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1. 发明授权

US08889230B2 Side chain fluorochemicals with crystallizable spacer groups 有权
标题翻译：具有可结晶间隔基团的侧链含氟化合物
公开(公告)号：US08889230B2
公开(公告)日：2014-11-18
申请号：US12377873
申请日：2007-08-17
申请人： Richard M. Flynn , Michael A. Yandrasits
发明人： Richard M. Flynn , Michael A. Yandrasits
IPC分类号： C08F18/20 , C09D133/16 , C08F220/24 , C07C67/14 , C07C29/62 , C07C29/58 , C07C69/653
CPC分类号： C07C69/653 , C07C29/58 , C07C29/62 , C07C67/14 , C08F220/24 , Y10T428/3154 , C07C29/147 , C07C33/025 , C07C31/34 , C07C31/38
摘要： A fluorochemical derived from monomers with a side chain, wherein the side chain includes a perfluoroalkyl group with 1-6 carbon atoms and a hydrocarbon spacer group attached to the perfluoroalkyl group, wherein the spacer group has 15-50 carbon atoms. The perfluoroalkyl group is non-crystallizable at room temperature and the spacer group is crystallizable at room temperature.
摘要翻译：衍生自具有侧链的单体的含氟化合物，其中侧链包括具有1-6个碳原子的全氟烷基和连接到全氟烷基的烃间隔基，其中间隔基具有15-50个碳原子。全氟烷基在室温下不可结晶，间隔基在室温下可结晶。

2. 发明申请

US20100234521A1 SIDE CHAIN FLUOROCHEMICALS WITH CRYSTALLIZABLE SPACER GROUPS 有权
标题翻译：具有可结晶间隔组的侧链荧光化学
公开(公告)号：US20100234521A1
公开(公告)日：2010-09-16
申请号：US12377873
申请日：2007-08-17
申请人： Richard M. Flynn , Michael A. Yandrasits
发明人： Richard M. Flynn , Michael A. Yandrasits
IPC分类号： C08L27/12 , C08F220/22 , C08F214/18 , C07C69/54
CPC分类号： C07C69/653 , C07C29/58 , C07C29/62 , C07C67/14 , C08F220/24 , Y10T428/3154 , C07C29/147 , C07C33/025 , C07C31/34 , C07C31/38
摘要： A fluorochemical derived from monomers with a side chain, wherein the side chain includes a perfluoroalkyl group with 1-6 carbon atoms and a hydrocarbon spacer group attached to the perfluoroalkyl group, wherein the spacer group has 15-50 carbon atoms. The perfluoroalkyl group is non-crystallizable at room temperature and the spacer group is crystallizable at room temperature.
摘要翻译：衍生自具有侧链的单体的含氟化合物，其中侧链包括具有1-6个碳原子的全氟烷基和连接到全氟烷基的烃间隔基，其中间隔基具有15-50个碳原子。全氟烷基在室温下不可结晶，间隔基在室温下可结晶。

3. 发明授权

US06649719B2 Degradable, amorphous, fluorochemical acrylate polymers 有权
标题翻译：可降解的，无定形的含氟丙烯酸酯聚合物
公开(公告)号：US06649719B2
公开(公告)日：2003-11-18
申请号：US09931215
申请日：2001-08-16
申请人： George G. I. Moore , Michael A. Yandrasits , Jay F. Schulz , Richard M. Flynn
发明人： George G. I. Moore , Michael A. Yandrasits , Jay F. Schulz , Richard M. Flynn
IPC分类号： C08F1418
CPC分类号： C09D133/16 , C07C69/63 , C08F20/24 , C08F120/24
摘要： Described is a compound having at least one acrylate monomer, said monomer including at least one pendant group of the structure —O—CH(Rf)(Rf′), wherein Rf is a straight chain or branched perfluoroalkyl group with five or less carbon atoms, and Rf′ is a branched perfluoroalkyl group with three to five carbon atoms; and a method of reducing the surface tension of a liquid by adding a compound of the invention to the liquid. Also described is a composition that includes a compound of the invention in an aqueous solution or dispersion; a method of treating a substrate to render it oil- and/or water-repellent that includes treating a substrate with a composition of the invention; a method of coating an electrical device that includes applying a composition of the invention; a method of coating optical fibers that includes applying a composition of the invention; and an article that includes a substrate treated with a composition of the invention.
摘要翻译：描述了具有至少一种丙烯酸酯单体的化合物，所述单体包括至少一个-O-CH（Rf）（Rf'）结构的侧基，其中Rf是具有五个或更少碳原子的直链或支链全氟烷基，Rf'为3〜5个碳原子的支链全氟烷基; 以及通过将本发明的化合物加入到液体中来降低液体的表面张力的方法。还描述了在水溶液或分散体中包含本发明化合物的组合物; 处理基材以使其具有油和/或防水性的方法，其包括用本发明的组合物处理基材; 包括施用本发明的组合物的电气装置的涂覆方法; 涂布光纤的方法，其包括施加本发明的组合物; 以及包含用本发明的组合物处理的基材的制品。

4. 发明授权

US08920679B2 Fluorinated silylethynyl pentacene compounds and compositions and methods of making and using the same 有权
标题翻译：氟化甲硅烷基乙炔并五苯化合物及其制备和使用方法
公开(公告)号：US08920679B2
公开(公告)日：2014-12-30
申请号：US13318617
申请日：2010-05-28
申请人： Robert Steven Clough , Richard M. Flynn , George G. I. Moore , John E. Anthony , Marcia M. Payne
发明人： Robert Steven Clough , Richard M. Flynn , George G. I. Moore , John E. Anthony , Marcia M. Payne
IPC分类号： H01B1/00 , H01L29/08 , H01J1/62 , C07F7/08
CPC分类号： C07F7/081
摘要： Fluorinated silylethynyl pentacenes and compositions containing fluorinated silylethynyl pentacenes are disclosed. Methods of making and using fluorinated silylethynyl pentacenes and compositions containing fluorinated silylethynyl pentacenes are also disclosed.
摘要翻译：公开了含氟化的甲硅烷基乙炔戊烯和含有氟化的甲硅烷基乙炔基并五苯的组合物。还公开了制备和使用氟化甲硅烷基乙炔基并五苯的方法和含有氟化的甲硅烷基乙炔戊腈的组合物。

5. 发明授权

US08535559B2 Nitrogen-containing fluoroketones for high temperature heat transfer 有权
标题翻译：含氮氟代酮用于高温传热
公开(公告)号：US08535559B2
公开(公告)日：2013-09-17
申请号：US12732608
申请日：2010-03-26
申请人： Richard M. Flynn , Michael G. Costello , Michael J. Bulinski , Daniel R. Vitcak , Phillip E. Tuma
发明人： Richard M. Flynn , Michael G. Costello , Michael J. Bulinski , Daniel R. Vitcak , Phillip E. Tuma
IPC分类号： C09K5/00
CPC分类号： C07D295/108 , B23K35/0244 , B23K35/3616 , C07C225/06 , C07C229/16 , C07D207/10 , C07D211/38
摘要： Nitrogen-containing fluorochemical ketones are provided that can be useful in apparatuses that includes a device and a mechanism for transferring heat. The provided fluorochemical ketones are stable at temperatures above 170° C., are environmentally friendly, and are economical to produce. The provided apparatuses can be useful for vapor phase soldering of electronic devices.
摘要翻译：提供了含氮含氟酮，其可用于包括装置和用于传递热量的机构的装置中。所提供的氟化学酮在高于170℃的温度下是稳定的，是环境友好的，并且是经济的。所提供的装置可用于电子装置的气相焊接。

6. 发明授权

US08222322B2 Method of making fluoropolymer dispersion 有权
标题翻译：制备含氟聚合物分散体的方法
公开(公告)号：US08222322B2
公开(公告)日：2012-07-17
申请号：US12684239
申请日：2010-01-08
申请人： Klaus Hintzer , Michael Jürgens , Harald Kaspar , Herbert Koenigsmann , Kai Helmut Lochhaas , Andreas R. Maurer , Werner Schwertfeger , Tilman Zipplies , Ludwig Mayer , Michael C Dadalas , George G. I. Moore , Jay F. Schulz , Richard M. Flynn
发明人： Klaus Hintzer , Michael Jürgens , Harald Kaspar , Herbert Koenigsmann , Kai Helmut Lochhaas , Andreas R. Maurer , Werner Schwertfeger , Tilman Zipplies , Ludwig Mayer , Michael C Dadalas , George G. I. Moore , Jay F. Schulz , Richard M. Flynn
IPC分类号： C08L1/00
CPC分类号： C08L27/12 , C08L71/02 , Y02C20/30 , C08L2666/22
摘要： A method of making a fluoropolymer dispersion by first providing a fluoropolymer dispersion comprising fluoropolymer particles and one or more fluorinated surfactants selected from fluorinated carboxylic acids or salts thereof having the general formula: [Rf—O-L-COO−]iXi+ (I) wherein L represents a linear fully fluorinated alkylene group, Rf represents a linear partially or fully fluorinated aliphatic group or a linear partially or fully fluorinated aliphatic group interrupted with one oxygen atom, Xi+ represents a cation having the valence i and i is 1, 2 or 3; then adding one or more non-fluorinated surfactants selected from anionic and non-ionic surfactants followed by reducing the total amount of the one or more fluorinated surfactants to an amount of not more than 500 ppm, for example not more than 250 ppm based on the total weight of the dispersion while maintaining or increasing the amount of solids in the dispersion.
摘要翻译：首先提供含氟聚合物颗粒和一种或多种选自氟化羧酸或其盐的含氟表面活性剂的含氟聚合物分散体的制备方法，所述含氟聚合物分散体具有以下通式：[Rf-OL-COO-] iXi +（I）其中L表示线性全氟化亚烷基，Rf表示直链部分或完全氟化的脂族基团或被一个氧原子间隔的直链部分或全氟化的脂族基团，X i +表示i为i且i为1,2或3的阳离子; 然后加入一种或多种选自阴离子和非离子表面活性剂的非氟化表面活性剂，然后将一种或多种氟化表面活性剂的总量减少至不超过500ppm，例如不超过250ppm，基于分散体的总重量，同时保持或增加分散体中固体的量。

7. 发明授权

US07988877B2 Methods of making fluorinated ethers, fluorinated ethers, and uses thereof 失效
标题翻译：制备氟化醚，氟化醚的方法及其用途
公开(公告)号：US07988877B2
公开(公告)日：2011-08-02
申请号：US12263661
申请日：2008-11-03
申请人： Richard M. Flynn , Michael J. Bulinski , Michael G. Costello
发明人： Richard M. Flynn , Michael J. Bulinski , Michael G. Costello
IPC分类号： A62D1/00 , C07C43/00 , C07C43/12
CPC分类号： C07C41/16 , C07C43/123 , C07C43/126 , C07C213/06 , C07C217/26
摘要： A method of making a fluorinated ether includes combining, in a polar aprotic solvent: a fluorinated alcohol represented by the formula X—Rf1CH2OH, and a fluorinated sulfonate ester represented by the formula Rf2CH2OS(═O)2Rf3, and base; and obtaining a fluorinated ether represented by the formula Y—Rf1CH2OCH2Rf2—Y. Rf1 is selected from perfluorinated C1-C10 alkylene groups having from 1 to 10 carbon atoms and partially fluorinated C1-C10 alkylene groups, and derivatives thereof having catenated heteroatom(s). X represents H, F, or an HOCH2— group. Rf2 is selected from perfluorinated C1-C10 alkyl groups and partially fluorinated C1-C10 alkyl groups, and derivatives thereof having catenated heteroatom(s). Rf3 is a C1-C4 alkyl group. Y represents H, F, or an Rf2CH2OCH2— group. A variant method, useful for preparing symmetric fluorinated ethers, is also disclosed. The present disclosure also provides fluorinated ethers preparable according to the methods. Use of fluorinated ethers in various applications is also disclosed.
摘要翻译：氟化醚的制造方法包括在极性非质子传递溶剂：由式X-Rf 1 CH 2 OH表示的氟化醇和由式Rf2CH2OS（= O）2Rf3表示的氟化磺酸酯）和碱的组合; 得到式Y-Rf 1 CH 2 OCH 2 R f 2 -Y表示的氟代醚。 Rf1选自具有1至10个碳原子的全氟化C 1 -C 10亚烷基和部分氟化的C 1 -C 10亚烷基，及其具有连接的杂原子的衍生物。 X表示H，F或HOCH 2 - 基团。 Rf2选自全氟化的C 1 -C 10烷基和部分氟化的C 1 -C 10烷基，以及其具有连接的杂原子的衍生物。 Rf 3是C 1 -C 4烷基。 Y表示H，F或Rf2CH2OCH2-基团。还公开了可用于制备对称氟化醚的变体方法。本公开还提供了根据该方法可制备的氟化醚。还公开了在各种应用中使用氟化醚。

8. 发明授权

US07754795B2 Coating composition 有权
标题翻译：涂料组成
公开(公告)号：US07754795B2
公开(公告)日：2010-07-13
申请号：US11420431
申请日：2006-05-25
申请人： Klaus Hintzer , Michael Jürgens , Harald Kaspar , Herbert Koenigsmann , Kai Helmut Lochhaas , Andreas R. Maurer , Werner Schwertfeger , Tilman Zipplies , Ludwig Mayer , Michael C. Dadalas , George G. I. Moore , Jay F. Schulz , Richard M. Flynn
发明人： Klaus Hintzer , Michael Jürgens , Harald Kaspar , Herbert Koenigsmann , Kai Helmut Lochhaas , Andreas R. Maurer , Werner Schwertfeger , Tilman Zipplies , Ludwig Mayer , Michael C. Dadalas , George G. I. Moore , Jay F. Schulz , Richard M. Flynn
IPC分类号： C08K5/00
CPC分类号： C09D127/18 , C08K5/06 , C08K5/09 , C08L27/12 , C08L71/02 , C08L2205/02 , C08L2205/03 , C08L2205/035 , C08L2666/02 , C08L2666/14
摘要： A coating composition having (i) an aqueous dispersion of fluoropolymer particles comprising a non-melt processible polymer of tetrafluoroethylene, (ii) a fluorinated surfactant, (iii) a non-ionic non-fluorinated surfactant and (iv) a non-fluorinated polymer, wherein the fluorinated surfactant is selected from fluorinated carboxylic acids or salts thereof of the general formula (I): [Rf—O-L-COO−]iXi+ (I) wherein L represents a linear partially or fully fluorinated alkylene group or an aliphatic hydrocarbon group, Rf represents a linear partially or fully fluorinated aliphatic group or a linear partially or fully fluorinated aliphatic group interrupted with one or more oxygen atoms, Xi+ represents a cation having the valence i and i is 1, 2 or 3.
摘要翻译：一种涂料组合物，其具有（i）含氟聚合物颗粒的水分散体，其包含四氟乙烯的不可熔融加工聚合物，（ii）氟化表面活性剂，（iii）非离子非氟化表面活性剂和（iv）非氟化聚合物其中氟化表面活性剂选自通式（I）的氟化羧酸或其盐：[Rf-OL-COO-] iXi +（I）其中L表示直链部分或完全氟化的亚烷基或脂族烃基 Rf表示直链部分或完全氟化的脂族基团或被一个或多个氧原子间隔的线性部分或全部氟化的脂肪族基团，Xi +表示i为i且i为1,2或3的阳离子。

9. 发明申请

US20100113679A1 METHOD OF MAKING FLUOROPOLYMER DISPERSION 有权
标题翻译：制备氟聚合物分散体的方法
公开(公告)号：US20100113679A1
公开(公告)日：2010-05-06
申请号：US12684239
申请日：2010-01-08
申请人： Klaus Hintzer , Michael Jürgens , Harald Kaspar , Herbert Koenigsmann , Kai Helmut Lochhaas , Andreas R. Maurer , Werner Schwertfeger , Tilman Zipplies , Ludwig Mayer , Michael C. Dadalas , George G.I. Moore , Jay F. Schulz , Richard M. Flynn
发明人： Klaus Hintzer , Michael Jürgens , Harald Kaspar , Herbert Koenigsmann , Kai Helmut Lochhaas , Andreas R. Maurer , Werner Schwertfeger , Tilman Zipplies , Ludwig Mayer , Michael C. Dadalas , George G.I. Moore , Jay F. Schulz , Richard M. Flynn
IPC分类号： C08L27/18
CPC分类号： C08L27/12 , C08L71/02 , Y02C20/30 , C08L2666/22
摘要： A method of making a fluoropolymer dispersion by first providing a fluoropolymer dispersion comprising fluoropolymer particles and one or more fluorinated surfactants selected from fluorinated carboxylic acids or salts thereof having the general formula: [Rf—O-L-COO−]iXi+ (I) wherein L represents a linear fully fluorinated alkylene group, Rf represents a linear partially or fully fluorinated aliphatic group or a linear partially or fully fluorinated aliphatic group interrupted with one oxygen atom, Xi+ represents a cation having the valence i and i is 1, 2 or 3;then adding one or more non-fluorinated surfactants selected from anionic and non-ionic surfactants followed by reducing the total amount of the one or more fluorinated surfactants to an amount of not more than 500 ppm, for example not more than 250 ppm based on the total weight of the dispersion while maintaining or increasing the amount of solids in the dispersion.
摘要翻译：首先提供含氟聚合物颗粒和一种或多种选自氟化羧酸或其盐的含氟表面活性剂的含氟聚合物分散体的制备方法，所述含氟聚合物分散体具有以下通式：[Rf-OL-COO-] iXi +（I）其中L表示线性全氟化亚烷基，Rf表示直链部分或完全氟化的脂族基团或被一个氧原子间隔的直链部分或全氟化的脂族基团，X i +表示i为i且i为1,2或3的阳离子; 然后加入一种或多种选自阴离子和非离子表面活性剂的非氟化表面活性剂，然后将一种或多种氟化表面活性剂的总量减少至不超过500ppm，例如不超过250ppm，基于分散体的总重量，同时保持或增加分散体中固体的量。

10. 发明授权

US07659333B2 Fluorinated surfactants for use in making a fluoropolymer 有权
标题翻译：用于制造含氟聚合物的氟化表面活性剂
公开(公告)号：US07659333B2
公开(公告)日：2010-02-09
申请号：US11562277
申请日：2006-11-21
申请人： Klaus Hintzer , Michael Jürgens , Harald Kaspar , Herbert Königsmann , Kai Helmut Lochhaas , Andreas R. Maurer , Tilman C. Zipplies , Richard M. Flynn
发明人： Klaus Hintzer , Michael Jürgens , Harald Kaspar , Herbert Königsmann , Kai Helmut Lochhaas , Andreas R. Maurer , Tilman C. Zipplies , Richard M. Flynn
IPC分类号： C08K5/41
CPC分类号： C07C51/367 , C07C51/412 , C07C59/315 , C08L27/12 , C08L71/02 , C09D127/12 , C08L2666/22
摘要： The present invention provides a fluorinated surfactant having the general formula: [Rf—(O)t—CQH—CF2—O]n—R—G (I) wherein Rf represents a partially or fully fluorinated aliphatic group optionally interrupted with one or more oxygen atoms, Q is CF3 or F, R is an aliphatic or aromatic hydrocarbon group, G represents a carboxylic or sulphonic acid or salt thereof, t is 0 or 1 and n is 1, 2 or 3. The surfactant is particularly useful in polymerizing fluorinated monomers in an aqueous emulsion polymerization.
摘要翻译：本发明提供具有以下通式的氟化表面活性剂：[Rf-（O）t-CQH-CF2-O] nRG（I）其中Rf表示任选被一个或多个氧原子间隔的部分或完全氟化的脂族基团，Q 是CF 3或F，R是脂族或芳族烃基，G表示羧酸或磺酸或其盐，t为0或1，n为1,2或3.该表面活性剂特别可用于将氟化单体在水乳液聚合。

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