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1. 发明申请

US20100316552A1 PROCESS FOR PREPARING HYDROGEN CYANIDE BY CATALYTIC DEHYDRATION OF GASEOUS FORMAMIDE 审中-公开
标题翻译：通过气相甲酰胺催化脱氢制备氢氰化物的方法
公开(公告)号：US20100316552A1
公开(公告)日：2010-12-16
申请号：US12742773
申请日：2008-11-10
申请人： Ralf Boehling , Andreas Deckers , Thomas Schneider , Guenther Achhammer , Hermann Luyken , Peter Pfab , Klaus Schubert , Manfred Kraut
发明人： Ralf Boehling , Andreas Deckers , Thomas Schneider , Guenther Achhammer , Hermann Luyken , Peter Pfab , Klaus Schubert , Manfred Kraut
IPC分类号： C01C3/02
CPC分类号： C01C3/0204 , B01J19/0093 , B01J2219/00783 , B01J2219/00822 , B01J2219/00835 , B01J2219/0086 , B01J2219/00873
摘要： A process for preparing hydrogen cyanide, comprising the provision of gaseous formamide by evaporating liquid formamide in an evaporator (step i)) and the catalytic dehydration of the gaseous formamide (step ii)), and also an apparatus for performing the process according to the invention, comprising at least one microevaporator and a tubular reactor, and the use of a microevaporator for evaporating formamide in a process for preparing hydrogen cyanide from formamide.
摘要翻译：一种制备氰化氢的方法，包括通过在蒸发器中蒸发液体甲酰胺（步骤i））和气态甲酰胺的催化脱水（步骤ii）提供气态甲酰胺），以及用于执行根据本发明包括至少一个微蒸发器和管式反应器，以及在从甲酰胺制备氰化氢的方法中使用微蒸发器蒸发甲酰胺。

2. 发明申请

US20100284889A1 METHOD FOR PRODUCING HYDROCYANIC ACID BY CATALYTIC DEHYDRATION OF GASEOUS FORMAMIDE 审中-公开
标题翻译：通过气相甲醛催化脱氢生产氢氯酸的方法
公开(公告)号：US20100284889A1
公开(公告)日：2010-11-11
申请号：US12742845
申请日：2008-11-12
申请人： Ralf Boehling , Andreas Deckers , Thomas Schneider , Guenther Achhammer , Hermann Luyken , Peter Pfab
发明人： Ralf Boehling , Andreas Deckers , Thomas Schneider , Guenther Achhammer , Hermann Luyken , Peter Pfab
IPC分类号： C01C3/02 , B01J8/04
CPC分类号： C01C3/0204 , B01J19/0093 , B01J2219/00783 , B01J2219/00822 , B01J2219/00835 , B01J2219/0086 , B01J2219/00873
摘要： A process for preparing hydrogen cyanide by catalytically dehydrating gaseous formamide in a tubular reactor formed from at least one reaction channel in which the catalytic dehydration proceeds, said reaction channel having an inner surface which is formed from a material having an iron content of ≧50% by weight, and no additional catalysts and/or internals being present in the reaction channel, and the at least one reaction channel having a mean hydraulic diameter of from 0.5 to 6 mm, and a reactor with the features specified above and the use of the inventive reactor for preparing hydrogen cyanide by catalytically dehydrating gaseous formamide.
摘要翻译：一种通过在由催化脱水进行的至少一个反应通道形成的管式反应器中催化脱水气态甲酰胺制备氰化氢的方法，所述反应通道具有由铁含量为≥50％的材料形成的内表面，，并且在反应通道中不存在另外的催化剂和/或内部物质，并且所述至少一个反应通道具有0.5-6mm的平均水力直径，以及具有上述特征的反应器和使用通过催化脱水气态甲酰胺制备氰化氢的本发明反应器。

3. 发明授权

US09249029B2 Single chamber vaporizer and use thereof in chemical synthesis 有权
标题翻译：单室蒸发器及其在化学合成中的应用
公开(公告)号：US09249029B2
公开(公告)日：2016-02-02
申请号：US13011315
申请日：2011-01-21
申请人： Ralf Boehling , Michael Schipper , Stefan Birnbach , Peter Petersen , Achim Gritsch , Alois Wellisch , Hermann Luyken , Albert Steiner , Peter Zehner
发明人： Ralf Boehling , Michael Schipper , Stefan Birnbach , Peter Petersen , Achim Gritsch , Alois Wellisch , Hermann Luyken , Albert Steiner , Peter Zehner
IPC分类号： C01C3/02 , F22B33/00 , F01K23/06 , F22B27/00
CPC分类号： C01C3/0204 , F01K23/064 , F22B27/00 , F22B33/00
摘要： The invention relates to an improved process for vaporizing organic compounds and the further conversion thereof.
摘要翻译：本发明涉及一种汽化有机化合物的改进方法及其进一步转化。

4. 发明申请

US20110033363A1 PROCESS FOR PREPARING HYDROCYANIC ACID BY CATALYTIC DEHYDRATION OF GASEOUS FORMAMIDE - DIRECT HEATING 有权
标题翻译：通过气相脱除气相法直接加热制备油酸的方法
公开(公告)号：US20110033363A1
公开(公告)日：2011-02-10
申请号：US12935840
申请日：2009-03-30
申请人： Ralf Boehling , Andreas Deckers , Achim Gritsch , Stefan Kotrel
发明人： Ralf Boehling , Andreas Deckers , Achim Gritsch , Stefan Kotrel
IPC分类号： C01C3/02
CPC分类号： C01C3/0204 , B01J19/0093 , B01J19/249 , B01J2219/00783 , B01J2219/00788 , B01J2219/00822 , B01J2219/00824 , B01J2219/00835 , B01J2219/0086 , B01J2219/00873 , B01J2219/00889 , B01J2219/2453 , B01J2219/2459 , B01J2219/2465 , B01J2219/2474 , B01J2219/2479 , B01J2219/2481 , B01J2219/2486 , B01J2219/2487 , B01J2219/2497 , C01C3/02
摘要： Process for preparing hydrocyanic acid by catalytic dehydration of gaseous formamide, wherein the dehydration of formamide is coupled with an exothermic reaction by the reactor used in the dehydration comprising two separate fluid paths which are separated by a common reactor wall, with one fluid path being provided for the dehydration of formamide and the second fluid path being provided for the exothermic reaction.
摘要翻译：通过气态甲酰胺的催化脱水制备氢氰酸的方法，其中甲酰胺的脱水通过用于脱水的反应器与放热反应相结合，所述反应器包括由共同反应器壁分离的两个分离的流体路径，其中提供一个流体路径用于甲酰胺的脱水和为放热反应提供的第二流体路径。

5. 发明授权

US09034293B2 Process for preparing hydrocyanic acid by catalytic dehydration of gaseous formamide—direct heating 有权
标题翻译：通过气态甲酰胺直接加热催化脱水制备氢氰酸的方法
公开(公告)号：US09034293B2
公开(公告)日：2015-05-19
申请号：US12935840
申请日：2009-03-30
申请人： Ralf Boehling , Andreas Deckers , Achim Gritsch , Stefan Kotrel
发明人： Ralf Boehling , Andreas Deckers , Achim Gritsch , Stefan Kotrel
IPC分类号： C01C3/02 , B01J19/00 , B01J19/24
CPC分类号： C01C3/0204 , B01J19/0093 , B01J19/249 , B01J2219/00783 , B01J2219/00788 , B01J2219/00822 , B01J2219/00824 , B01J2219/00835 , B01J2219/0086 , B01J2219/00873 , B01J2219/00889 , B01J2219/2453 , B01J2219/2459 , B01J2219/2465 , B01J2219/2474 , B01J2219/2479 , B01J2219/2481 , B01J2219/2486 , B01J2219/2487 , B01J2219/2497 , C01C3/02
摘要： Process for preparing hydrocyanic acid by catalytic dehydration of gaseous formamide, wherein the dehydration of formamide is coupled with an exothermic reaction by the reactor used in the dehydration comprising two separate fluid paths which are separated by a common reactor wall, with one fluid path being provided for the dehydration of formamide and the second fluid path being provided for the exothermic reaction.
摘要翻译：通过气态甲酰胺的催化脱水制备氢氰酸的方法，其中甲酰胺的脱水通过用于脱水的反应器与放热反应相结合，所述反应器包括由共同反应器壁分离的两个分离的流体路径，其中提供一个流体路径用于甲酰胺的脱水和为放热反应提供的第二流体路径。

6. 发明申请

US20100048960A1 PROCESS FOR PREPARING ISOPROPANOL AND 2-BUTANOL FROM THE CORRESPONDING ALKANES 失效
标题翻译：从相应的碱中制备异丙醇和2-丁醇的方法
公开(公告)号：US20100048960A1
公开(公告)日：2010-02-25
申请号：US12374351
申请日：2007-07-16
申请人： Georg Degen , Sven Crone , Ralf Boehling , Ansgar Gereon Altenhoff , Wolfgang Rohde , Jochen Buerkle , Goetz-Peter Schindler , Thomas Holtmann , Markus Schmitt
发明人： Georg Degen , Sven Crone , Ralf Boehling , Ansgar Gereon Altenhoff , Wolfgang Rohde , Jochen Buerkle , Goetz-Peter Schindler , Thomas Holtmann , Markus Schmitt
IPC分类号： C07C29/04
CPC分类号： C07C67/04 , C07C29/095 , Y02P20/127 , C07C31/10 , C07C31/12 , C07C69/06 , C07C69/14
摘要： A process for preparing alkanols (I) selected from the group consisting of isopropanol and 2-butanol from the corresponding alkanes (II) selected from the group consisting of propane and n-butane, comprising the steps of: A) providing a starting gas stream a comprising the alkane (II); B) feeding the starting gas stream a comprising the alkane (II) into a dehydrogenation zone and subjecting the alkane (II) to a dehydrogenation to the alkene (III) to obtain a product gas stream b comprising the alkene (III) and unconverted alkane (II), with or without high boilers, steam, hydrogen and low boilers; C) at least compressing product gas stream b, optionally separating product gas stream b into an aqueous phase c1, a phase c2 comprising the alkene (III) and the alkane (II), with or without high boilers, and a gas phase c3 comprising hydrogen and low boilers; D) reacting product gas stream b or the phase c2 comprising alkene (III) and alkane (II) with an organic acid (IV) in an esterification zone to obtain a product mixture d comprising the corresponding alkyl ester (V) of the organic acid and the unconverted alkane (II); E) removing from product mixture d a gas stream e1 which comprises an alkane (II) and is recycled into the dehydrogenation zone if appropriate, and a product mixture e2 comprising the alkyl ester; F) reacting the product mixture e2 comprising the alkyl ester with water in an ester hydrolysis zone to give a product mixture f comprising the alkanol (I) and the organic acid (IV); G) removing the alkanol (I) and the organic acid (IV) from product mixture f and, if appropriate, recycling the organic acid into the esterification zone.
摘要翻译：从选自丙烷和正丁烷的相应的烷烃（II）制备选自异丙醇和2-丁醇的链烷醇（I）的方法，包括以下步骤：A）提供起始气流 a包含烷烃（II）; B）将包含烷烃（II）的起始气体流（a）进料到脱氢区中并使烷烃（II）脱氢至烯烃（III），得到包含烯烃（III）和未转化烷烃的产物气流b （II），有或没有高锅炉，蒸汽，氢气和低锅炉; C）至少压缩产物气流b，任选地将产物气流b分离成水相c1，包含烯烃（III）和烷烃（II）的阶段c2，具有或不具有高锅炉，以及气相c3，其包含氢和低锅炉; D）使产物气流b或包含烯烃（III）和烷烃（II）的相c与酯化区中的有机酸（IV）反应，得到包含相应的有机酸烷基酯（V）的产物混合物d 和未转化的烷烃（II）; E）从产物混合物d除去包含烷烃（II）的气流e1，并且如果合适的话再循环到脱氢区中，以及包含烷基酯的产物混合物e2; F）在酯水解区中使包含烷基酯的产物混合物e2与水反应，得到包含链烷醇（I）和有机酸（IV）的产物混合物f; G）从产物混合物f中除去链烷醇（I）和有机酸（IV），如果合适，将有机酸再循环到酯化区。

7. 发明申请

US20080283384A1 Process for Producing Trioxane and at Least One Comonomer 审中-公开
标题翻译：生产三恶烷和至少一种共聚单体的方法
公开(公告)号：US20080283384A1
公开(公告)日：2008-11-20
申请号：US12091976
申请日：2006-10-27
申请人： Neven Lang , Ralf Boehling , Achim Stammer , Jan Oldenburg , Markus Siegert , Eckhard Stroefer
发明人： Neven Lang , Ralf Boehling , Achim Stammer , Jan Oldenburg , Markus Siegert , Eckhard Stroefer
IPC分类号： C08G2/10 , B01D3/34 , C07D317/12 , C07D323/06
CPC分类号： C08G2/10 , C07D317/12 , C07D323/06 , C08G2/20 , Y02P20/127 , Y02P20/582
摘要： The invention relates to a process for preparing trioxane and at least one comonomer for preparing (co)polymers based on trioxane, in which, in a first step, formaldehyde the at least one comonomer reactant are reacted in aqueous solution to give trioxane and comonomer, to obtain a reaction mixture A1 comprising trioxane, comonomer, formaldehyde and water, with or without comonomer reactant. In a second step, the reaction mixture A1 is distilled in a first distillation stage at a first pressure to obtain a stream B1 enriched in trioxane and comonomer and a stream B2 comprising essentially water and formaldehyde, with or without comonomer reactant. In a third step, stream B1 is distilled in a second distillation stage at a pressure which is above the pressure of the first distillation stage to obtain a stream C1 comprising trioxane, comonomer and water and a product stream C2 consisting essentially of comonomer and trioxane.
摘要翻译：本发明涉及一种制备三恶烷和至少一种共聚单体的方法，该共聚单体用于制备基于三恶烷的（共）聚合物，其中在第一步中，甲醛将至少一种共聚单体反应物在水溶液中反应得到三恶烷和共聚单体，得到含有或不含共聚单体反应物的三恶烷，共聚单体，甲醛和水的反应混合物A 1。在第二步中，将反应混合物A 1在第一压力下在第一蒸馏阶段进行蒸馏，以获得富含三恶烷和共聚单体的物流B 1和基本上含有水和甲醛的物流B 2，具有或不含共聚单体反应物。在第三步骤中，在第二蒸馏阶段，在高于第一蒸馏阶段的压力的压力下蒸馏出料流B 1，以获得包含三恶烷，共聚单体和水的料流C 1和基本上由共聚单体组成的产物流C 2 和三恶烷。

8. 发明授权

US08772535B2 Process for preparing isocyanates 失效
标题翻译：异氰酸酯的制备方法
公开(公告)号：US08772535B2
公开(公告)日：2014-07-08
申请号：US13442401
申请日：2012-04-09
申请人： Ralf Boehling , Sven Kueber , Stefan Maixner , Eckhard Stroefer , Jochem Henkelmann , Georg Krug , Werner Bolz
发明人： Ralf Boehling , Sven Kueber , Stefan Maixner , Eckhard Stroefer , Jochem Henkelmann , Georg Krug , Werner Bolz
IPC分类号： C07C263/00
CPC分类号： C07C263/10 , B01J2219/00038 , B01J2219/00869 , C07C2601/14 , C07C265/14
摘要： Process for preparing isocyanates by phosgenation of amines, wherein phosgene and amine are brought into contact in at least 2 mixing chambers connected in parallel.
摘要翻译：通过胺的光气化制备异氰酸酯的方法，其中光气和胺在至少两个并联连接的混合室中接触。

9. 发明申请

US20100227997A1 METHOD FOR PREPARING ISOCYANATE ADDUCTS 审中-公开
标题翻译：制备异氰酸酯添加剂的方法
公开(公告)号：US20100227997A1
公开(公告)日：2010-09-09
申请号：US11916600
申请日：2006-06-14
申请人： Martin Fiene , Ralf Boehling , Eckhard Stroefer , Herbert Vogel , Fatima Mesri
发明人： Martin Fiene , Ralf Boehling , Eckhard Stroefer , Herbert Vogel , Fatima Mesri
IPC分类号： C08G18/08
CPC分类号： C07C263/20 , C07C209/62 , C08G18/4833 , C08G18/485 , C08G18/7621 , C08G2101/0008 , C08J11/16 , C08J2375/04 , Y02W30/705 , C07C211/50 , C07C265/14
摘要： The present invention provides a process for working up isocyanate adducts, comprising the steps of a) reacting the isocyanate adducts with pure ammonia, b) working up the reaction products obtained in step a), c) recycling the amines formed into the isocyanate production.
摘要翻译：本发明提供了一种加工异氰酸酯加合物的方法，包括以下步骤：a）使异氰酸酯加合物与纯氨反应，b）处理步骤a）中得到的反应产物，c）将形成的胺再生成异氰酸酯生产。

10. 发明授权

US08487127B2 Process for preparing isocyanates in the gas phase 有权
标题翻译：在气相中制备异氰酸酯的方法
公开(公告)号：US08487127B2
公开(公告)日：2013-07-16
申请号：US13035166
申请日：2011-02-25
申请人： Torsten Mattke , Ralf Boehling , Carsten Knoesche , Vanessa Simone Lehr
发明人： Torsten Mattke , Ralf Boehling , Carsten Knoesche , Vanessa Simone Lehr
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C07C265/14
摘要： The invention relates to a process for preparing isocyanates by reacting the corresponding amines with phosgene in the gas phase, in the presence or absence of an inert medium, which comprises the following steps: (a) vaporization of the amine in a vaporizer, (b) superheating of the amine, (c) mixing of the gaseous amine with the phosgene and introduction into a reaction zone, (d) reaction of amine and phosgene to give isocyanate in the reaction zone, with a reaction mixture comprising isocyanate and hydrogen chloride being formed, (e) cooling of the reaction mixture comprising isocyanate and hydrogen chloride, wherein the vaporizer comprises a vessel in which tubes through which a heating medium flows are comprised, where number and diameter of the tubes are designed so that the tubes have a specific heat transfer area based on the volume through which the amine flows of at least 300 m2/m3.
摘要翻译：本发明涉及通过在惰性介质存在或不存在的情况下使气相中相应的胺与光气反应来制备异氰酸酯的方法，其包括以下步骤：（a）蒸发器中胺的蒸发，（b ）胺的过热，（c）将气态胺与光气混合并引入反应区，（d）胺和光气在反应区中反应得到异氰酸酯，反应混合物包含异氰酸酯和氯化氢形成（e）包含异氰酸酯和氯化氢的反应混合物的冷却，其中蒸发器包括容器，其中包含加热介质流过的管，其中管的数量和直径被设计成使得管具有特定的基于胺流动的体积至少为300m 2 / m 3的传热面积。

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