 , D06N3/0063 , D06N2205/023 , Y10T428/237 , Y10T428/249955 , Y10T428/249956 , Y10T428/273 , Y10T442/20 , Y10T442/2139 , Y10T442/2926 , Y10T442/2992 , Y10T442/60
摘要： A coated glass mat comprises a glass mat substrate having non-woven glass fibers and a coating which essentially uniformly penetrates the glass mat substrate to desired fractional thickness of the coated glass mat. The coating imparts a tensile strength to the coated glass mat which on average is at least 1.33 times greater than the tensile strength of the glass mat substrate without the coating. In example embodiments, penetration of the coating into the glass mat substrate preferably extends to a depth of from twenty five percent of a thickness of the coated glass mat to seventy five percent of the thickness of the coated glass mat. Moreover, a non-coated thickness of the coated glass mat is sufficiently thick for bonding purposes with, e.g., a gypsum slurry or other core materials such as thermoplastic or thermosetting plastics. The coating has a porosity in a range of from 1.3 CFM to 5.0 CFM, e.g., the coating comprises a coating blend which provides the coated glass mat with a porosity sufficient to allow water vapor to escape from a gypsum slurry when heated. The coating is preferably a coating blend comprised of water, latex binder, inorganic pigment, and inorganic binder.
摘要翻译：涂覆的玻璃垫包括具有无纺玻璃纤维的玻璃垫基材和基本上均匀地穿透玻璃垫基材的涂层，以使涂覆的玻璃垫的所需分数厚度。涂层赋予涂覆的玻璃毡的拉伸强度，其平均比玻璃垫基材的拉伸强度平均高1.33倍，而不需要涂层。在示例性实施例中，将涂层穿透到玻璃垫衬底中优选地延伸到涂覆的玻璃垫的厚度的二十五％的深度至涂覆的玻璃垫的厚度的百分之七十五。此外，涂覆的玻璃毡的未涂覆厚度足够厚以用于例如石膏浆料或其它芯材料如热塑性或热固性塑料的粘合目的。该涂层具有在1.3CFM至5.0CFM范围内的孔隙度，例如，该涂层包括一涂层共混物，该涂层共混物提供具有足够的孔隙度的涂覆的玻璃毡，以允许水蒸汽在加热时从石膏浆料逸出。涂层优选是由水，胶乳粘合剂，无机颜料和无机粘合剂组成的涂料共混物。

6. 发明授权

US5254600A Method of producing rigid foams and products produced therefrom 失效
标题翻译：生产硬质泡沫的产品及由其生产的产品的方法
公开(公告)号：US5254600A
公开(公告)日：1993-10-19
申请号：US851889
申请日：1992-03-16
申请人： Robert H. Blanpied , Robert J. Butkus , Andy I. McLaughlin , Richard L. Donald
发明人： Robert H. Blanpied , Robert J. Butkus , Andy I. McLaughlin , Richard L. Donald
IPC分类号： C08G18/16 , C08G18/76 , C08J9/14 , C08J9/30 , C08G18/18 , C08G18/22 , C08J9/08
CPC分类号： C08J9/30 , C08G18/163 , C08G18/7664 , C08J9/144 , C08G2101/0025 , C08G2105/02 , C08J2375/04
摘要： In a method of producing a thermosetting foam, a first of two foam forming blends ("A-Blend") is prepared using a multi-functional isocyanate such as polymeric polymethylene polyphenylisocyanate ("PMDI"). A second of two foam forming blends ("B-Blend") is prepared by mixing together a polyol; water; a tertiary amine catalyst having at least two hydrogen bonding sites for one molecule; and, an alkali metal organo-salt catalyst. The tertiary amine catalyst is of a type wherein both the hydrogen segment and the hydroxyl segment of water are attracted by both of the hydrogen bonding cites on the catalyst molecule essentially simultaneously. A first blowing agent is included with one of the two foam forming blends. When the first and second foam forming blends are mixed together, the tertiary amine catalyst quickly initiates a reaction predominately of the polymeric polymethylene polyphenylisocyanate with water (as opposed to a reaction with the polyol). The quick reaction of the PMDI with water causes, prior to a gel point of the foam, both (1) the production of a second blowing agent for forming cells in the blends and for causing expansion in the liquid blends; and (2) sufficient exothermic heat to initiate boiling of the first blowing agent. Relatively large amounts of alkali metal organo-salt catalyst induce rapid vaporizing of the first blowing agent due to a high level of exothermic heat, whereby expansion of the mixed blends is substantially completed prior to the effective conversion of the mixed liquid blends to a solid. According to the method, a degree of completion of expansion of the foam at any point in time exceeds a degree of completion of chemical reactions of the foam. In another mode of the invention, a frothing agent is also employed.
摘要翻译：在制备热固性泡沫的方法中，使用多官能异氰酸酯如聚合多亚甲基多苯基异氰酸酯（“PMDI”）制备两种泡沫形成共混物中的第一种（“A-Blend”）。通过将多元醇混合在一起制备两种泡沫形成共混物（“B-Blend”）中的第二种; 水; 一个分子具有至少两个氢键位置的叔胺催化剂; 和碱金属有机盐催化剂。叔胺催化剂是一种类型，其中氢链段和水的羟基部分基本上同时地被催化剂分子上的氢键引物吸引。第一发泡剂包括在两种泡沫形成共混物之一中。当第一和第二泡沫形成共混物混合在一起时，叔胺催化剂迅速引发聚合物多亚甲基多苯基异氰酸酯与水的反应（与与多元醇的反应相反）。 PMDI与水的快速反应在泡沫的凝胶点之前导致（1）生产用于在共混物中形成细胞并引起液体共混物膨胀的第二发泡剂; 和（2）足够的放热以引发第一发泡剂的沸腾。相对大量的碱金属有机盐催化剂由于高水平的放热导致第一发泡剂的快速蒸发，从而在将混合液体共混物有效转化为固体之前基本上完成了混合共混物的膨胀。根据该方法，泡沫在任何时间点的膨胀完成程度都超过了泡沫化学反应的完成程度。在本发明的另一方式中，也采用发泡剂。

7. 发明授权

US5102728A Method and composition for coating mat and articles produced therewith 失效
标题翻译：用于涂覆垫和用其制造的制品的方法和组合物
公开(公告)号：US5102728A
公开(公告)日：1992-04-07
申请号：US658523
申请日：1991-02-21
申请人： William M. Gay , Robert H. Blanpied , Philip W. Bush , Richard L. Donald , James L. Williams , James H. Williams
发明人： William M. Gay , Robert H. Blanpied , Philip W. Bush , Richard L. Donald , James L. Williams , James H. Williams
IPC分类号： B29C67/24 , B29C70/00
CPC分类号： B29C70/00 , B29C67/248 , B29K2309/08 , Y10T428/31815 , Y10T442/2221
摘要： A coating composition and method of producing a non-porous mat includes coating a predominantly glass fiber porous web substrate. The coating comprises an aqueous mixture of a mineral pigment; a first binder material comprised of a polymer latex adhesive material; and, a second binder material comprised of asphalt emulsion material. The total dry weight basis of both binders does not exceed 24% of the total coating.
摘要翻译：涂料组合物和无孔垫的制造方法包括涂覆主要为玻璃纤维多孔网的基材。涂层包含矿物颜料的水性混合物; 由聚合物胶乳粘合剂材料构成的第一粘合剂材料; 和由沥青乳液材料组成的第二粘合剂材料。两种粘合剂的总干重基础不超过总涂层的24％。

8. 发明授权

US07645490B2 Method and composition for coating mat and articles produced therewith 有权
标题翻译：用于涂覆垫和用其制造的制品的方法和组合物
公开(公告)号：US07645490B2
公开(公告)日：2010-01-12
申请号：US10891485
申请日：2004-07-15
申请人： Philip Bush , Robert H. Blanpied , Freddie Lee Murphy , Jimmy Rogers DuBose , Joseph M. Konieczka
发明人： Philip Bush , Robert H. Blanpied , Freddie Lee Murphy , Jimmy Rogers DuBose , Joseph M. Konieczka
IPC分类号： B05D1/28 , B05D7/00
CPC分类号： B28B19/0092 , B05C1/12 , B05C11/04 , B28B23/0006 , B32B17/10018 , B32B27/36 , D06N3/0022 , D06N3/0086 , D06N2209/1692 , Y10T442/2139
摘要： A coated glass mat comprises a glass mat substrate having non-woven glass fibers and a coating which essentially uniformly penetrates the glass mat substrate to desired fractional thickness of the coated glass mat. The coating imparts a tensile strength to the coated glass mat which on average is at least 1.33 times greater than the tensile strength of the glass mat substrate without the coating. In example embodiments, penetration of the coating into the glass mat substrate preferably extends to a depth of from twenty five percent of a thickness of the coated glass mat to seventy five percent of the thickness of the coated glass mat. Moreover, a non-coated thickness of the coated glass mat is sufficiently thick for bonding purposes with, e.g., a gypsum slurry or other core materials such as thermoplastic or thermosetting plastics. The coating has a porosity in a range of from 1.3 CFM to 5.0 CFM, e.g., the coating comprises a coating blend which provides the coated glass mat with a porosity sufficient to allow water vapor to escape from a gypsum slurry when heated. The coating is preferably a coating blend comprised of water, latex binder, inorganic pigment, and inorganic binder.
摘要翻译：涂覆的玻璃垫包括具有无纺玻璃纤维的玻璃垫基材和基本上均匀地穿透玻璃垫基材的涂层，以使涂覆的玻璃垫的所需分数厚度。涂层赋予涂覆的玻璃毡的拉伸强度，其平均比玻璃垫基材的拉伸强度平均高1.33倍，而不需要涂层。在示例性实施例中，将涂层穿透到玻璃垫衬底中优选地延伸到涂覆的玻璃垫的厚度的二十五％的深度至涂覆的玻璃垫的厚度的百分之七十五。此外，涂覆的玻璃毡的未涂覆厚度足够厚以用于例如石膏浆料或其它芯材料如热塑性或热固性塑料的粘合目的。该涂层具有在1.3CFM至5.0CFM范围内的孔隙度，例如，该涂层包括一涂层共混物，该涂层共混物提供具有足够的孔隙度的涂覆的玻璃毡，以允许水蒸汽在加热时从石膏浆料逸出。涂层优选是由水，胶乳粘合剂，无机颜料和无机粘合剂组成的涂料共混物。

9. 发明授权

US07138346B2 Method and composition for coating mat and articles produced therewith 有权
公开(公告)号：US07138346B2
公开(公告)日：2006-11-21
申请号：US10324109
申请日：2002-12-20
申请人： Philip Bush , Robert H. Blanpied , Freddie Lee Murphy , Jimmy Rogers Dubose
发明人： Philip Bush , Robert H. Blanpied , Freddie Lee Murphy , Jimmy Rogers Dubose
IPC分类号： B32B17/02
CPC分类号： D06N3/0022 , B05C1/12 , B05C11/04 , B28B19/0092 , B28B23/0006 , B32B17/10018 , B32B27/36 , D06N3/0063 , D06N2205/023 , Y10T428/237 , Y10T428/249955 , Y10T428/249956 , Y10T428/273 , Y10T442/20 , Y10T442/2139 , Y10T442/2926 , Y10T442/2992 , Y10T442/60
摘要： A coated glass mat comprises a glass mat substrate having non-woven glass fibers and a coating which essentially uniformly penetrates the glass mat substrate to desired fractional thickness of the coated glass mat. The coating imparts a tensile strength to the coated glass mat which on average is at least 1.33 times greater than the tensile strength of the glass mat substrate without the coating. In example embodiments, penetration of the coating into the glass mat substrate preferably extends to a depth of from twenty five percent of a thickness of the coated glass mat to seventy five percent of the thickness of the coated glass mat. Moreover, a non-coated thickness of the coated glass mat is sufficiently thick for bonding purposes with, e.g., a gypsum slurry or other core materials such as thermoplastic or thermosetting plastics. The coating has a porosity in a range of from 1.3 CFM to 5.0 CFM, e.g., the coating comprises a coating blend which provides the coated glass mat with a porosity sufficient to allow water vapor to escape from a gypsum slurry when heated. The coating is preferably a coating blend comprised of water, latex binder, inorganic pigment, and inorganic binder.

10. 发明授权

US06572736B2 Non-woven web made with untreated clarifier sludge 有权
公开(公告)号：US06572736B2
公开(公告)日：2003-06-03
申请号：US09971772
申请日：2001-10-09
申请人： Philip Bush , Ricky Burkeen , Robert H. Blanpied
发明人： Philip Bush , Ricky Burkeen , Robert H. Blanpied
IPC分类号： D21H1701
CPC分类号： B32B5/18 , B32B5/02 , B32B5/245 , B32B5/26 , B32B2262/062 , B32B2262/101 , D21B1/32 , D21F1/66 , D21F11/00 , D21H11/14 , D21H13/40 , D21H17/01 , D21J1/16 , Y02W30/646 , Y10T428/249953 , Y10T428/249976 , Y10T428/249987
摘要： The non-woven web of the present invention is comprised of recycled cellulose fiber and untreated Clarifier Sludge, and optionally, recycled glass fiber. Unlike uses of reclaimed Clarifier Sludge whereby the material has been treated in some fashion to improve its quality, the non-woven web of the present invention utilizes untreated Clarifier Sludge. The Clarifier Sludge of the present invention is dry enough to handle, and in one example varies between about 30% and about 45% solids. The Clarifier Sludge can be added to web-forming equipment (e.g., papermaking equipment) either in a waste paper disintegrator or into a recycling apparatus (e.g., broke pulper) whose output is metered into a refiner tank of the web-forming equipment. In an embodiment utilizing a broke pulper for introduction of the Clarifier Sludge, the broke pulper is filled with clarifier sludge and water to a consistency of about 3.5% solids.

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