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1. 发明申请

US20130230476A1 Fragrance Compositions Comprising Special Mixtures of Diastereomers of 2-Isobutyl-4-Methyl-Tetrahydro-2H-Pyran-4-OL 审中-公开
标题翻译：包含2-异丁基-4-甲基 - 四氢-2H-吡喃-4-醇的非对映异构体的特殊混合物的香料组合物
公开(公告)号：US20130230476A1
公开(公告)日：2013-09-05
申请号：US13884503
申请日：2011-11-08
申请人： Ralf Pelzer , Wolfgang Krause , Karl Beck , Francis Bocris
发明人： Ralf Pelzer , Wolfgang Krause , Karl Beck , Francis Bocris
IPC分类号： C11B9/00
CPC分类号： C11B9/008
摘要： The present invention relates to a fragrance composition comprising a mixture of diastereomers of 2-isobutyl-4-methyl-tetrahydro-2H-pyran-4-ol, which comprises more than 95 wt. % of the optically inactive cis-racemate and less than 5 wt. % of the optically inactive trans-racemate. The present invention further relates to a method for producing a perfumed product or article as well as perfumed or aromatized articles comprising the fragrance compositions of the present invention.
摘要翻译：本发明涉及包含2-异丁基-4-甲基 - 四氢-2H-吡喃-4-醇的非对映异构体的混合物的香料组合物，其包含大于95wt。％的光学活性的顺式外消旋物和小于5wt。％的光学无活性反式外消旋物。本发明还涉及一种用于生产加香产品或制品的方法，以及包含本发明的香料组合物的加香或芳香化制品。

2. 发明申请

US20100222606A1 METHOD FOR PRODUCING BISABOLOL WHICH IS FARNESOL FREE OR IS LOW IN FARNESOL 审中-公开
标题翻译：无机化学物质的双酚A的生产方法
公开(公告)号：US20100222606A1
公开(公告)日：2010-09-02
申请号：US12160918
申请日：2007-01-12
申请人： Hansgeorg Ernst , Klaus-Peter Pfaff , Karl Beck , Jürgen Schubert , Günther Gottwald , Wolfgang Krause
发明人： Hansgeorg Ernst , Klaus-Peter Pfaff , Karl Beck , Jürgen Schubert , Günther Gottwald , Wolfgang Krause
IPC分类号： C07C35/18 , C11C1/00
CPC分类号： C07C29/1285 , C07C29/095 , C07C67/02 , C07C67/03 , C07C403/08 , C07C2601/16 , C07C33/14 , C07C69/007 , C07C69/78 , C07C69/06 , C07C69/145
摘要： The present invention relates to a method of producing pure or enriched bisabolol by separating substance mixtures comprising bisabolol and farnesol by selective esterification of farnesol and subsequent distillative separation. The invention relates specifically to a method as specified above comprising the selective transesterification of mixtures comprising formyl-bisabolol and formyl-farnesol and subsequent distillative separation.The present invention furthermore relates to a method of producing farnesol esters.
摘要翻译：本发明涉及通过用法呢醇的选择性酯化和随后的蒸馏分离来分离包含红没药醇和法呢醇的物质混合物来生产纯的或富含的赤铁矿的方法。本发明具体涉及如上所述的方法，其包括含有甲酰基 - 对映体和甲酰法尼醇的混合物的选择性酯交换和随后的蒸馏分离。本发明还涉及一种生产法呢醇酯的方法。

3. 发明申请

US20130046118A1 METHOD FOR PRODUCING OPTICALLY ACTIVE, RACEMIC MENTHOL 审中-公开
标题翻译：用于生产光学活性的，法定的MENTHOL的方法
公开(公告)号：US20130046118A1
公开(公告)日：2013-02-21
申请号：US13658003
申请日：2012-10-23
申请人： Gunnar Heydrich , Gabriele Gralla , Matthias Rauls , Joachim Schmidt-Leithoff , Klaus Ebel , Wolfgang Krause , Steffen Oehlenschläger , Christoph Jäkel , Marko Friedrich , Eike Johannes Bergner , Nawid Kashani-Shirazi , Rocco Paciello
发明人： Gunnar Heydrich , Gabriele Gralla , Matthias Rauls , Joachim Schmidt-Leithoff , Klaus Ebel , Wolfgang Krause , Steffen Oehlenschläger , Christoph Jäkel , Marko Friedrich , Eike Johannes Bergner , Nawid Kashani-Shirazi , Rocco Paciello
IPC分类号： C07C29/17
CPC分类号： C07C29/56 , C07B2200/07 , C07C29/172 , C07C29/78 , C07C45/62 , C07C45/82 , C07C2601/14 , C07C2601/16 , C07C47/21 , C07C35/12 , C07C35/17
摘要： The present invention relates to a particularly economic overall method for producing menthol, specifically for producing optically active, essentially enantiomerically and diastereomerically pure L-menthol and racemic menthol, starting from the starting material citral which is available inexpensively on an industrial scale. The method comprises the following steps a.1) catalytic hydrogenation of neral and/or geranial to give citronellal, b.1) cyclization of citronellal to isopulegol in the presence of an acidic catalyst, c.1) purification of isopulegol by crystallization and d.1) catalytic hydrogenation of isopulegol to give menthol.
摘要翻译：本发明涉及一种特别经济的制备薄荷醇的总体方法，特别用于制备光学活性的，基本上是对映异构体和非对映异构体纯的L-薄荷醇和外消旋薄荷醇，其原料柠檬醛以工业规模廉价地得到。该方法包括以下步骤a.1）在酸性催化剂的存在下，将柠檬醛和/或香叶醇进行催化氢化以产生香茅醛，b.1）将香茅醛环化成异胡仑醇，c.1）通过结晶和d进行异丙醇的纯化 .1）异丙醇的催化氢化得到薄荷醇。

4. 发明授权

US08212084B2 Method for the production of 4,4′-[1-trifluoromethyl)alkylidene]-bis-(2,6-diphenylphenols) 有权
标题翻译：制备4,4' - [1-三氟甲基）亚烷基] - 双（2,6-二苯基苯酚）
公开(公告)号：US08212084B2
公开(公告)日：2012-07-03
申请号：US12808865
申请日：2008-12-17
申请人： Gabriele Gralla , Gunnar Heydrich , Klaus Ebel , Wolfgang Krause
发明人： Gabriele Gralla , Gunnar Heydrich , Klaus Ebel , Wolfgang Krause
IPC分类号： C07C39/16 , C07C39/12
CPC分类号： C07C45/74 , C07C37/07 , C07C37/20 , C07C37/62 , C07C49/613 , C07C49/653 , C07C39/15 , C07C39/367
摘要： The present invention relates to a process for preparing 4,4′-[1-(trifluoromethyl)alkylidene]bis(2,6-diphenylphenols), in particular for preparing 4,4′-[1-(trifluoromethyl)ethylidene]bis(2,6-diphenylphenol), which comprises the self-condensation of cyclohexanone in the presence of a basic catalyst to form tricyclic condensation products, dehydrogenation of the resulting tricyclic condensation products in the presence of a supported transition metal catalyst in the condensed phase to form 2,6-diphenylphenol and reaction of the 2,6-diphenylphenol with a trifluoromethyl ketone. The invention further provides an improved process for preparing 2,6-diphenylphenol by aldol self-condensation of cyclohexanone.
摘要翻译：本发明涉及一种制备4,4' - [1-（三氟甲基）亚烷基]双（2,6-二苯基苯酚）的方法，特别是制备4,4' - [1-（三氟甲基）亚乙基]双（ 2,6-二苯基苯酚），其包括环己酮在碱性催化剂存在下的自缩合以形成三环缩合产物，所得三环缩合产物在冷凝相中负载的过渡金属催化剂存在下脱氢形成 2,6-二苯基苯酚和2,6-二苯基苯酚与三氟甲基酮的反应。本发明还提供了通过环己酮的醛醇自缩合制备2,6-二苯基苯酚的改进方法。

5. 发明申请

US20100206712A1 CONTINUOUS PROCESS FOR PREPARING MENTHOL IN PURE OR ENRICHED FORM 有权
标题翻译：用于制备纯净或增强形式的MENTHOL的连续方法
公开(公告)号：US20100206712A1
公开(公告)日：2010-08-19
申请号：US12677688
申请日：2008-07-23
申请人： Gunnar Heydrich , Gabriele Gralla , Klaus Ebel , Wolfgang Krause , Nawid Kashani-Shirazi
发明人： Gunnar Heydrich , Gabriele Gralla , Klaus Ebel , Wolfgang Krause , Nawid Kashani-Shirazi
IPC分类号： C07C29/80 , B01D3/14 , B01J19/00 , C07C35/12
CPC分类号： B01D3/141 , B01D3/14 , C07B2200/07 , C07C29/80 , C07C2601/14 , C07C35/12 , C07C35/17
摘要： The present invention relates to a continuous process for preparing racemic or optically active menthol in pure or enriched form by distillatively separating menthol from substance mixtures which comprise essentially menthol and diastereomers thereof. This distillatiive separation is performed in a dividing wall column with 50 to 300 theoretical plates and one or more side draw points at an absolute operating pressure of 5 to 500 mbar.
摘要翻译：本发明涉及通过将薄荷醇与基本上含有薄荷醇和非对映异构体的物质混合物蒸馏分离来制备纯的或富集形式的外消旋或光学活性薄荷醇的连续方法。该蒸馏分离在具有50至300个理论塔板和一个或多个侧向牵引点的分隔壁塔中进行，绝对操作压力为5至500毫巴。

6. 发明申请

US20100204083A1 PROCESS FOR THE PREPARATION OF ETHYLGERANONITRILE 审中-公开
标题翻译：乙酰胆碱酯酶的制备方法
公开(公告)号：US20100204083A1
公开(公告)日：2010-08-12
申请号：US12670689
申请日：2008-07-16
申请人： Martine Weis , Bernhard Brunner , Klaus Ebel , Wolfgang Krause
发明人： Martine Weis , Bernhard Brunner , Klaus Ebel , Wolfgang Krause
IPC分类号： C07C253/30 , A61K8/40
CPC分类号： C11B9/0023 , A61K8/40 , A61L9/01 , A61Q13/00 , C07C253/30 , C07C255/07 , C11D3/50
摘要： The present invention relates to a method of producing ethylgeranonitrile through reaction of ethylheptenone with a deprotonated nitrile and, if appropriate, subsequent saponification and decarboxylation. Moreover, the invention relates to mixtures comprising 3,7-dimethyl-2,6-nonadienenitrile and at least one compound selected from the group of compounds 3,7-dimethyl-3,6-nonadienenitrile and 3-methylene-7-methyl-6-nonenenitrile, and to fragrance compositions comprising these.
摘要翻译：本发明涉及通过乙基庚烯酮与去质子化腈的反应以及如果合适的话随后皂化和脱羧反应生产乙腈的方法。此外，本发明涉及包含3,7-二甲基-2,6-壬二腈和至少一种选自化合物3,7-二甲基-3,6-壬二腈和3-亚甲基-7-甲基 - 6-壬烯腈，以及包含它们的香料组合物。

7. 发明授权

US08414744B2 Continuous process for preparing menthol in pure or enriched form 有权
标题翻译：用于制备纯粹或富集形式的薄荷醇的连续方法
公开(公告)号：US08414744B2
公开(公告)日：2013-04-09
申请号：US12677688
申请日：2008-07-23
申请人： Gunnar Heydrich , Gabriele Gralla , Klaus Ebel , Wolfgang Krause , Nawid Kashani-Shirazi
发明人： Gunnar Heydrich , Gabriele Gralla , Klaus Ebel , Wolfgang Krause , Nawid Kashani-Shirazi
IPC分类号： B01D3/14
CPC分类号： B01D3/141 , B01D3/14 , C07B2200/07 , C07C29/80 , C07C2601/14 , C07C35/12 , C07C35/17
摘要： The present invention relates to a continuous process for preparing racemic or optically active menthol in pure or enriched form by distillatively separating menthol from substance mixtures which comprise essentially menthol and diastereomers thereof. This distillatiive separation is performed in a dividing wall column with 50 to 300 theoretical plates and one or more side draw points at an absolute operating pressure of 5 to 500 mbar.
摘要翻译：本发明涉及通过将薄荷醇与基本上含有薄荷醇和非对映异构体的物质混合物蒸馏分离来制备纯的或富集形式的外消旋或光学活性薄荷醇的连续方法。该蒸馏分离在具有50至300个理论塔板和一个或多个侧向牵引点的分隔壁塔中进行，绝对操作压力为5至500毫巴。

8. 发明申请

US20100106066A1 ANKLE JOINT ORTHESIS 有权
公开(公告)号：US20100106066A1
公开(公告)日：2010-04-29
申请号：US12439982
申请日：2007-09-05
申请人： Heinrich Hess , Rainer Scheuermann , Wolfgang Krause
发明人： Heinrich Hess , Rainer Scheuermann , Wolfgang Krause
IPC分类号： A61F5/00
CPC分类号： A61F5/0111
摘要： The invention relates to an ankle orthosis comprising a U-shaped support stirrup made of a flexible material, the sides of which stirrup converge beneath the foot in a web projecting as a tab toward the metatarsus, extend past the bones, and are held together at their end regions by a fastening strap wrapping around the leg. The tab has a convexity, which presses against the cuboid bone of the foot due to a preloading of the tab.
摘要翻译：本发明涉及一种踝关节矫形器，其包括由柔性材料制成的U形支撑箍，其两侧的镫骨在脚下方会聚在以朝向跖骨的突出部突出的腹板中延伸超过骨骼，并且保持在一起它们的端部区域通过围绕腿部的紧固带缠绕。突片具有凸起，其由于突片的预加载而压靠脚的长方体骨。

9. 发明授权

US06242653B1 Process for the preparation of &agr;-diketones from ketols or ketals from ketols 失效
标题翻译：从酮基酮或酮缩酮制备α-二酮的方法
公开(公告)号：US06242653B1
公开(公告)日：2001-06-05
申请号：US09377732
申请日：1999-08-19
申请人： Werner Aquila , Jörg Botzem , Melanie Brunner , Hartwig Fuchs , Wolfgang Krause , Klaus Pandl , Ulrich Schäfer-Lüderssen
发明人： Werner Aquila , Jörg Botzem , Melanie Brunner , Hartwig Fuchs , Wolfgang Krause , Klaus Pandl , Ulrich Schäfer-Lüderssen
IPC分类号： C07C4529
CPC分类号： C07C45/39 , C07C45/515 , C07C49/12 , C07C49/175 , C07C49/517
摘要： The process for the preparation of carbonyl compounds of the formula I where R1 and R2 are a hydrocarbon radical, or R1 and R2 together are an unsubstituted or substituted alkylene group, and X is=O or two alkoxy groups, comprises oxidizing alcohols of the formula II where R1 to R2 and X are as defined above, with oxygen in the gaseous phase a) at temperatures of from 270 to 600° C. on silver coated catalysts which comprise an abrasion-resistant coating of metallic silver on a core of inert support material, or b) at temperatures of from 450 to 750° C. on silver crystals and/or copper crystals having a particle size of from 0.1 to 2.5 mm for a residence time of at most 0.1 second. Also claimed is an advantageous overall process for the preparation of &agr;-diketones, preferably diacetal, from the corresponding ketone, in particular methyl ethyl ketone, via the carbonyl compounds of the formula I where X is two alkoxy groups.
摘要翻译：制备式I的羰基化合物的方法，其中R 1和R 2是烃基，或者R 1和R 2一起是未取代或取代的亚烷基，并且X是= O或两个烷氧基，包括氧化式II的醇，其中R 1 在含有惰性载体材料芯上的金属银的耐磨涂层的银涂覆的催化剂上，在温度为270-600℃的温度下，R2和X如上定义，在气相中为氧）在450至750℃的温度下，在银晶体和/或具有0.1至2.5mm的粒度的铜晶体上，停留时间至多为0.1秒。还要求保护的是制备α 二酮，优选二缩醛，通过其中X是两个烷氧基的式I的羰基化合物从相应的酮，特别是甲基乙基酮中获得。

10. 发明授权

US5893392A Regulating valve 失效
标题翻译：调节阀
公开(公告)号：US5893392A
公开(公告)日：1999-04-13
申请号：US748039
申请日：1996-11-12
申请人： Karl-Heinz Spies , Thomas Barth , Wolfgang Krause
发明人： Karl-Heinz Spies , Thomas Barth , Wolfgang Krause
IPC分类号： F01P7/14 , F16K11/076 , F16K11/085 , F16K11/02
CPC分类号： F16K11/076 , F16K11/0853 , F01P2007/146 , Y10T137/86871
摘要： A regulating valve comprising a housing having a cylindrical valve chamber, the valve chamber being provided with at least one inlet and at least two outlets, the inlet and the outlets being at least partially closeable as needed by a common valve body arranged in the valve chamber and rotatable around an axis, the valve body being operable by an actuator, the inlet and/or at least one of the outlets being surrounded by a sealing device on the side of the housing facing the valve body and the sealing device being able to be brought into sealing engagement with the valve body under elastic preload. The valve body is designed having the shape of the segment of a cylinder and is bounded on the peripheral side by two boundary surfaces which each have an edge on the side facing the housing, the edge overtravelling the inlet during its opening being designed as an efflux edge and having an elliptically shaped recess extending in axial direction. Configured in the valve body is a duct-shaped opening which extends between the boundary surfaces and penetrates them.
摘要翻译：一种调节阀，包括具有圆柱形阀室的壳体，所述阀室设置有至少一个入口和至少两个出口，所述入口和所述出口根据需要至少部分地可关闭，所述公共阀体布置在所述阀室中并且可围绕轴线旋转，所述阀体可由致动器操作，所述入口和/或所述至少一个出口被所述壳体面向所述阀体的侧面上的密封装置包围，并且所述密封装置能够在弹性预载下与阀体密封接合。阀体被设计成具有圆柱形部分的形状并且在周边侧边界由两个边界面，每个边界面在面向壳体的一侧上具有边缘，在其开口期间过度进入入口的边缘被设计为外流并且具有沿轴向方向延伸的椭圆形凹部。在阀体中配置的是在边界表面之间延伸并穿透其的管状开口。

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