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1. 发明申请

US20090012297A1 Ionic liquids as solvents 有权
标题翻译：离子液体作为溶剂
公开(公告)号：US20090012297A1
公开(公告)日：2009-01-08
申请号：US12108347
申请日：2008-04-23
申请人： Philip F. Pagoria , Amitesh Maiti , Alexander Gash , Thomas Yong Han , Christine Orme , Laurence Fried
发明人： Philip F. Pagoria , Amitesh Maiti , Alexander Gash , Thomas Yong Han , Christine Orme , Laurence Fried
IPC分类号： C07C209/84 , C07D241/20
CPC分类号： C07C209/84 , C07D241/20 , Y02P20/542 , C07C211/52
摘要： A method in one embodiment includes contacting a strongly hydrogen bonded organic material with an ionic liquid having a fluoride anion for solubilizing the strongly hydrogen bonded organic material; and maintaining the ionic liquid at a temperature of about 90° C. or less during the contacting. A method in another embodiment includes contacting a strongly hydrogen bonded organic material with an ionic liquid having an acetate or formate anion for solubilizing the strongly hydrogen bonded organic material; and maintaining the ionic liquid at a temperature of less than about 90° C. during the contacting. A method for purifying a strongly hydrogen bonded organic material according to one another embodiment includes dissolving a strongly hydrogen bonded organic material, selected from a group consisting of 1,3,5-triamino-2,4,6-trinitrobenzene and 2,6-diamino-3,5-dinitropyrazine-1-oxide, in a solution comprising an ionic liquid, the ionic liquid having an anion selected from a group consisting of a fluoride anion, an acetate anion, and a formate anion; maintaining the solution at a temperature of about 70° C. or less during the contacting; and recrystallizing the strongly hydrogen bonded organic material.
摘要翻译：在一个实施方案中的方法包括使强氢键合有机材料与具有氟阴离子的离子液体接触，以溶解强氢键合的有机材料; 并且在接触期间将离子液体维持在约90℃或更低的温度。在另一个实施方案中的方法包括使强氢键合有机材料与具有乙酸盐或甲酸根阴离子的离子液体接触，以溶解强氢键合有机材料; 并且在接触期间将离子液体保持在小于约90℃的温度。根据另一个实施方案的用于纯化强氢键合的有机材料的方法包括将选自1,3,5-三氨基-2,4,6-三硝基苯和2,6-二硝基苯的强氢键合有机材料溶解，二氨基-3,5-二硝基吡嗪-1-氧化物，在包含离子液体的溶液中，所述离子液体具有选自氟化物阴离子，乙酸根阴离子和甲酸根阴离子的阴离子; 在接触期间将溶液保持在约70℃或更低的温度; 并重结晶强氢键合的有机材料。

2. 发明授权

US06706889B1 Dinitropyrazolopyrazole-amine salts useful in gun propellants 失效
标题翻译：用于枪式推进剂的二硝基吡唑并吡唑 - 胺盐
公开(公告)号：US06706889B1
公开(公告)日：2004-03-16
申请号：US10326964
申请日：2002-12-20
申请人： Alfred G. Stern , Jesse S. Moran , R. Jason Jouet , Michael E. Sitzman , Philip F. Pagoria , Gregory S. Lee
发明人： Alfred G. Stern , Jesse S. Moran , R. Jason Jouet , Michael E. Sitzman , Philip F. Pagoria , Gregory S. Lee
IPC分类号： C07D23154
CPC分类号： C07D487/04
摘要： Dinitropyrazolopyrazole-amine salts are used as burn modifier ingredients in gun propellant compositions.
摘要翻译：二硝基吡唑并吡唑 - 胺盐用作枪式推进剂组合物中的燃烧改性剂成分。

3. 发明授权

US08815606B2 Thin-layer chromatography and colorimetric analysis of multi-component explosive mixtures 有权
标题翻译：多组分爆炸性混合物的薄层色谱和比色分析
公开(公告)号：US08815606B2
公开(公告)日：2014-08-26
申请号：US12106400
申请日：2008-04-21
申请人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman
发明人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman
IPC分类号： G01N30/90 , G01N30/96
CPC分类号： G01N30/94 , G01N30/90 , G01N33/22
摘要： A thin-layer chromatography method for detection and identification of common military and peroxide explosives in samples includes the steps of provide a reverse-phase thin-layer chromatography plate; prepare the plate by marking spots on which to deposit the samples by touching the plate with a marker; spot one micro liter of a first standard onto one of the spots, spot one micro liter of a second standard onto another of the spots, and spot samples onto other of spots producing a spotted plate; add eluent to a developing chamber; add the spotted plate to the developing chamber; remove the spotted plate from the developing chamber producing a developed plate; place the developed plate in an ultraviolet light box; add a visualization agent to a dip tank; dip the developed plate in the dip tank and remove the developed plate quickly; and detect explosives by viewing said developed plate.
摘要翻译：用于检测和鉴定样品中常见的军用和过氧化物炸药的薄层色谱法包括提供反相薄层色谱板的步骤; 通过用标记触摸板来标记沉积样品的斑点来准备板; 将一微升第一标准物放在其中一个斑点上，将一微升第二标准物放在另一个斑点上，并将样品点样到产生斑点板的其他斑点上; 将洗脱液加入显影室; 将点样板加到显影室; 从显影室中取出点样板，产生显影板; 将显影的板放在紫外灯箱中; 将一个可视化代理添加到浸槽中; 将显影的板块浸入浸渍槽中，快速取出显影板; 并通过查看所述显影板来检测爆炸物。

4. 发明申请

US20100229633A1 Spot Test Kit For Explosives Detection 有权
标题翻译：爆炸物检测用现货检测套件
公开(公告)号：US20100229633A1
公开(公告)日：2010-09-16
申请号：US12785299
申请日：2010-05-21
申请人： Philip F. Pagoria , Richard E. Whipple , Peter J. Nunes , Joel Del Eckels , John G. Reynolds , Robin R. Miles , Marina L. Chiarappa-Zucca
发明人： Philip F. Pagoria , Richard E. Whipple , Peter J. Nunes , Joel Del Eckels , John G. Reynolds , Robin R. Miles , Marina L. Chiarappa-Zucca
IPC分类号： G01N33/22
CPC分类号： G01N31/22 , B01L3/5023 , B01L3/5029 , B01L2200/16 , B01L2300/0867 , B01L2300/1827 , B01L2300/1877 , B01L2400/0406 , B01L2400/0683 , G01N1/02 , G01N33/227 , G01N2001/022 , G01N2001/028
摘要： An explosion tester system comprising a body, a lateral flow membrane swab unit adapted to be removeably connected to the body, a first explosives detecting reagent, a first reagent holder and dispenser operatively connected to the body, the first reagent holder and dispenser containing the first explosives detecting reagent and positioned to deliver the first explosives detecting reagent to the lateral flow membrane swab unit when the lateral flow membrane swab unit is connected to the body, a second explosives detecting reagent, and a second reagent holder and dispenser operatively connected to the body, the second reagent holder and dispenser containing the second explosives detecting reagent and positioned to deliver the second explosives detecting reagent to the lateral flow membrane swab unit when the lateral flow membrane swab unit is connected to the body.
摘要翻译：一种爆炸测试器系统，包括主体，适于可移除地连接到主体的侧面流动的薄膜拭子单元，第一爆炸物检测试剂，可操作地连接到主体的第一试剂保持器和分配器，第一试剂保持器和分配器包含第一爆炸物检测试剂，并且定位成当侧流膜拭子单元连接到身体时将第一炸药检测试剂输送到侧流膜拭子单元，第二爆炸物检测试剂和可操作地连接到身体的第二试剂保持器和分配器，所述第二试剂保持器和分配器包含所述第二炸药检测试剂，并且定位成当所述侧流膜拭子单元连接到所述主体时将所述第二炸药检测试剂输送到所述侧流膜拭子单元。

5. 发明申请

US20090299067A1 New synthesis of 2,6-diamino-3,5-dinitropyrazine-1-oxide from 2,6-diaminopyrazine-1-oxide 审中-公开
标题翻译： 2,6-二氨基吡嗪-1-氧化物新合成2,6-二氨基-3,5-二硝基吡嗪-1-氧化物
公开(公告)号：US20090299067A1
公开(公告)日：2009-12-03
申请号：US12130444
申请日：2008-05-30
申请人： Philip F. Pagoria , Alexander R. Mitchell , Kason Bala
发明人： Philip F. Pagoria , Alexander R. Mitchell , Kason Bala
IPC分类号： C07D241/20
CPC分类号： C07D241/20
摘要： A method for the synthesis of 2,6-Diamino-3,5-dinitropyrazine-1-oxide including nitration of 2,6-diaminopyrazine-1-oxide. The step of nitration may use nitrating agents 20% Oleum/100% HNO3, 100% HNO3 and conc. H2504/100% HNO3 or nitronium tetrfluoraoborate. The synthesis of 2,6-diaminopyrazine-1-oxide may involve both the oxidation of 2,6-diaminopyrazine, the amination of a precursor 2,6-disubstitutedpyrazine-1-oxide or direct formation of the 2,6-diaminopyrazine-l-oxide from the precursor, 2-amino-6-hydroxamino-pyrazine-1-oxide.
摘要翻译：合成2,6-二氨基-3,5-二硝基吡嗪-1-氧化物的方法，包括2,6-二氨基吡嗪-1-氧化物的硝化。硝化步骤可以使用硝化剂20％油/ 100％HNO 3，100％HNO 3和浓度。 H2504 / 100％HNO3或硝基四氟硼酸盐。 2,6-二氨基吡嗪-1-氧化物的合成可能涉及2,6-二氨基吡嗪的氧化，前体2,6-二取代吡嗪-1-氧化物的胺化或直接形成2,6-二氨基吡嗪-1 氧化物，2-氨基-6-羟基 - 吡嗪-1-氧化物。

6. 发明申请

US20110239745A1 Rapid Identification of Explosives Using Thin-Layer Chromatography and Colorimetric Techniques 审中-公开
标题翻译：使用薄层色谱和比色技术快速鉴定炸药
公开(公告)号：US20110239745A1
公开(公告)日：2011-10-06
申请号：US13028072
申请日：2011-02-15
申请人： Joe H. Satcher, JR. , Philip F. Pagoria , Richard E. Whipple , M. Leslie Carman
发明人： Joe H. Satcher, JR. , Philip F. Pagoria , Richard E. Whipple , M. Leslie Carman
IPC分类号： G01N30/02
CPC分类号： G01N30/90 , G01N30/95 , G01N33/22
摘要： A thin-layer chromatography method for identifying material present in a sample on a location including the steps of provide a thin-layer chromatography plate, wetting a swab is with a solvent providing a wetted swab, contacted the location of interest is with the wetted swab to obtain the sample providing a wetted swab with sample, placing the wetted swab with sample in the solvent to dissolve the sample and provide a solvent with sample, dipping a micropipette into the solvent with sample to obtain an amount of the solvent with sample, spotting the amount of the solvent with sample on the thin-layer chromatography plate, allowed the amount of the solvent with sample on the thin-layer chromatography plate to dry providing a thin-layer chromatography plate with sample, placing the a thin-layer chromatography plate with sample into a developing chamber with solvent mixture, allowing the thin-layer chromatography plate with sample to develop producing a developed thin-layer chromatography plate with sample, removing the developed thin-layer chromatography plate with sample from the developing chamber, and illuminating the developed thin-layer chromatography plate with sample with ultra violet light to produce an image for identifying the material present in the sample.
摘要翻译：用于识别样品中存在的位置的薄层色谱法包括提供薄层色谱板，润湿拭子的步骤是用提供湿拭子的溶剂，与感染的位置接触的湿拭子为了获得样品提供湿润的棉签，将带有样品的浸湿棉签放在溶剂中以溶解样品并向样品中提供溶剂，将样品浸入溶剂中以获得一定量的溶剂与样品，点样在薄层色谱板上的样品溶剂量允许在薄层色谱板上的样品溶剂的量干燥，提供具有样品的薄层色谱板，将薄层色谱板将样品放入具有溶剂混合物的显影室中，允许具有样品的薄层色谱板开发生产显影的薄层色谱仪 y板，样品从显影室中取出开发的薄层色谱板，并用紫外光照射显影的薄层色谱板，以产生用于鉴定样品中存在的材料的图像。

7. 发明申请

US20090068065A1 Simple, Field Portable Colorimetric Detection Device For Organic Peroxides and Hydrogen Peroxide 有权
标题翻译：用于有机过氧化物和过氧化氢的简单现场便携式比色检测装置
公开(公告)号：US20090068065A1
公开(公告)日：2009-03-12
申请号：US12183210
申请日：2008-07-31
申请人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman , John G. Reynolds , Peter Nunes , Sharon J. Shields
发明人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman , John G. Reynolds , Peter Nunes , Sharon J. Shields
IPC分类号： G01N21/00 , B23P11/00
CPC分类号： G01N21/78 , G01N31/228 , Y10T29/49826 , Y10T436/206664
摘要： A simple and effective system for the calorimetric determination of organic peroxides and hydrogen peroxide. A peroxide pen utilizing a swipe material attached to a polyethylene tube contains two crushable vials. The two crushable vials contain a calorimetric reagent separated into dry ingredients and liquid ingredients. After swiping a suspected substance or surface the vials are broken, the reagent is mixed thoroughly and the reagent is allowed to wick into the swipe material. The presence of organic peroxides or hydrogen peroxide is confirmed by a deep blue color.
摘要翻译：有机过氧化物和过氧化氢的量热测定的简单而有效的系统。使用连接到聚乙烯管上的滑动材料的过氧化物笔包含两个可压碎的小瓶。两个可压碎的小瓶含有分配成干成分和液体成分的量热试剂。打扫怀疑的物质或表面后，小瓶破裂，将试剂充分混合，使试剂吸入滑动材料。有机过氧化物或过氧化氢的存在通过深蓝色证实。

8. 发明授权

US07057072B2 Synthesis and purification of 1,3,5-triamino-2,4,6-trinitrobenzene (TATB) 失效
标题翻译： 1,3,5-三氨基-2,4,6-三硝基苯（TATB）的合成与纯化
公开(公告)号：US07057072B2
公开(公告)日：2006-06-06
申请号：US10910659
申请日：2004-08-02
申请人： Alexander R. Mitchell , Michael D. Coburn , Gregory S. Lee , Robert D. Schmidt , Philip F. Pagoria , Peter C. Hsu
发明人： Alexander R. Mitchell , Michael D. Coburn , Gregory S. Lee , Robert D. Schmidt , Philip F. Pagoria , Peter C. Hsu
IPC分类号： C07C209/18 , C07C211/50 , C07C209/84
CPC分类号： C06B25/04 , C06B21/0091 , C07C211/52
摘要： A method to convert surplus nitroarene explosives (picric acid, ammonium picrate,) into TATB is described. The process comprises three major steps: conversion of picric acid/ammonium picrate into picramide; conversion of picramide to TATB through vicarious nucleophilic substitution (VNS) of hydrogen chemistry; and purification of TATB.
摘要翻译：描述了将过量的硝基芳烃炸药（苦味酸，苦味酸铵）转化成TATB的方法。该方法包括三个主要步骤：将苦味酸/苦味酸铵转化成草甘膦; 通过氢化学的替代亲核取代（VNS）将picramide转化为TATB; 和TATB的纯化。

9. 发明授权

US5633406A Vicarious nucleophilic substitution using 4-amino-1,2,4-triazole, hydroxylamine or O-alkylhydroxylamine to prepare 1,3-diamino-2,4,6-trinitrobenzene or 1,3,5-triamino-2,4,6-trinitrobenzene 失效
标题翻译：使用4-氨基-1,2,4-三唑，羟胺或O-烷基羟胺代替亲核取代，制备1,3-二氨基-2,4,6-三硝基苯或1,3,5-三氨基-2,4,6 - 二硝基苯
公开(公告)号：US5633406A
公开(公告)日：1997-05-27
申请号：US440024
申请日：1995-05-12
申请人： Alexander R. Mitchell , Philip F. Pagoria , Robert D. Schmidt
发明人： Alexander R. Mitchell , Philip F. Pagoria , Robert D. Schmidt
IPC分类号： C07C209/02
CPC分类号： C07C209/02
摘要： The present invention relates to a process to produce 1,3-diamino-2,4,6-trinitrobenzene (DATB) or 1,3,5-triamino-2,4,6,-trinitrobenzene (TATB) by:(a) reacting at ambient pressure and a temperature of between about 0.degree. and 50.degree. C. for between about 0.1 and 24 hr, a trinitroaromatic compound of structure V: ##STR1## wherein X, Y, and Z are each independently selected from the group consisting of --H and --NH.sub.2, with the proviso that at least 1 or 2 of X, Y, and Z are hydrogen;with an effective amount of 1-amino-1,2,4-triazole, hydroxylamine or O-alkylhydroxamine to produce DATB or TATB;in the presence of a strong base selected from sodium butoxide, potassium butoxide, potassium propoxide, sodium propoxide, sodium ethoxide, potassium ethoxide, sodium methoxide, potassium methoxide, and combinations thereof;in a solvent selected from the group consisting of methanol, ethanol, propanol, butanol, dimethylsulphoxide, N-methylpyrrolidone, hexamethylphosphoramide, dimethylformide, dimethylacetamide and mixtures thereof, provided that when alcohols are present or when hydroxylamine or its O-alkyl derivatives replace ATA primarily DATB is formed; and (b) isolating the DATB or TATB produced. DATB and TATB are important and useful specialty explosives and intermediates for other materials.
摘要翻译：本发明涉及通过以下方法制备1,3-二氨基-2,4,6-三硝基苯（DATB）或1,3,5-三氨基-2,4,6-三硝基苯（TATB）的方法：（a）在环境压力和约0℃至50℃的温度下反应约0.1至24小时，结构V的三硝基芳族化合物：其中X，Y和Z各自独立地选自由-H和-NH2组成的组，条件是X，Y和Z中至少有1或2个是氢; 与有效量的1-氨基-1,2,4-三唑，羟胺或O-烷基羟胺反应生成DATB或TATB; 在选自丁醇钠，丁醇钾，丙醇钾，丙醇钠，乙醇钠，乙醇钾，甲醇钠，甲醇钾及其组合的强碱的存在下，在选自甲醇，乙醇，丙醇，丁醇，二甲基亚砜，N-甲基吡咯烷酮，六甲基磷酰胺，二甲基甲酰胺，二甲基乙酰胺及其混合物的溶剂中，条件是当存在醇时或当羟胺或其O-烷基衍生物主要代替ATA时 DATB形成; 和（b）分离产生的DATB或TATB。 DATB和TATB是其他材料的重要和有用的特种炸药和中间体。

10. 发明授权

US08669115B2 Spot test kit for explosives detection 有权
标题翻译：用于爆炸物检测的现货测试套件
公开(公告)号：US08669115B2
公开(公告)日：2014-03-11
申请号：US12785299
申请日：2010-05-21
申请人： Philip F. Pagoria , Richard E. Whipple , Peter J. Nunes , Joel Del Eckels , John G. Reynolds , Robin R. Miles , Marina L. Chiarappa-Zucca
发明人： Philip F. Pagoria , Richard E. Whipple , Peter J. Nunes , Joel Del Eckels , John G. Reynolds , Robin R. Miles , Marina L. Chiarappa-Zucca
IPC分类号： G01N21/00
CPC分类号： G01N31/22 , B01L3/5023 , B01L3/5029 , B01L2200/16 , B01L2300/0867 , B01L2300/1827 , B01L2300/1877 , B01L2400/0406 , B01L2400/0683 , G01N1/02 , G01N33/227 , G01N2001/022 , G01N2001/028
摘要： An explosion tester system comprising a body, a lateral flow membrane swab unit adapted to be removeably connected to the body, a first explosives detecting reagent, a first reagent holder and dispenser operatively connected to the body, the first reagent holder and dispenser containing the first explosives detecting reagent and positioned to deliver the first explosives detecting reagent to the lateral flow membrane swab unit when the lateral flow membrane swab unit is connected to the body, a second explosives detecting reagent, and a second reagent holder and dispenser operatively connected to the body, the second reagent holder and dispenser containing the second explosives detecting reagent and positioned to deliver the second explosives detecting reagent to the lateral flow membrane swab unit when the lateral flow membrane swab unit is connected to the body.
摘要翻译：一种爆炸测试器系统，包括主体，适于可移除地连接到主体的侧面流动的薄膜拭子单元，第一爆炸物检测试剂，可操作地连接到主体的第一试剂保持器和分配器，第一试剂保持器和分配器包含第一爆炸物检测试剂，并且定位成当侧流膜拭子单元连接到身体时将第一炸药检测试剂输送到侧流膜拭子单元，第二爆炸物检测试剂和可操作地连接到身体的第二试剂保持器和分配器，所述第二试剂保持器和分配器包含所述第二炸药检测试剂，并且定位成当所述侧流膜拭子单元连接到所述主体时将所述第二炸药检测试剂输送到所述侧流膜拭子单元。

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