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1. 发明申请

US20100029160A1 FORMALDEHYDE FREE BINDER 有权
公开(公告)号：US20100029160A1
公开(公告)日：2010-02-04
申请号：US12534319
申请日：2009-08-03
申请人： Ramji Srinivasan , Kurt D. Gabrielson , John B. Hines , Cornel Hagiopol
发明人： Ramji Srinivasan , Kurt D. Gabrielson , John B. Hines , Cornel Hagiopol
IPC分类号： D04H13/00 , C08G63/00 , B32B37/12
CPC分类号： C03C25/26 , C08F8/12 , C08F8/14 , C08F8/44 , C08F2810/20 , C08F2810/50 , C08J5/18 , C08K5/053 , C08K5/1545 , C08K5/17 , C08L2201/54 , C08L2203/12 , C08L2312/00 , C08L2666/34 , C09D125/08 , C09D135/06 , D04H1/4218 , D04H1/587 , D04H1/64 , D04H1/641 , D04H13/008 , D06M15/233 , D06M15/285 , H05K1/0366 , Y10T442/60 , C08L35/06 , C08F212/08 , C08F222/06 , C08F222/08 , C08F8/32
摘要： An aqueous binder composition, useful for making fiber products, especially fiberglass insulation, comprising an aqueous substantially alkaline (pH of at least 5.0) solution of a polyol and a hydrolyzed (solubilized) copolymer of maleic anhydride and a vinyl aromatic compound, preferably styrene (i.e., a SMA copolymer); the copolymer is solubilized using ammonia, an ammine, a primary alkanolamines (preferably monoethanolamine), a secondary alkanolamine (preferably diethanolamine (DEA)), a tertiary alkanolamine (preferably triethanolamine (TEA)), or a mixture thereof and the binder composition is cured as a consequence of cross-linking, esterification reactions between pendant carboxyls on the solubilized (hydrolyzed) copolymer (SMA) chains and hydroxyl groups of the polyol, including the diethanolamine and/or triethanolamine preferably used in the solubilization of the SMA.
摘要翻译：用于制备纤维产品，特别是玻璃纤维绝缘物的水性粘合剂组合物，其包含多元醇和马来酸酐和乙烯基芳族化合物的水解（增溶）共聚物的水性基本上碱性（pH至少为5.0）的水溶液，优选苯乙烯（即SMA共聚物）; 使用氨，氨，主链烷醇胺（优选单乙醇胺），仲链烷醇胺（优选二乙醇胺（DEA）），叔链烷醇胺（优选三乙醇胺（TEA））或其混合物溶解共聚物，并将粘合剂组合物固化作为交联的结果，溶解的（水解的）共聚物（SMA）链上的侧羧基与多元醇的羟基（包括优选用于溶解SMA的二乙醇胺和/或三乙醇胺）的羟基之间的酯化反应。

2. 发明授权

US09169157B2 Formaldehyde free binder 有权
标题翻译：无甲醛粘合剂
公开(公告)号：US09169157B2
公开(公告)日：2015-10-27
申请号：US12534319
申请日：2009-08-03
申请人： Ramji Srinivasan , Kurt D. Gabrielson , John B. Hines , Cornel Hagiopol
发明人： Ramji Srinivasan , Kurt D. Gabrielson , John B. Hines , Cornel Hagiopol
IPC分类号： C08F222/08 , C03C25/26 , C08K5/053 , C08K5/1545 , C08K5/17 , C09D125/08 , C09D135/06 , D04H1/64 , D04H13/00 , D06M15/233 , D06M15/285 , C08J5/18 , C08F8/12 , C08F8/14 , H05K1/03
CPC分类号： C03C25/26 , C08F8/12 , C08F8/14 , C08F8/44 , C08F2810/20 , C08F2810/50 , C08J5/18 , C08K5/053 , C08K5/1545 , C08K5/17 , C08L2201/54 , C08L2203/12 , C08L2312/00 , C08L2666/34 , C09D125/08 , C09D135/06 , D04H1/4218 , D04H1/587 , D04H1/64 , D04H1/641 , D04H13/008 , D06M15/233 , D06M15/285 , H05K1/0366 , Y10T442/60 , C08L35/06 , C08F212/08 , C08F222/06 , C08F222/08 , C08F8/32
摘要： An aqueous binder composition, useful for making fiber products, especially fiberglass insulation, comprising an aqueous substantially alkaline (pH of at least 5.0) solution of a polyol and a hydrolyzed (solubilized) copolymer of maleic anhydride and a vinyl aromatic compound, preferably styrene (i.e., a SMA copolymer); the copolymer is solubilized using ammonia, an ammine, a primary alkanolamines (preferably monoethanolamine), a secondary alkanolamine (preferably diethanolamine (DEA)), a tertiary alkanolamine (preferably triethanolamine (TEA)), or a mixture thereof and the binder composition is cured as a consequence of cross-linking, esterification reactions between pendant carboxyls on the solubilized (hydrolyzed) copolymer (SMA) chains and hydroxyl groups of the polyol, including the diethanolamine and/or triethanolamine preferably used in the solubilization of the SMA.
摘要翻译：用于制备纤维产品，特别是玻璃纤维绝缘物的水性粘合剂组合物，其包含多元醇和马来酸酐和乙烯基芳族化合物的水解（增溶）共聚物的水性基本上碱性（pH至少为5.0）的水溶液，优选苯乙烯（即SMA共聚物）; 使用氨，氨，主链烷醇胺（优选单乙醇胺），仲链烷醇胺（优选二乙醇胺（DEA）），叔链烷醇胺（优选三乙醇胺（TEA））或其混合物溶解共聚物，并将粘合剂组合物固化作为交联的结果，溶解的（水解的）共聚物（SMA）链上的侧羧基与多元醇的羟基（包括优选用于溶解SMA的二乙醇胺和/或三乙醇胺）的羟基之间的酯化反应。

3. 发明授权

US07795354B2 Formaldehyde free binder 有权
标题翻译：无甲醛粘合剂
公开(公告)号：US07795354B2
公开(公告)日：2010-09-14
申请号：US11454327
申请日：2006-06-16
申请人： Ramji Srinivasan , Kurt Gabrielson , John B. Hines , Cornel Hagiopol
发明人： Ramji Srinivasan , Kurt Gabrielson , John B. Hines , Cornel Hagiopol
IPC分类号： C08F8/32 , C08F20/08
CPC分类号： C03C25/1095 , C08K5/053 , C08K5/17 , C08L35/06 , D04H1/587 , D04H1/64 , D06M15/233 , D06M15/263 , C08L2666/02
摘要： An aqueous binder composition, useful for making fiber products, especially fiberglass insulation, comprising an aqueous substantially alkaline (pH of at least 5.0) solution of a polyol and a hydrolyzed (solubilized) copolymer of maleic anhydride and a vinyl aromatic compound, preferably styrene (i.e., a SMA copolymer); the copolymer is solubilized using ammonia, a secondary alkanolamine (preferably diethanolamine (DEA)), a tertiary alkanolamine (preferably triethanolamine (TEA)), or a mixture thereof and the binder composition is cured as a consequence of cross-linking, esterification reactions between pendant carboxyls on the solubilized (hydrolyzed) copolymer (SMA) chains and hydroxyl groups of the polyol, including the diethanolamine and/or triethanolamine preferably used in the solubilization of the SMA.
摘要翻译：用于制备纤维产品，特别是玻璃纤维绝缘物的水性粘合剂组合物，其包含多元醇和马来酸酐和乙烯基芳族化合物的水解（增溶）共聚物的水性基本上碱性（pH至少为5.0）的水溶液，优选苯乙烯（即SMA共聚物）; 使用氨，仲链烷醇胺（优选二乙醇胺（DEA）），叔链烷醇胺（优选三乙醇胺（TEA））或其混合物来溶解共聚物，并且粘合剂组合物由于交联而固化，共聚物（SMA）链上的羧基和多元醇的羟基上的羧基，包括二乙醇胺和/或三乙醇胺，优选用于溶解SMA。

4. 发明申请

US20070292619A1 Formaldehyde free binder 有权
标题翻译：无甲醛粘合剂
公开(公告)号：US20070292619A1
公开(公告)日：2007-12-20
申请号：US11454327
申请日：2006-06-16
申请人： Ramji Srinivasan , Kurt Gabrielson , John B. Hines , Cornel Hagiopol
发明人： Ramji Srinivasan , Kurt Gabrielson , John B. Hines , Cornel Hagiopol
IPC分类号： B05D3/02
CPC分类号： C03C25/1095 , C08K5/053 , C08K5/17 , C08L35/06 , D04H1/587 , D04H1/64 , D06M15/233 , D06M15/263 , C08L2666/02
摘要： An aqueous binder composition, useful for making fiber products, especially fiberglass insulation, comprising an aqueous substantially alkaline (pH of at least 5.0) solution of a polyol and a hydrolyzed (solubilized) copolymer of maleic anhydride and a vinyl aromatic compound, preferably styrene (i.e., a SMA copolymer); the copolymer is solubilized using ammonia, a secondary alkanolamine (preferably diethanolamine (DEA)), a tertiary alkanolamine (preferably triethanolamine (TEA)), or a mixture thereof and the binder composition is cured as a consequence of cross-linking, esterification reactions between pendant carboxyls on the solubilized (hydrolyzed) copolymer (SMA) chains and hydroxyl groups of the polyol, including the diethanolamine and/or triethanolamine preferably used in the solubilization of the SMA.
摘要翻译：用于制备纤维产品，特别是玻璃纤维绝缘物的水性粘合剂组合物，其包含多元醇和马来酸酐和乙烯基芳族化合物的水解（增溶）共聚物的水性基本上碱性（pH至少为5.0）的水溶液，优选苯乙烯（即SMA共聚物）; 使用氨，仲链烷醇胺（优选二乙醇胺（DEA）），叔链烷醇胺（优选三乙醇胺（TEA））或其混合物来溶解共聚物，并且粘合剂组合物由于交联而固化，共聚物（SMA）链上的羧基和多元醇的羟基上的羧基，包括二乙醇胺和/或三乙醇胺，优选用于溶解SMA。

5. 发明授权

US07803879B2 Formaldehyde free binder 有权
标题翻译：无甲醛粘合剂
公开(公告)号：US07803879B2
公开(公告)日：2010-09-28
申请号：US11454326
申请日：2006-06-16
申请人： Ramji Srinivasan , Kurt Gabrielson , John B. Hines , Cornel Hagiopol
发明人： Ramji Srinivasan , Kurt Gabrielson , John B. Hines , Cornel Hagiopol
IPC分类号： C08F8/32 , C08F20/08
CPC分类号： C03C25/26 , C03C25/28 , C08F8/14 , C08F8/32 , C08F8/44 , C08F8/48 , C08K5/17 , C08L2312/00 , C09D125/08 , C09D135/06 , D04H1/587 , D04H1/64 , H05K1/0366 , C08L25/08 , C08F222/08 , C08F212/08 , C08F222/06
摘要： An aqueous, formaldehyde-free binder composition comprising a modified copolymer of maleic anhydride and a vinyl aromatic compound such as styrene, the copolymer being modified by reaction with a primary alkanolamine, such as monoethanolamine (MEA), to produce a modified copolymer that is self-curing and cures as a consequence of cross-linking, esterification reactions between pendant carboxyls and hydroxyl groups on the solubilized (hydrolyzed) modified copolymer chains; the invention also relates to the corresponding method of using the binder composition for making fiber products, especially fiberglass insulation.
摘要翻译：含有不含甲醛的粘合剂组合物，其包含马来酸酐和乙烯基芳族化合物如苯乙烯的改性共聚物，所述共聚物通过与主链烷醇胺如单乙醇胺（MEA）的反应进行改性，以产生自身的改性共聚物由于交联，溶解（水解）改性共聚物链上的侧羧基和羟基之间的酯化反应，固化和固化; 本发明还涉及使用粘合剂组合物制造纤维制品，特别是玻璃纤维绝缘体的相应方法。

6. 发明申请

US20070292618A1 Formaldehyde free binder 有权
标题翻译：无甲醛粘合剂
公开(公告)号：US20070292618A1
公开(公告)日：2007-12-20
申请号：US11454326
申请日：2006-06-16
申请人： Ramji Srinivasan , Kurt Gabrielson , John B. Hines , Cornel Hagiopol
发明人： Ramji Srinivasan , Kurt Gabrielson , John B. Hines , Cornel Hagiopol
IPC分类号： B05D3/02
CPC分类号： C03C25/26 , C03C25/28 , C08F8/14 , C08F8/32 , C08F8/44 , C08F8/48 , C08K5/17 , C08L2312/00 , C09D125/08 , C09D135/06 , D04H1/587 , D04H1/64 , H05K1/0366 , C08L25/08 , C08F222/08 , C08F212/08 , C08F222/06
摘要： An aqueous, formaldehyde-free binder composition comprising a modified copolymer of maleic anhydride and a vinyl aromatic compound such as styrene, the copolymer being modified by reaction with a primary alkanolamine, such as monoethanolamine (MEA), to produce a modified copolymer that is self-curing and cures as a consequence of cross-linking, esterification reactions between pendant carboxyls and hydroxyl groups on the solubilized (hydrolyzed) modified copolymer chains; the invention also relates to the corresponding method of using the binder composition for making fiber products, especially fiberglass insulation.
摘要翻译：含有不含甲醛的粘合剂组合物，其包含马来酸酐和乙烯基芳族化合物如苯乙烯的改性共聚物，所述共聚物通过与主链烷醇胺如单乙醇胺（MEA）的反应进行改性，以产生自身的改性共聚物由于交联，溶解（水解）改性共聚物链上的侧羧基和羟基之间的酯化反应，固化和固化; 本发明还涉及使用粘合剂组合物制造纤维制品，特别是玻璃纤维绝缘体的相应方法。

7. 发明申请

US20050059770A1 Formaldehyde free insulation binder 审中-公开
标题翻译：无甲醛绝缘胶粘剂
公开(公告)号：US20050059770A1
公开(公告)日：2005-03-17
申请号：US10661768
申请日：2003-09-15
申请人： Ramji Srinivasan , Cornel Hagiopol , Natasha Bailey
发明人： Ramji Srinivasan , Cornel Hagiopol , Natasha Bailey
IPC分类号： C03C25/26 , C08F220/04 , C08F220/28 , D04H1/64 , C08F118/02 , C08K3/40 , E04B1/74
CPC分类号： C08F220/04 , C03C25/26 , C08F220/28 , D04H1/587 , D04H1/64
摘要： An aqueous binder composition containing a water-soluble and substantially infinitely water-dilutable free radical polymerized adduct of a monomeric carboxylic acid component and a monomeric hydroxyl component, polymerized in the presence of a chain transfer agent, and the related method of its use for making glass fiber products, especially fiberglass insulation.
摘要翻译：一种水性粘合剂组合物，其含有在链转移剂存在下聚合的单体羧酸组分和单体羟基组分的水溶性且基本上无限水可稀释自由基聚合的加合物及其制备方法玻璃纤维制品，特别是玻璃纤维绝缘。

8. 发明授权

US08785593B2 Polyamidoamine-epihalohydrin resins, method of manufacture, and uses thereof 有权
标题翻译：聚酰胺胺 - 表卤代醇树脂，其制造方法及其用途
公开(公告)号：US08785593B2
公开(公告)日：2014-07-22
申请号：US13448982
申请日：2012-04-17
申请人： Karla D. Favors , Clay E. Ringold , Yuping Luo , Cornel Hagiopol
发明人： Karla D. Favors , Clay E. Ringold , Yuping Luo , Cornel Hagiopol
IPC分类号： C08F6/00 , C08G73/02
CPC分类号： C08G73/0286
摘要： A novel process for producing a polyamidoamine-epihalohydrin resin composition comprises (a) reacting a polyamidoamine with epihalohydrin to obtain a reaction mixture comprising a polyamidoamine-epihalohydrin resin; (b) adding a first acid to the reaction mixture obtained in step (a) to obtain an acid treatment composition; (c) adding a base to the acid treatment composition in step (b) to obtain a base treatment composition; and (d) adding a second acid to the base treatment composition in step (c) to obtain a polyamidoamine-epihalohydrin resin composition; wherein the polyamidoamine-epihalohydrin resin composition obtained in step (d) has less than about 700 ppm of dihalopropanol (DHP) and 3-halopropanediol (HPD).
摘要翻译：制备聚酰胺胺 - 表卤代醇树脂组合物的新方法包括（a）使聚酰胺胺与表卤代醇反应，得到包含聚酰胺胺 - 表卤醇树脂的反应混合物; （b）向步骤（a）获得的反应混合物中加入第一种酸，得到酸处理组合物; （c）在步骤（b）中向酸处理组合物中加入碱以得到碱处理组合物; 和（d）在步骤（c）中向基础处理组合物中加入第二种酸以获得聚酰胺胺 - 表卤代醇树脂组合物; 其中在步骤（d）中获得的聚酰胺胺 - 表卤代醇树脂组合物具有小于约700ppm的二卤丙醇（DHP）和3-卤代丙二醇（HPD）。

9. 发明授权

US07868071B2 Method of stabilizing aqueous cationic polymers 有权
标题翻译：稳定水性阳离子聚合物的方法
公开(公告)号：US07868071B2
公开(公告)日：2011-01-11
申请号：US11830426
申请日：2007-07-30
申请人： Yuping Luo , Clay E. Ringold , Dexter C. Johnson , Cornel Hagiopol
发明人： Yuping Luo , Clay E. Ringold , Dexter C. Johnson , Cornel Hagiopol
IPC分类号： C08G18/28 , C08K5/00 , C08K5/15 , C08K5/16 , A61K9/16 , C08L5/00 , C08L29/04 , D21H21/14 , C08F2/24
CPC分类号： D21H17/55 , C08K5/0091 , C08L79/02
摘要： Cationic thermosetting resins and especially resins having azetidinium functional groups, such as polyamidoamine-epichlorohydrin resins, are stabilized against premature gelation by the addition of (1) a low molecular weight, non-aldehyde, non-ionic, water soluble organic stabilizing compound (preferably one that is reactive with the cationic moiety), preferably in combination with (2) a water soluble, inorganic complexing metal salt.
摘要翻译：阳离子热固性树脂，尤其是具有氮杂环丁烷基官能团的树脂，如聚酰胺胺 - 表氯醇树脂，通过加入（1）低分子量非醛非离子水溶性有机稳定化合物（优选优选与（2）水溶性无机配位金属盐组合使用。

10. 发明申请

US20080214738A1 BLENDS OF ANIONIC COPOLYMERS SUITABLE FOR SURFACE SIZE AND METHODS OF MAKING THE SAME 有权
标题翻译：适用于表面尺寸的阴离子共聚物的混合物及其制备方法
公开(公告)号：US20080214738A1
公开(公告)日：2008-09-04
申请号：US12038250
申请日：2008-02-27
申请人： Cornel Hagiopol , James W. Johnston , Sean M. Tyler , Michael J. Bush
发明人： Cornel Hagiopol , James W. Johnston , Sean M. Tyler , Michael J. Bush
IPC分类号： C08L23/08 , C08L33/02
CPC分类号： C08L31/00 , C08L23/0869 , C08L35/06 , C08L2666/06
摘要： A sizing composition comprises a blend of at least two anionic copolymers.
摘要翻译：定型组合物包含至少两种阴离子共聚物的共混物。

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