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1. 发明授权

US06310348B1 Spectroscopic accessory for examining films and coatings on solid surfaces 失效
标题翻译：用于检查固体表面上的膜和涂层的光谱附件
公开(公告)号：US06310348B1
公开(公告)日：2001-10-30
申请号：US09344692
申请日：1999-06-25
申请人： Peter J. Melling , Paul H. Shelley
发明人： Peter J. Melling , Paul H. Shelley
IPC分类号： G01N2101
CPC分类号： G01N21/3563 , G01N21/8422 , G01N2021/3595
摘要： An accessory for an FTIR spectrometer comprises fiber-optic cables connected to a framework within which two mirrors are housed. The mirrors, which are preferably off-axis parabolas, are positionable with respect to each other and with respect to the ends of the fiber-optic cables. The beam from the first cable is reflected by the first mirror onto a sample surface at or near the grazing angle, after which it is captured by the second mirror and focused onto the end of the return cable which transmits it back to the spectrometer. Very thin films and coatings can be spectroscopically detected and characterized using the accessory.
摘要翻译：用于FTIR光谱仪的附件包括连接到框架的光纤电缆，其中容纳两个反射镜。优选离轴抛物线的反射镜可相对于彼此和相对于光纤电缆的端部定位。来自第一缆索的梁在掠角处或附近被第一反射镜反射到样品表面上，然后由第二反射镜捕获并聚焦到将其传送回光谱仪的返回电缆的末端。可以使用附件对非常薄的膜和涂层进行光谱检测和表征。

2. 发明授权

US5170056A Optical fiber coupled devices for remote spectroscopy in the infrared 失效
标题翻译：用于红外线远程光谱的光纤耦合器件
公开(公告)号：US5170056A
公开(公告)日：1992-12-08
申请号：US662281
申请日：1991-02-28
申请人： Joseph R. Berard , Robert J. Burger , Peter J. Melling , William R. Moser
发明人： Joseph R. Berard , Robert J. Burger , Peter J. Melling , William R. Moser
IPC分类号： G01N21/35 , G01N21/55 , G01N21/85
CPC分类号： G01N21/552 , G01N21/8507 , G01N21/35 , G01N21/3504 , G01N21/3563 , G01N21/3577
摘要： The invention is directed to a probe operative in the infrared region of the electromagnetic spectrum for in situ sensing of the absorption of IR energy in a sample. The probe comprises an attenuated total reflection (ATR) element having an input end and an output end for respectively receiving IR and transmitting attenuated IR. The ATR element has wall portions disposed about a central or long axis thereof for reflecting IR energy transverse to the central axis. A bundle of infrared transmitting fibers is located at the input end of the ATR element for transmitting and receiving IR energy into and out of the element. The fibers have end faces proximate the ATR element lying in a plane perpendicular to the central axis.
摘要翻译：本发明涉及在电磁光谱的红外区域中操作的探针，用于原位感测样品中IR能量的吸收。该探头包括衰减的全反射（ATR）元件，其具有用于分别接收IR并发送衰减的IR的输入端和输出端。 ATR元件具有围绕其中心轴或长轴布置的壁部分，用于反射横向于中心轴线的IR能量。一束红外线发射光纤位于ATR元件的输入端，用于发射和接收IR能量进出元件。纤维具有靠近ATR元件的端面，其位于垂直于中心轴线的平面中。

3. 发明授权

US5093095A Crystallization in a force field 失效
标题翻译：力场中的结晶
公开(公告)号：US5093095A
公开(公告)日：1992-03-03
申请号：US233287
申请日：1988-08-17
申请人： David T. Hayhurst , Peter J. Melling , Wha J. Kim
发明人： David T. Hayhurst , Peter J. Melling , Wha J. Kim
IPC分类号： C30B29/34 , C30B7/00 , C30B30/08
CPC分类号： C30B7/00 , C30B29/34 , Y10S423/21 , Y10S423/22 , Y10S423/23 , Y10S423/24 , Y10S423/29 , Y10S423/30 , Y10S423/33
摘要： The production of enhanced crystals is achieved through the use of forces greater than 1 G. This enhanced force technique has wide application to various crystal growth methodologies and produces crystals that are larger, of more uniform size, of better quality, or in higher yields than can be obtained for the same technique using similar times in a 1 G force.
摘要翻译：增强的晶体的生产通过使用大于1G的力来实现。该增强的力技术广泛地应用于各种晶体生长方法，并且产生更大，更均匀的尺寸，更好的质量或更高的产量的晶体可以使用相同的时间在1 G力中获得相同的技术。

4. 发明申请

US20130037719A1 Method for Detecting and Measuring Low Concentrations of Contaminants Using Attenuated Total Reflectance Spectroscopy in the Mid-IR Range 有权
标题翻译：在中红外范围内使用减弱的全反射光谱检测和测量低浓度污染物的方法
公开(公告)号：US20130037719A1
公开(公告)日：2013-02-14
申请号：US13208674
申请日：2011-08-12
申请人： Peter J. Melling , Mary A. Thomson
发明人： Peter J. Melling , Mary A. Thomson
IPC分类号： G01J3/42
CPC分类号： G01N21/3577 , G01N21/552 , G01N21/85
摘要： A spectroscopic method is disclosed for detecting and measuring contaminants in fluids such as water or oil, where the hydrophilicity of the contaminant is substantially different from that of the contaminated fluid. Good calibrations can be obtained at very low concentrations using infrared spectroscopy with ATR crystals that have not been additionally coated or otherwise modified.
摘要翻译：公开了一种用于检测和测量诸如水或油的流体中的污染物的分光方法，其中污染物的亲水性与污染流体的亲水性基本上不同。使用没有另外涂覆或以其他方式修饰的ATR晶体的红外光谱可以在非常低的浓度下获得良好的校准。

5. 发明授权

US5923808A Mid-infrared fiber-optic spectroscopic probe for use at elevated temperatures 失效
标题翻译：在高温下使用的中红外光纤光谱探头
公开(公告)号：US5923808A
公开(公告)日：1999-07-13
申请号：US880691
申请日：1997-06-23
申请人： Peter J. Melling
发明人： Peter J. Melling
IPC分类号： G01N21/55 , G01N21/77 , G02B6/24 , G02B6/36
CPC分类号： G01N21/7703 , G01N21/552 , G02B6/241 , Y10S385/902
摘要： A mid-infrared spectroscopic probe attached to a fiber-optic cable comprises an optically transparent, heat-insulating crystal which is placed between the ATR crystal and the end of the fiber-optic cable so as to provide optical coupling from the cable to the ATR crystal while protecting the fiber-optic assembly inside the cable from excessive heat when the probe is used in high-temperature sample streams. The ATR crystal is tapered outwards towards the sampling end to ensure that pressure from the sample stream, e.g., in a plastics extruder, does not displace the crystal, but rather forces it into tighter contact with the seal in the probe head.
摘要翻译：连接到光纤电缆的中红外光谱探头包括光学透明的绝热晶体，其被放置在ATR晶体和光纤电缆的端部之间，以便提供从电缆到ATR的光耦合晶体，同时当探头用于高温样品流时，保护电缆内的光纤组件免受过热。 ATR晶体向采样端向外锥形，以确保来自样品流的压力例如在塑料挤出机中不会移动晶体，而是迫使其与探头中的密封件紧密接触。

6. 发明授权

US4704299A Process for low temperature curing of sol-gel thin films 失效
标题翻译：溶胶 - 凝胶薄膜的低温固化工艺
公开(公告)号：US4704299A
公开(公告)日：1987-11-03
申请号：US795393
申请日：1985-11-06
申请人： Roy F. Wielonski , Peter J. Melling
发明人： Roy F. Wielonski , Peter J. Melling
IPC分类号： C23C8/36 , C23C26/00 , B05D3/06
CPC分类号： C23C8/36 , C23C26/00
摘要： A process for curing and densifying a sol-gel derived inorganic thin film at lower temperatures (between 10.degree. C. and 400.degree. C.) by applying the films to a substrate, drying the film at a low temperature, exposing the film to a low pressure plasma. The film may be an oxide (e.g. SiO.sub.2), nitride (e.g. Si.sub.3 N.sub.4), oxynitride (e.g. SiO.sub.x N.sub.y) or sulfide (e.g. GeS.sub.2).
摘要翻译：一种在较低温度（10℃至400℃）下将溶胶 - 凝胶衍生的无机薄膜固化并致密化的方法，该方法是通过将膜施加到基底上，在低温下干燥该膜，将该膜暴露于低压等离子体该膜可以是氧化物（例如SiO 2），氮化物（例如Si 3 N 4），氧氮化物（例如SiO x N y）或硫化物（例如GeS 2）。

7. 发明授权

US5198269A Process for making sol-gel deposited ferroelectric thin films insensitive to their substrates 失效
标题翻译：制造对其基材不敏感的溶胶 - 凝胶沉积铁电薄膜的方法
公开(公告)号：US5198269A
公开(公告)日：1993-03-30
申请号：US399724
申请日：1989-08-28
申请人： Scott L. Swartz , Peter J. Melling
发明人： Scott L. Swartz , Peter J. Melling
IPC分类号： C01G23/00 , C01G25/00 , C01G35/00 , C03C17/34 , C04B41/50 , C04B41/52 , C04B41/87 , C04B41/89 , C23C18/04 , C23C18/12 , C30B29/30 , C30B29/32 , H01L21/8242 , H01L27/10 , H01L27/108
CPC分类号： C23C18/04 , C03C17/3417 , C04B41/009 , C04B41/5025 , C04B41/52 , C04B41/87 , C04B41/89 , C23C18/1216 , C23C18/1225 , C23C18/1254 , C04B2111/00405 , C04B2111/90
摘要： A method for producing a thin film of a ferroelectric perovskite material having the steps of providing a first substrate; depositing a first layer of a sol-gel perovskite precursor material wherein the crystallization of this precursor material to the pervoskite phase is insensitive to the first substrate; depositing a second layer of a sol-gel perovskite precursor material wherein the crystallization is sensitive to the first substrate; and heat-treating the deposited layers to form ferroelectric perovskites. A heat treatment step to form perovskites may optionally follow the deposition of the first layer. The first layer of sol-gel perovskite precursor material is selected to produce a perovskite upon heat treatment of: lead titanate (PbTiO.sub.3), or strontium titanate (SrTiO.sub.3). The second layer of sol-gel perovskite precursor material is selected to produce a perovskite upon heat treatment of: lead zirconate titanate (Pb(Zr,Ti)O.sub.3), lead zirconate (PbZrO.sub.3), lead lanthanum titanate ((Pb,La)TiO.sub.3), lead lanthanum zirconate ((Pb,La)ZrO.sub.3), lead lanthanum zirconate titanate ((Pb,La)(Zr,Ti)O.sub.3), lead magnesium niobate (Pb(Mg.sub.1/3 Nb.sub.2/3)O.sub.3), lead zinc niobate (Pb(Zn.sub.1/3 Nb.sub.2/3)O.sub.3), barium titanate (BaTiO.sub.3), strontium barium titanate ((Sr,Ba)TiO.sub.3), barium titanate zirconate (Ba(Ti,Zr)O.sub.3), potassium niobate (KNbO.sub.3), potassium tantalate (KTaO.sub.3), or potassium tantalate niobate (K(Ta,Nb)O.sub.3).
摘要翻译：一种铁电体钙钛矿材料薄膜的制造方法，具有提供第一基板的工序。沉积溶胶 - 凝胶钙钛矿前体材料的第一层，其中该前体材料结晶到渗透相中对第一基底不敏感; 沉积第二层溶胶 - 凝胶钙钛矿前体材料，其中结晶对第一基底敏感; 并对沉积的层进行热处理以形成铁电体钙钛矿。形成钙钛矿的热处理步骤可以任选地遵循第一层的沉积。选择第一层溶胶 - 凝胶钙钛矿前体材料，以便在热处理时产生钛酸铅（PbTiO3）或钛酸锶（SrTiO3）时产生钙钛矿。选择第二层溶胶 - 凝胶钙钛矿前体材料，在热处理后生成钙钛矿：锆钛酸铅（Pb（Zr，Ti）O3），锆酸铅（PbZrO3），铅镧钛酸铅（（Pb，La）TiO3 ），锆酸锆铅（（Pb，La）ZrO 3），锆钛酸铅（（Pb，La）（Zr，Ti）O 3），铌酸铅镁（Pb（Mg1 / 3Nb2 / 3）O3），铌酸铅锌（Pb（Zn1 / 3Nb2 / 3）O3），钛酸钡（BaTiO3），钛酸锶钡（（Sr，Ba）TiO3），钛酸钡（Ba（Ti，Zr）O3），铌酸钾（KNbO3）钽酸钾（KTaO3）或钽酸钾（K（Ta，Nb）O 3）。

8. 发明授权

US4806330A Process for preparing high purity aluminum nitride 失效
标题翻译：制备高纯度氮化铝的方法
公开(公告)号：US4806330A
公开(公告)日：1989-02-21
申请号：US57579
申请日：1987-06-02
申请人： Peter J. Melling , Beebhas C. Mutsuddy , Ibrahim Sekercioglu
发明人： Peter J. Melling , Beebhas C. Mutsuddy , Ibrahim Sekercioglu
IPC分类号： C01B21/072 , C01B21/06
CPC分类号： C01B21/072 , C01P2006/80
摘要： Process for producing high purity aluminum nitride powder by reacting aluminum sulfide with gaseous ammonia at an intermediate temperature (about 700.degree. C.) and holding at that temperature until an intermediate product (Al.sub.x N.sub.y S.sub.z) is formed where x, y, and z are integers; then further heating to a temperature above 1100.degree. C. and reacting with gaseous ammonia. A high purity, low oxygen containing, free flowing powder is produced. A posttreatment using a carbon source such as graphite further reduces the oxygen content. The oxygen content can be further reduced by reacting the aluminum nitride formed with carbon at about 1600.degree. C.
摘要翻译：通过在中等温度（约700℃）下使硫化铝与气态氨反应并保持在该温度下直到形成中间产物（Al x N y S z），其中x，y和z为整数来生产高纯度氮化铝粉末的方法; 然后进一步加热至高于1100℃的温度并与气态氨反应。产生高纯度，低含氧量的自由流动的粉末。使用诸如石墨的碳源的后处理进一步降低氧含量。通过在约1600℃下与碳形成的氮化铝反应，可以进一步降低氧含量。

9. 发明授权

US5754722A Fiber-optic spectroscopic probe with interchangeable sampling heads 失效
标题翻译：具有可互换采样头的光纤光谱探头
公开(公告)号：US5754722A
公开(公告)日：1998-05-19
申请号：US380078
申请日：1995-01-30
申请人： Peter J. Melling
发明人： Peter J. Melling
IPC分类号： G01N21/85 , G02B6/24 , G02B6/04
CPC分类号： G01N21/8507 , G02B6/241 , G01N21/552
摘要： A fiber-optic spectroscopic probe for use with a Fourier Transform Infrared (FTIR) spectrometer for sensing the absorption of infrared energy by a sample has a shaft containing a fiber optic bundle which terminates proximate the end of the shaft for transmitting and receiving infrared energy from the sample being measured by a measuring head. The shaft has means for detachably attaching interchangeable measuring heads for measuring attenuated total reflectance, diffuse or specular reflectance of the sample, or for measuring the infrared energy transmitted through the sample. The interchangeable heads are coupled to the shaft without the use of additional optics or mechanical positioning devices. The shaft assembly may include a cooling jacket for measuring samples at elevated temperatures. Having different, interchangeable spectral sampling heads makes it possible to obtain quantitative spectral data from a wide range of samples in varying states of agglomeration and homogeneity using a single device.
摘要翻译：用于用于感测样品对红外能量的吸收的傅立叶变换红外（FTIR）光谱仪的光纤光谱探测器具有包含光纤束的轴，该光纤束在轴的端部附近终止，用于发射和接收红外能量样品由测量头测量。轴具有用于可拆卸地附接可互换的测量头的装置，用于测量样品的衰减的全反射率，漫反射或镜面反射率，或用于测量透过样品的红外能量。可互换的头部连接到轴上，而不使用附加的光学元件或机械定位装置。轴组件可以包括用于在升高的温度下测量样品的冷却套。具有不同的，可互换的光谱采样头使得可以使用单个装置从变化的聚集状态和均匀性的广泛范围的样品获得定量光谱数据。

10. 发明授权

US5754715A Mid-infrared fiber-optic spectroscopic probe 失效
标题翻译：中红外光纤光谱探头
公开(公告)号：US5754715A
公开(公告)日：1998-05-19
申请号：US747393
申请日：1996-11-12
申请人： Peter J. Melling
发明人： Peter J. Melling
IPC分类号： G01J3/42 , G01N21/35 , G02B6/04 , G02B6/24 , G02B6/00 , G01B9/02
CPC分类号： G01N21/35 , G01J3/42 , G02B6/04 , G01N2021/3595 , G02B6/241
摘要： A fiber-optic spectroscopic probe for use with an FTIR spectrometer comprises two or more types of optical fibers made from materials with overlapping transmissions in the infrared region of the spectrum. The fiber materials are chosen so that so that any regions of low or zero transmission in their respective transmission windows, arising from impurities or defects in the material, occur in different spectral regions, thus ensuring that the probe is able to transmit across the entire transmission window without exhibiting the characteristic "blind spots" that are observed using probes comprising a single type of optical fiber.
摘要翻译：用于FTIR光谱仪的光纤光谱探测器包括由在光谱的红外区域中具有重叠传输的材料制成的两种或更多种类型的光纤。纤维材料被选择为使得在其各自的传输窗口中由材料中的杂质或缺陷产生的低或零透射的任何区域出现在不同的光谱区域中，从而确保探头能够跨越整个传输窗口，而不显示使用包括单一类型的光纤的探针观察到的特征“盲点”。

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