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1. 发明授权

US09266738B2 Organometallic chemistry of extended periodic II-electron systems 有权
标题翻译：扩展周期性II电子系统的有机金属化学
公开(公告)号：US09266738B2
公开(公告)日：2016-02-23
申请号：US13879477
申请日：2011-10-14
申请人： Robert C. Haddon , Santanu Sarkar , Sandip Niyogi , Elena Bekyarova , Mikhail E. Itkis , Xiaojuan Tian , Feihu Wang
发明人： Robert C. Haddon , Santanu Sarkar , Sandip Niyogi , Elena Bekyarova , Mikhail E. Itkis , Xiaojuan Tian , Feihu Wang
IPC分类号： C01B31/04 , C01B31/02 , B82Y10/00 , H01B1/04 , H01L29/16 , H01L51/00 , B82Y30/00 , B82Y40/00
CPC分类号： C01B31/0484 , B82Y10/00 , B82Y30/00 , B82Y40/00 , C01B32/174 , C01B32/19 , C01B32/194 , C01B32/20 , C01B2202/02 , C01B2202/04 , C01B2202/06 , C01B2204/02 , C01B2204/04 , H01B1/04 , H01L29/1606 , H01L51/0049
摘要： A method of modifying a carbon material is disclosed. The method comprises: bonding a metal to a carbon material to form a metal-carbon complex comprising the metal and a benzene unit, wherein the carbon material comprises extended sp2-bonded carbon atoms.
摘要翻译：公开了一种改性碳材料的方法。该方法包括：将金属键合到碳材料上以形成包含金属和苯单元的金属 - 碳络合物，其中碳材料包含延伸的sp2键合的碳原子。

2. 发明授权

US08454923B2 Continuous extraction technique for the purification of carbon nanomaterials 有权
标题翻译：用于碳纳米材料净化的连续提取技术
公开(公告)号：US08454923B2
公开(公告)日：2013-06-04
申请号：US12969534
申请日：2010-12-15
申请人： Robert C. Haddon
发明人： Robert C. Haddon
IPC分类号： D01F9/12
CPC分类号： B82Y30/00 , B01D21/2427 , B82Y40/00 , C01B32/17 , C01B2202/02 , C01B2202/04 , C01B2202/06 , C07D307/12
摘要： Systems and methods for the extraction of carbon nanotubes (CNTs) by continuous and/or batch processing are disclosed. Generally, a carbon nanotube material including carbon nanotubes (CNTs), carbon nanoparticles (CNPs), and carboxylated carbon (CC) is provided and agitated to produce a well-dispersed mixture. The well-dispersed mixture can be allowed to stand in a vessel having a lower end and an upper end. In some cases, the CNPs settle at the lower end. In some cases, at least some of the CNTs and CC are disposed at the upper end and can be removed in a dispersion, which can be pH adjusted and/or filtered to extract the CNTs from the CC.
摘要翻译：公开了通过连续和/或间歇处理提取碳纳米管（CNT）的系统和方法。通常，提供包含碳纳米管（CNT），碳纳米颗粒（CNP）和羧化碳（CC）的碳纳米管材料并搅拌以产生良好分散的混合物。可将良好分散的混合物静置在具有下端和上端的容器中。在某些情况下，国家调查组织处于低端地位。在一些情况下，至少一些CNT和CC设置在上端，并且可以在分散体中除去，其可以进行pH调节和/或过滤以从CC中提取CNT。

3. 发明授权

US4249013A Conjugatively linked tetrathiafulvalenes and method for preparation thereof 失效
标题翻译：共轭连接的四硫富瓦烯及其制备方法
公开(公告)号：US4249013A
公开(公告)日：1981-02-03
申请号：US6655
申请日：1979-01-26
申请人： Robert C. Haddon , Martin L. Kaplan , Fred Wudl
发明人： Robert C. Haddon , Martin L. Kaplan , Fred Wudl
IPC分类号： C07D339/06
CPC分类号： C07D339/06
摘要： A technique is described for the preparation of novel conjugatively linked tetrathiafulvalenes. The resultant molecule includes two donor moieties which allow the preparation of charge transfer complexes with a band structure higher than the quasi one dimensional structure indigenous to presently known electrically conducting organic complexes.
摘要翻译：描述了一种用于制备新型共轭连接的四硫富瓦烯的技术。所得分子包括两个供体部分，其允许制备具有高于目前已知的导电有机络合物所固有的准一维结构的带结构的电荷转移络合物。

4. 发明授权

US08592612B1 Water soluble carbon nanotubes 有权
标题翻译：水溶性碳纳米管
公开(公告)号：US08592612B1
公开(公告)日：2013-11-26
申请号：US13087306
申请日：2011-04-14
申请人： Robert C. Haddon , Irina Kalinina , Elena Bekyarova
发明人： Robert C. Haddon , Irina Kalinina , Elena Bekyarova
IPC分类号： C07D307/12
CPC分类号： C07D307/12
摘要： Embodiments of the present disclosure present systems and methods for the synthesis of carbon nanotubes (CNTs) functionalized with mono-terminated, protected polyethylene glycol (PEG). As compared with bi-functional PEG, mono-terminated PEG the PEG-THFF oligomer has only one reaction site. The use of mono-terminated PEG may enhance the solubility of CNTs functionalized with mono-terminated PEG by inhibiting cross-linking between nanotubes and leads to a dramatic increase in aqueous solubility. In an example, single-walled carbon nanotubes functionalized with PEG having a tetrahydrofurfuryl (THFF) terminal group (SWNT-PEG-THFF) is found to disperse in water by ultrasonication and forms stable viscous dispersions at concentrations as high as about 9 g/L. This result exceeds the solubility of a previously reported SWNT-PEG graft copolymer, approximately 6 g/L, by more than 30%.
摘要翻译：本公开的实施方案提供用于合成用单末端，保护的聚乙二醇（PEG）官能化的碳纳米管（CNT）的系统和方法。与双功能PEG相比，单封端PEG PEG-THFF低聚物只有一个反应位点。使用单封端PEG可以通过抑制纳米管之间的交联来增强用单末端PEG功能化的CNT的溶解度，并导致水溶性的显着增加。在一个实例中，发现用具有四氢糠基（THFF）端基（SWNT-PEG-THFF）的PEG官能化的单壁碳纳米管通过超声波分散在水中，并以高达约9g / L的浓度形成稳定的粘稠分散体。该结果超过先前报道的约6g / L的SWNT-PEG接枝共聚物的溶解度超过30％。

5. 发明授权

US07867468B1 Multiscale carbon nanotube-fiber reinforcements for composites 有权
标题翻译：用于复合材料的多尺度碳纳米管纤维增强材料
公开(公告)号：US07867468B1
公开(公告)日：2011-01-11
申请号：US12039526
申请日：2008-02-28
申请人： Robert C. Haddon , Mikhail E. Itkis , Elena Bekyarova , Aiping Yu
发明人： Robert C. Haddon , Mikhail E. Itkis , Elena Bekyarova , Aiping Yu
IPC分类号： D01F9/12
CPC分类号： D01F11/125 , B29C70/081 , B29C70/24 , B29K2105/122 , B82Y30/00 , B82Y40/00 , C01B32/158 , C01B32/174 , C01B2202/02 , C01B2202/06 , C01B2202/34 , C25D13/02 , C25D13/04 , C25D13/20 , D06M10/06 , D06M11/74 , Y10S977/72 , Y10S977/742
摘要： Systems and methods for the preparation of reinforcements for composite materials, whereby single- and/or multi-walled carbon nanotubes (CNTs) may be electrophoretically deposited on fibrous substrates for the production of hybrid CNT/fibers. The fibers may include carbon fibers and woven carbon fabrics. The length, as well as the density and orientation of the deposited nanotubes on the fiber surfaces may also be tailored. The strength of the CNT/fiber-matrix interface formed in composites fabricated from the hybrid CNT/fibers may be adjusted by introduction of functional groups on the CNT/fiber surfaces, such as aminophenyl and carboxyphenyl groups.
摘要翻译：用于制备复合材料增强物的系统和方法，其中单壁和/或多壁碳纳米管（CNT）可以电泳沉积在纤维基材上用于生产杂化CNT /纤维。纤维可以包括碳纤维和编织碳织物。纤维表面上沉积的纳米管的长度以及密度和取向也可以被定制。可以通过在CNT /纤维表面上引入官能团，例如氨基苯基和羧基苯基来调节由杂化CNT /纤维制成的复合材料中形成的CNT /纤维 - 基质界面的强度。

6. 发明授权

US06670179B1 Molecular functionalization of carbon nanotubes and use as substrates for neuronal growth 有权
标题翻译：碳纳米管的分子官能化和用作神经元生长的底物
公开(公告)号：US06670179B1
公开(公告)日：2003-12-30
申请号：US09920213
申请日：2001-08-01
申请人： Mark P. Mattson , Robert C. Haddon , Apparao M. Rao
发明人： Mark P. Mattson , Robert C. Haddon , Apparao M. Rao
IPC分类号： C12N500
CPC分类号： C12N5/0075 , B82Y5/00 , C12N5/0619 , C12N2533/10 , Y10S977/746
摘要： A cell and substrate system and nerve regeneration implant are disclosed including a carbon nanotube and a neuron growing on the carbon nanotube. Both unfunctionalized carbon nanotubes and carbon nanotubes functionalized with a neuronal growth promoting agent may be utilized in the invention. A method is also disclosed for promoting neuronal growth.
摘要翻译：公开了一种细胞和底物系统和神经再生植入物，包括碳纳米管和在碳纳米管上生长的神经元。在本发明中可以使用两种未官能化的碳纳米管和用神经元生长促进剂官能化的碳纳米管。还公开了用于促进神经元生长的方法。

7. 发明授权

US5391323A Conductivity in carbonaceous compounds and devices using such compounds 失效
标题翻译：含碳化合物和使用这些化合物的装置的电导率
公开(公告)号：US5391323A
公开(公告)日：1995-02-21
申请号：US156664
申请日：1993-11-22
申请人： Robert C. Haddon , Arthur F. Hebard , Donald W. Murphy , Matthew J. Rosseinsky
发明人： Robert C. Haddon , Arthur F. Hebard , Donald W. Murphy , Matthew J. Rosseinsky
IPC分类号： C01B31/02 , H01B1/04 , C01B31/00
CPC分类号： B82Y30/00 , B82Y40/00 , C01B31/0206 , C01B31/0213 , H01B1/04 , Y10S423/39 , Y10S423/40 , Y10S505/80 , Y10S977/735
摘要： Carbonaceous materials based on the fullerene molecules have been developed which allow for high conductivity (comparable to or higher than those attained by n-type doped polyacetylene). The fullerene materials are soluble in common solvents.
摘要翻译：已经开发了基于富勒烯分子的碳质材料，其允许高导电性（与由n型掺杂的聚乙炔获得的那些相当或更高）。富勒烯材料可溶于普通溶剂。

8. 发明授权

US08449858B2 Continuous extraction technique for the purification of carbon nanomaterials 有权
标题翻译：用于碳纳米材料净化的连续提取技术
公开(公告)号：US08449858B2
公开(公告)日：2013-05-28
申请号：US12813239
申请日：2010-06-10
申请人： Robert C. Haddon
发明人： Robert C. Haddon
IPC分类号： C09C1/56
CPC分类号： B82Y30/00 , B03D3/00 , B82Y40/00 , C01B32/15
摘要： Systems and methods for the purification of carbon nanotubes (CNTs) by continuous liquid extraction are disclosed. Carbon nanotubes are introduced to a flow of liquid that enables the separation of CNTs from impurities due to differences in the dispersibility of the CNTs and the impurities within the liquid. Examples of such impurities may include amorphous carbon, graphitic nanoparticles, and metal containing nanoparticles. The continuous extraction process may be performed in one or more stages, where one or more of extraction parameters may be varied between the stages of the continuous extraction process in order to effect removal of selected impurities from the CNTs. The extraction parameters may include, but are not limited to, the extraction liquid, the flow rate of the extraction liquid, the agitation of the liquid, and the pH of the liquid, and may be varied, depending on the impurity to be removed from the CNTs.
摘要翻译：公开了通过连续液体提取来净化碳纳米管（CNT）的系统和方法。将碳纳米管引入到液体流中，由于CNT和液体中的杂质的分散性的差异，能够将CNT与杂质分离。这种杂质的实例可以包括无定形碳，石墨纳米颗粒和含金属的纳米颗粒。连续提取过程可以在一个或多个阶段中进行，其中一个或多个提取参数可以在连续提取过程的阶段之间变化，以便从CNT中去除所选择的杂质。提取参数可以包括但不限于提取液体，萃取液的流速，液体的搅拌和液体的pH值，并且可以根据要除去的杂质而变化碳纳米管。

9. 发明申请

US20110068290A1 CHEMICAL MODULATION OF ELECTRONIC AND MAGNETIC PROPERTIES OF GRAPHENE 审中-公开
标题翻译：石墨的电子和磁性的化学调制
公开(公告)号：US20110068290A1
公开(公告)日：2011-03-24
申请号：US12994678
申请日：2009-05-29
申请人： Robert C. Haddon , Mikhail E. Itkis , Palanisamy Ramesh , Elena Bekyarova , Sakhrat Khizroev , Jeongmin Hong
发明人： Robert C. Haddon , Mikhail E. Itkis , Palanisamy Ramesh , Elena Bekyarova , Sakhrat Khizroev , Jeongmin Hong
IPC分类号： H01F1/42 , C07C63/42 , C07C39/225 , C07C22/04 , C07C15/20 , H01B1/12 , C07C17/02 , C07C45/27 , C07C49/603 , C01B31/00 , C07D303/04 , C25B3/00 , B82Y30/00 , B82Y40/00
CPC分类号： G01N33/6893 , C12Q1/6881 , C12Q2600/158 , G01N33/5088 , G01N2800/085 , G01N2800/122 , G01N2800/324 , G01N2800/347 , H01F1/405
摘要： Compounds, compositions, systems and methods for the chemical and electrochemical modification of the electronic structure of graphene and especially epitaxial graphene (EG) are presented. Beneficially, such systems and methods allow the large-scale fabrication of electronic EG devices. Vigorous oxidative conditions may allow substantially complete removal of the EG carbon atoms and the generation of insulating regions; such processing is equivalent to that which is currently used in the semiconductor industry to lithographically etch or oxidize silicon and thereby define the physical features and electronic structure of the devices. However graphene offers an excellent opportunity for controlled modification of the hybridization of the carbon atoms from sp2 to sp3 states by chemical addition of organic functional groups. We show that such chemistries offer opportunities far beyond those currently employed in the semiconductor industry for control of the local electronic structure of the graphene sheet and do not require the physical removal of areas of graphene or its oxidation, in order to generate the full complement of electronic devices necessary to produce functional electronic circuitry. Selective saturation of the π-bonds opens a band gap in the graphene electronic structure which results in a semiconducting or insulating form of graphene, while allowing the insertion of new functionality with the possibility of 3-D electronic architectures. Beneficially, these techniques allow for large-scale fabrication of electronic EG devices and integrated circuits, as they allow the generation of wires (interconnects), semiconductors (transistors), dielectrics, and insulators.
摘要翻译：介绍了石墨烯，特别是外延石墨烯（EG）的电子结构的化学和电化学改性的化合物，组合物，体系和方法。有利的是，这种系统和方法允许电子EG装置的大规模制造。强烈的氧化条件可以允许基本上完全除去EG碳原子和产生绝缘区域; 这种处理相当于目前在半导体工业中用于光刻蚀刻或氧化硅的方法，从而限定了器件的物理特征和电子结构。然而，石墨烯提供了通过化学添加有机官能团来控制改变sp2到sp3状态的碳原子的杂化的极好的机会。我们表明，这些化学品提供的机会远远超出目前在半导体工业中使用的机会，用于控制石墨烯片的局部电子结构，并且不需要物理去除石墨烯的区域或其氧化，以产生完整的生产功能电子电路所需的电子设备。石墨烯电子结构的选择饱和打开了石墨烯电子结构中的带隙，导致石墨烯的半导体或绝缘形式，同时允许以3-D电子架构的可能性插入新功能。有利的是，这些技术允许电子EG器件和集成电路的大规模制造，因为它们允许生成导线（互连），半导体（晶体管），电介质和绝缘体。

10. 发明申请

US20100140792A1 GRAPHITE NANOPLATELETS FOR THERMAL AND ELECTRICAL APPLICATIONS 审中-公开
标题翻译：用于热和电应用的石墨纳米薄膜
公开(公告)号：US20100140792A1
公开(公告)日：2010-06-10
申请号：US12513151
申请日：2007-10-31
申请人： Robert C. Haddon , Mikhail E. Itkis , Palanisamy Ramesh , Aiping Yu , Elena Bekyarova , Kimberly Worsley
发明人： Robert C. Haddon , Mikhail E. Itkis , Palanisamy Ramesh , Aiping Yu , Elena Bekyarova , Kimberly Worsley
IPC分类号： H01L23/36 , C01B31/04 , C09K5/00 , B32B9/00
CPC分类号： H01L23/3737 , B82Y30/00 , B82Y40/00 , C01B32/15 , C01B32/19 , C01B32/22 , C01B32/225 , C01B2204/04 , C10M103/02 , C10M125/02 , C10M2201/041 , C10N2220/082 , H01L23/373 , H01L2924/0002 , Y10T428/2982 , H01L2924/00
摘要： This disclosure concerns a procedure for bulk scale preparation of high aspect ratio, 2-dimensional nano platelets comprised of a few graphene layers, Gn. n may, for example, vary between about 2 to 10. Use of these nano platelets in applications such as thermal interface materials, advanced composites, and thin film coatings provide material systems with superior mechanical, electrical, optical, thermal, and antifriction characteristics.
摘要翻译：本公开涉及用于大规模制备高纵横比，由几个石墨烯层Gn组成的二维纳米片晶的方法。例如，n可以在约2至10之间变化。在诸如热界面材料，高级复合材料和薄膜涂层的应用中使用这些纳米片晶为材料系统提供优异的机械，电学，光学，热和抗摩擦特性。

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