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1. 发明申请

US20140050855A1 PROCESS AND COMPOSITION FOR TREATING METAL SURFACES USING TRIVALENT CHROMIUM COMPOUNDS 有权
标题翻译：使用多种铬化合物处理金属表面的方法和组合物
公开(公告)号：US20140050855A1
公开(公告)日：2014-02-20
申请号：US14058902
申请日：2013-10-21
申请人： Richard J. Church
发明人： Richard J. Church
IPC分类号： C09D5/00 , C09D5/08
CPC分类号： C09D5/002 , C09D5/08 , C09D5/084 , C23C22/34 , C23C22/83 , C23C2222/10 , C23C2222/20
摘要： An acidic, aqueous composition contains a trivalent chromium compound, an organo-functional silane, and a compound of a group IV-B element. The composition protects metal surfaces, preferably aluminum and aluminum alloys, against corrosion and improves their paint adhesion. The trivalent chromium compound may comprise chromium fluoride and optionally others, such as chromium nitrate. The organo-functional silane is preferably an aminopropyltriethoxy silane, and the compound of a group IV-B element is preferably fluorozirconic acid. The composition can either be dried-in-place or rinsed before a further coating layer is applied. The composition may also include at least one polymer having a plurality of both carboxylic functional groups, alone or with hydroxyl groups. A process uses the aqueous composition either with or without the organo-functional silane along with a sealing step following the application of the aqueous composition; the sealing step involves applying a sealing composition, including an organo-functional silane, to the metal surface.
摘要翻译：酸性水性组合物含有三价铬化合物，有机功能性硅烷和IV-B族元素的化合物。该组合物保护金属表面，优选铝和铝合金，防止腐蚀并改善其涂料附着力。三价铬化合物可以包含氟化铬和任选的其它物质，例如硝酸铬。有机官能硅烷优选为氨基丙基三乙氧基硅烷，IV-B族元素的化合物优选为氟锆酸。组合物可以在施加另外的涂层之前进行就地干燥或漂洗。该组合物还可以包括至少一种具有多个单独或与羟基的两个羧基官能团的聚合物。一种方法使用具有或不具有有机官能硅烷的水性组合物以及施加含水组合物之后的密封步骤; 密封步骤包括将包括有机功能性硅烷的密封组合物施加到金属表面。

2. 发明申请

US20090280253A1 PROCESS AND COMPOSITION FOR TREATING METAL SURFACES USING TRIVALENT CHROMIUM COMPOUNDS 有权
标题翻译：使用多种铬化合物处理金属表面的方法和组合物
公开(公告)号：US20090280253A1
公开(公告)日：2009-11-12
申请号：US12116513
申请日：2008-05-07
申请人： Richard J. Church
发明人： Richard J. Church
IPC分类号： C09K13/08 , C23F1/00 , B05D3/10
CPC分类号： C09D5/002 , C09D5/08 , C09D5/084 , C23C22/34 , C23C22/83 , C23C2222/10 , C23C2222/20
摘要： An acidic, aqueous composition contains a trivalent chromium compound, an organo-functional silane, and a compound of a group IV-B element. The composition protects metal surfaces, preferably aluminum and aluminum alloys, against corrosion and improves their paint adhesion. The trivalent chromium compound may comprise chromium fluoride and optionally others, such as chromium nitrate. The organo-functional silane is preferably an aminopropyltriethoxy silane, and the compound of a group IV-B element is preferably fluorozirconic acid. The composition can either be dried-in-place or rinsed before a further coating layer is applied. The composition may also include at least one polymer having a plurality of both carboxylic functional groups, alone or with hydroxyl groups. A process uses the aqueous composition either with or without the organo-functional silane along with a sealing step following the application of the aqueous composition; the sealing step involves applying a sealing composition, including an organo-functional silane, to the metal surface.
摘要翻译：酸性水性组合物含有三价铬化合物，有机功能性硅烷和IV-B族元素的化合物。该组合物保护金属表面，优选铝和铝合金，防止腐蚀并改善其涂料附着力。三价铬化合物可以包含氟化铬和任选的其它物质，例如硝酸铬。有机官能硅烷优选为氨基丙基三乙氧基硅烷，IV-B族元素的化合物优选为氟锆酸。组合物可以在施加另外的涂层之前进行就地干燥或漂洗。该组合物还可以包括至少一种具有多个单独或与羟基的两个羧基官能团的聚合物。一种方法使用具有或不具有有机官能硅烷的水性组合物以及施加含水组合物之后的密封步骤; 密封步骤包括将包括有机功能性硅烷的密封组合物施加到金属表面。

3. 发明授权

US08591670B2 Process and composition for treating metal surfaces using trivalent chromium compounds 有权
标题翻译：使用三价铬化合物处理金属表面的方法和组成
公开(公告)号：US08591670B2
公开(公告)日：2013-11-26
申请号：US12116513
申请日：2008-05-07
申请人： Richard J. Church
发明人： Richard J. Church
IPC分类号： C23C22/30 , C23C22/34 , C23C22/00
CPC分类号： C09D5/002 , C09D5/08 , C09D5/084 , C23C22/34 , C23C22/83 , C23C2222/10 , C23C2222/20
摘要： An acidic, aqueous composition contains a trivalent chromium compound, an organo-functional silane, and a compound of a group IV-B element. The composition protects metal surfaces, preferably aluminum and aluminum alloys, against corrosion and improves their paint adhesion. The trivalent chromium compound may comprise chromium fluoride and optionally others, such as chromium nitrate. The organo-functional silane is preferably an aminopropyltriethoxy silane, and the compound of a group IV-B element is preferably fluorozirconic acid. The composition can either be dried-in-place or rinsed before a further coating layer is applied. The composition may also include at least one polymer having a plurality of both carboxylic functional groups, alone or with hydroxyl groups. A process uses the aqueous composition either with or without the organo-functional silane along with a sealing step following the application of the aqueous composition; the sealing step involves applying a sealing composition, including an organo-functional silane, to the metal surface.
摘要翻译：酸性水性组合物含有三价铬化合物，有机功能性硅烷和IV-B族元素的化合物。该组合物保护金属表面，优选铝和铝合金，防止腐蚀并改善其涂料附着力。三价铬化合物可以包含氟化铬和任选的其它物质，例如硝酸铬。有机官能硅烷优选为氨基丙基三乙氧基硅烷，IV-B族元素的化合物优选为氟锆酸。组合物可以在施加另外的涂层之前进行就地干燥或漂洗。该组合物还可以包括至少一种具有多个单独或与羟基的两个羧基官能团的聚合物。一种方法使用具有或不具有有机官能硅烷的水性组合物以及施加含水组合物之后的密封步骤; 密封步骤包括将包括有机功能性硅烷的密封组合物施加到金属表面。

4. 发明授权

US07479177B2 Coating for cold working metals 失效
标题翻译：冷加工金属涂层
公开(公告)号：US07479177B2
公开(公告)日：2009-01-20
申请号：US10789225
申请日：2004-02-27
申请人： Richard J. Church
发明人： Richard J. Church
IPC分类号： C22C22/07 , C22C22/17 , C10M157/08
CPC分类号： C23C22/10 , C10M125/10 , C10M125/22 , C10M125/24 , C10M125/26 , C10M129/40 , C10M133/44 , C10M135/10 , C10M135/28 , C10M135/32 , C10M135/34 , C10M145/36 , C10M173/02 , C10M2201/02 , C10M2201/041 , C10M2201/042 , C10M2201/062 , C10M2201/065 , C10M2201/066 , C10M2201/08 , C10M2201/081 , C10M2201/082 , C10M2201/084 , C10M2201/085 , C10M2201/087 , C10M2201/10 , C10M2201/102 , C10M2201/105 , C10M2207/046 , C10M2207/125 , C10M2207/126 , C10M2207/129 , C10M2207/40 , C10M2207/404 , C10M2209/103 , C10M2209/104 , C10M2209/108 , C10M2215/22 , C10M2215/221 , C10M2215/223 , C10M2215/225 , C10M2215/226 , C10M2215/30 , C10M2219/044 , C10M2219/086 , C10M2219/09 , C10M2219/10 , C10M2219/102 , C10M2219/104 , C10M2219/106 , C10N2210/01 , C10N2210/02 , C10N2220/02 , C10N2240/402 , C10N2240/403 , C10N2240/404 , C10N2240/405 , C10N2240/406 , C10N2240/407 , C10N2240/408 , C10N2240/409 , C10N2250/02 , C10N2250/10 , C10N2250/121 , C10N2270/00 , C10N2270/02 , C23C22/08
摘要： The invention involves a composition for forming a combined conversion and lubricating coating on a metal substrate with which the composition is brought into contact. The composition comprises (a) an oxyethylated aliphatic alcohol whose aliphatic hydrocarbon moiety contains 18 or more carbon atoms and (b) dissolved phosphate anions. Preferably the composition also comprises inorganic boron, an alkali metal salt of a fatty acid, and an accelerator for phosphate coating.
摘要翻译：本发明涉及一种用于在金属基底上形成组合的转化和润滑涂层的组合物，与组合物接触。组合物包含（a）脂族烃部分含有18个或更多个碳原子的氧乙基化脂族醇和（b）溶解的磷酸根阴离子。优选地，组合物还包含无机硼，脂肪酸的碱金属盐和磷酸盐涂层的促进剂。

5. 发明授权

US06727214B1 Cleaning metal salts of intermediate length carboxylic acids from surfaces 失效
标题翻译：从表面清除中等长度羧酸的金属盐
公开(公告)号：US06727214B1
公开(公告)日：2004-04-27
申请号：US10110493
申请日：2002-04-15
申请人： Richard J. Church , Paul A. Kulongowski
发明人： Richard J. Church , Paul A. Kulongowski
IPC分类号： C11D304
CPC分类号： C11D3/044 , C11D3/2075
摘要： A process of cleaning very sparingly water soluble soaps off workpieces after cold forming them is made considerably more economical by using a cleaning solution that causes the removed soap anions to form a separate floating solid phase that can easily be skimmed from the surface of the cleaning solution. When such a separation is made, much longer intervals between replacement of the cleaning solution are possible while still obtaining satisfactory results. A preferred cleaning solution for such a process comprises hydroxides, neutral salts, polymeric quaternary ammonium cations, and a sequestering agent for the counterions of the soap anions to be cleaned.
摘要翻译：通过使用清洁溶液使清除的皂阴离子形成分离的漂浮固相，其可以很容易地从清洁溶液的表面上撇去，在冷成型之后将非常微小的水溶性肥皂清除掉的工艺变得更加经济。当进行这种分离时，更换清洁溶液之间的更长的间隔是可能的，同时仍然获得令人满意的结果。用于这种方法的优选的清洁溶液包括氢氧化物，中性盐，聚合季铵阳离子和用于待洗涤的皂阴离子的抗衡离子的螯合剂。

6. 发明授权

US06248701B1 Aqueous metal coating composition and process with reduced staining and corrosion 失效
标题翻译：水性金属涂料组合物和工艺具有减少的染色和腐蚀
公开(公告)号：US06248701B1
公开(公告)日：2001-06-19
申请号：US08652141
申请日：1996-05-23
申请人： Richard J. Church
发明人： Richard J. Church
IPC分类号： C10M17300
CPC分类号： C23F11/10 , B21B45/0263 , C09D5/08 , C10M125/02 , C10M125/10 , C10M125/22 , C10M125/26 , C10M133/44 , C10M135/32 , C10M135/36 , C10M137/04 , C10M145/14 , C10M145/16 , C10M145/36 , C10M153/04 , C10M173/02 , C10M2201/041 , C10M2201/042 , C10M2201/05 , C10M2201/062 , C10M2201/065 , C10M2201/066 , C10M2201/084 , C10M2201/087 , C10M2201/10 , C10M2201/102 , C10M2201/105 , C10M2203/00 , C10M2205/00 , C10M2205/022 , C10M2205/024 , C10M2205/14 , C10M2207/125 , C10M2207/129 , C10M2207/281 , C10M2207/282 , C10M2207/283 , C10M2207/286 , C10M2207/40 , C10M2207/404 , C10M2209/084 , C10M2209/086 , C10M2209/104 , C10M2209/108 , C10M2215/22 , C10M2215/221 , C10M2215/223 , C10M2215/225 , C10M2215/226 , C10M2215/30 , C10M2219/09 , C10M2219/10 , C10M2219/102 , C10M2219/104 , C10M2219/106 , C10M2219/108 , C10M2223/04 , C10M2223/041 , C10M2223/042 , C10M2225/00 , C10M2225/02 , C10M2225/04 , C10M2225/041 , C10N2220/02 , C10N2250/02 , C10N2270/02
摘要： A combination of sulfur-free azoles, preferably benzotriazole and tolyltriazole, with sulfur-containing azoles, preferably 2-mercaptobenzothiazole or mercaptobenzimidazole, prevents discoloration, staining, or corrosion of metal surfaces being coated with an organic protective coating from aqueous dispersion or solution.
摘要翻译：无硫唑类，优选苯并三唑和甲苯基三唑与含硫唑类，优选2-巯基苯并噻唑或巯基苯并咪唑的组合防止由水性分散体或溶液涂覆有机保护涂层的金属表面的变色，污染或腐蚀。

7. 发明授权

US5531912A Composition and process for lubricating metal before cold forming 失效
标题翻译：冷成型前润滑金属的组成和工艺
公开(公告)号：US5531912A
公开(公告)日：1996-07-02
申请号：US300665
申请日：1994-09-02
申请人： Richard J. Church , Kenneth J. Hacias
发明人： Richard J. Church , Kenneth J. Hacias
IPC分类号： C10M107/02 , C10M107/06 , C10M107/08 , C10M107/28 , C10M111/04 , C10M125/26 , C10M169/04 , C10M173/02 , C10N30/00 , C10N30/04 , C10N30/06 , C10N30/12 , C10N40/24 , C10N50/08 , C10N80/00 , C10M173/00
CPC分类号： C10M169/044 , C10M173/02 , C10M2201/02 , C10M2201/087 , C10M2201/10 , C10M2201/102 , C10M2201/105 , C10M2209/08 , C10M2209/084 , C10M2209/0845 , C10M2209/0863 , C10M2209/1013 , C10M2209/1023 , C10M2209/104 , C10M2215/22 , C10M2215/221 , C10M2215/223 , C10M2215/225 , C10M2215/226 , C10M2215/30 , C10M2219/09 , C10M2219/10 , C10M2219/102 , C10M2219/104 , C10M2219/106 , C10M2219/108 , C10M2223/04 , C10M2223/041 , C10M2223/042 , C10N2240/402 , C10N2240/403 , C10N2240/404 , C10N2240/405 , C10N2240/406 , C10N2240/407 , C10N2240/408 , C10N2240/409 , C10N2250/02 , C10N2250/121 , C10N2270/00
摘要： A stearate free solid lubricant for cold working of metals contains approximately equal amounts of an alkene-acrylate ionomer and an alkoxylated alcohol in which the alcohol moiety has from 18-60 carbon atoms and the alkoxylate block has about the same number of carbon atoms. This lubricant can be conveniently applied from aqueous solution/suspension and works effectively even when the underlying steel surface has no conversion coating, which is usually required with stearate lubricants for best results.
摘要翻译：用于金属冷加工的不含硬脂酸盐的固体润滑剂含有大致相等量的烯烃 - 丙烯酸酯离聚物和烷氧基化醇，其中醇部分具有18-60个碳原子，烷氧基化物嵌段具有大约相同数目的碳原子。这种润滑剂可以方便地从水溶液/悬浮液中施加，并且即使当下面的钢表面没有转化涂层时也是有效的，通常用硬脂酸酯润滑剂需要转化涂层以获得最佳结果。

8. 发明授权

US08425692B2 Process and composition for treating metal surfaces 有权
标题翻译：处理金属表面的方法和组成
公开(公告)号：US08425692B2
公开(公告)日：2013-04-23
申请号：US12789108
申请日：2010-05-27
申请人： José B. Rivera , Richard J. Church
发明人： José B. Rivera , Richard J. Church
IPC分类号： C23C22/34 , C23C22/30
CPC分类号： C09D5/084 , C23C22/34 , C23C2222/10 , C23C2222/20
摘要： A composition for forming a protective coating on a metal surface includes water; Cr2(GF6)3 in which G is a Group IV-B element; and at least one polymer having a plurality of carboxylic acid groups and at least one polymer having a plurality of hydroxyl groups, and/or at least one polymer having a plurality of both carboxylic acid and hydroxyl groups; wherein the composition contains less than 500 ppm of alkali metal ions and less than 200 ppm of halide ions relative to chromium. A method of forming a protective coating on a metal surface includes contacting the metal surface with the composition.
摘要翻译：用于在金属表面形成保护涂层的组合物包括水; Cr 2（GF 6）3，其中G为IV-B族元素; 和至少一种具有多个羧酸基团的聚合物和至少一种具有多个羟基的聚合物，和/或至少一种具有多个羧酸和羟基的聚合物; 其中所述组合物相对于铬含有小于500ppm的碱金属离子和小于200ppm的卤离子。在金属表面上形成保护涂层的方法包括使金属表面与组合物接触。

9. 发明申请

US20110293841A1 PROCESS AND COMPOSITION FOR TREATING METAL SURFACES 有权
标题翻译：用于处理金属表面的方法和组合物
公开(公告)号：US20110293841A1
公开(公告)日：2011-12-01
申请号：US12789108
申请日：2010-05-27
申请人： José B. Rivera , Richard J. Church
发明人： José B. Rivera , Richard J. Church
IPC分类号： B05D3/02 , C09D1/00
CPC分类号： C09D5/084 , C23C22/34 , C23C2222/10 , C23C2222/20
摘要： A composition for forming a protective coating on a metal surface includes water;Cr2(GF6)3 in which G is a Group IV-B element; andat least one polymer having a plurality of carboxylic acid groups and at least one polymer having a plurality of hydroxyl groups, and/or at least one polymer having a plurality of both carboxylic acid and hydroxyl groups;wherein the composition contains less than 500 ppm of alkali metal ions and less than 200 ppm of halide ions relative to chromium. A method of forming a protective coating on a metal surface includes contacting the metal surface with the composition.
摘要翻译：用于在金属表面形成保护涂层的组合物包括水; Cr 2（GF 6）3，其中G为IV-B族元素; 和至少一种具有多个羧酸基团的聚合物和至少一种具有多个羟基的聚合物，和/或至少一种具有多个羧酸和羟基的聚合物; 其中所述组合物相对于铬含有小于500ppm的碱金属离子和小于200ppm的卤离子。在金属表面上形成保护涂层的方法包括使金属表面与组合物接触。

10. 发明授权

US06440917B1 Cleaning metal salts of intermediate length carboxylic acids from surfaces 失效
标题翻译：从表面清除中等长度羧酸的金属盐
公开(公告)号：US06440917B1
公开(公告)日：2002-08-27
申请号：US09530300
申请日：2000-04-27
申请人： Richard J. Church , Kenneth J. Hacias
发明人： Richard J. Church , Kenneth J. Hacias
IPC分类号： C11D304
CPC分类号： C11D3/044 , C11D1/72 , C11D3/2086 , C11D7/06 , C11D7/265 , C11D11/0029
摘要： Problems of extensive foaming and/or of sticky deposits on process equipment that often arise when metal soaps from metal articles that have been given a metal soap containing surface to aid in drawing are removed with aqueous alkaline clearners can be avoided by including in the cleaners used anions such as calcium and magnesium that are capable of precipitating the anions of the metal soaps. The cleaners advantageously also contain chelants, a mixture of nonionic and anionic surfactants, and phosphorus containing anions. Anions from the metal soaps are eventually precipitated from the cleaners used as non-sticky sludge that can be easily separated from the cleaners.
摘要翻译：通过在使用的清洁剂中包括在水性碱性清洁剂中除去已经被赋予含金属肥皂表面以辅助拉伸的金属制品的金属皂，通常在工艺设备上产生大量起泡和/或粘性沉积物的问题，阴离子如钙和镁，能够沉淀金属皂的阴离子。清洁剂有利地还含有螯合剂，非离子和阴离子表面活性剂的混合物以及含磷阴离子。来自金属皂的阴离子最终从用作非粘性污泥的清洁剂沉淀出来，其可以容易地与清洁剂分离。

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