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1. 发明授权

US5419957A Low heat release polymeric composites 失效
标题翻译：低放热聚合物复合材料
公开(公告)号：US5419957A
公开(公告)日：1995-05-30
申请号：US245152
申请日：1994-05-17
申请人： Patrick H. Martin , Peter K. Kim , Stephen E. Bales , Ritchie A. Wessling
发明人： Patrick H. Martin , Peter K. Kim , Stephen E. Bales , Ritchie A. Wessling
IPC分类号： B32B27/08 , C08K7/02 , B32B5/24
CPC分类号： B32B27/08 , C08K7/02 , Y10T428/249962 , Y10T428/249964 , Y10T428/249989
摘要： This invention relates to a low heat release, low density, fiber-reinforced composite comprising a matrix comprising a thermoplastic polymer selected from the group consisting of polyarylsulfone, polyethersulfone, polyetheretherketone, polyetherketoneketone, a copolycarbonate of 4,4'-thiodiphenol and at least one member of the group consisting of bisphenol A, 9,9-bis(4-hydroxyphenyl)fluorene, and 1,1-bis(4-hydroxyphenyl)-1-phenyl ethane, a copolycarbonate of bisphenol A and 9,9-bis(4-hydroxyphenyl)fluorene, 1,1-bis(4-hydroxyphenyl)-1-phenyl ethane polycarbonate, bisphenol A polycarbonate, and polyetherimide, and from about 10 to about 70 percent by weight of the composite of randomly oriented reinforcing fibers, less than 0.5 inch in length, distributed throughout the matrix. The matrix has a void volume of from about 20 to about 90 percent by volume. The composite has a thermoplastic skin layer on each of the major surfaces thereof. A process for making the composite is also disclosed.
摘要翻译：本发明涉及一种低放热，低密度纤维增强复合材料，其包含基质，其包含选自聚芳基砜，聚醚砜，聚醚醚酮，聚醚酮酮，4,4'-硫代二酚的共聚碳酸酯和至少一种由双酚A，9,9-双（4-羟基苯基）芴和1,1-双（4-羟基苯基）-1-苯基乙烷组成的组，双酚A的共聚碳酸酯和9,9-双（ 4-羟基苯基）芴，1,1-双（4-羟基苯基）-1-苯基乙烷聚碳酸酯，双酚A聚碳酸酯和聚醚酰亚胺，和约10至约70重量％的无规取向增强纤维的复合材料长度大于0.5英寸，分布在整个矩阵中。基质具有约20至约90体积％的空隙体积。复合材料在其每个主表面上具有热塑性表层。还公开了制备复合材料的方法。

2. 发明授权

US5490967A Low heat release polymeric composites 失效
标题翻译：低放热聚合物复合材料
公开(公告)号：US5490967A
公开(公告)日：1996-02-13
申请号：US371332
申请日：1995-01-11
申请人： Patrick H. Martin , Stephen E. Bales , Peter K. Kim , Ritchie A. Wessling
发明人： Patrick H. Martin , Stephen E. Bales , Peter K. Kim , Ritchie A. Wessling
IPC分类号： B32B27/08 , C08K7/02 , B32B5/24
CPC分类号： B32B27/08 , C08K7/02 , Y10T428/249962 , Y10T428/249964 , Y10T428/249989
摘要： This invention relates to a low heat release, low density, fiber-reinforced composite comprising a matrix comprising a thermoplastic polymer selected from the group consisting of polyarylsulfone, polyethersulfone, polyetheretherketone, polyetherketoneketone, a copolycarbonate of 4,4'-thiodiphenol and at least one member of the group consisting of bisphenol A, 9,9-bis(4-hydroxyphenyl) fluorene, and 1,1-bis-(4-hydroxyphenyl)-1-phenyl ethane, a copolycarbonate of bisphenol A and 9,9-bis(4-hydroxyphenyl) fluorene, 1,1-bis(4-hydroxyphenyl)-1-phenyl ethane polycarbonate, bisphenol A polycarbonate, and polyetherimide, and from about 10 to about 70 percent by weight of the composite of randomly oriented reinforcing fibers, less than 0.5 inch in length, distributed throughout the matrix. The matrix has a void volume of from about 20 to about 90 percent by volume. The composite has a thermoplastic skin layer on each of the major surfaces thereof. A process for making the composite is also disclosed.
摘要翻译：本发明涉及一种低放热，低密度纤维增强复合材料，其包含基质，其包含选自聚芳基砜，聚醚砜，聚醚醚酮，聚醚酮酮，4,4'-硫代二酚的共聚碳酸酯和至少一种由双酚A，9,9-双（4-羟基苯基）芴和1,1-双 - （4-羟基苯基）-1-苯基乙烷组成的组的成员，双酚A的共聚碳酸酯和9,9-双（4-羟基苯基）芴，1,1-双（4-羟基苯基）-1-苯基乙烷聚碳酸酯，双酚A聚碳酸酯和聚醚酰亚胺，和约10至约70重量％的无规取向增强纤维的复合材料，长度小于0.5英寸，分布在整个矩阵中。基质具有约20至约90体积％的空隙体积。复合材料在其每个主表面上具有热塑性表层。还公开了制备复合材料的方法。

3. 发明授权

US5352272A Gas separations utilizing glassy polymer membranes at sub-ambient temperatures 失效
标题翻译：在低于环境温度下使用玻璃状聚合物膜的气体分离
公开(公告)号：US5352272A
公开(公告)日：1994-10-04
申请号：US930059
申请日：1992-08-13
申请人： David J. Moll , Alan F. Burmester , Thomas C. Young , Kent B. McReynolds , James E. Clark , Charles Z. Hotz , Ritchie A. Wessling , George J. Quarderer , Ronald M. Lacher , Stephen E. Bales , Henry N. Beck , Thomas O. Jeanes , Bethanne L. Smith
发明人： David J. Moll , Alan F. Burmester , Thomas C. Young , Kent B. McReynolds , James E. Clark , Charles Z. Hotz , Ritchie A. Wessling , George J. Quarderer , Ronald M. Lacher , Stephen E. Bales , Henry N. Beck , Thomas O. Jeanes , Bethanne L. Smith
IPC分类号： B01D53/22 , B01D53/26 , B01D63/00 , B01D69/02 , B01D71/48 , B01D71/50 , B01D71/52 , B01D71/62 , B01D71/64 , B01D71/66 , B01D71/72 , C01B13/02 , C01B21/04 , C08G64/10 , C08G75/06 , C08G75/26 , C08L67/00 , C08L67/03 , C08L69/00 , C08L71/12
CPC分类号： B01D71/48 , B01D53/22 , B01D53/228 , B01D53/268 , B01D69/02 , B01D71/50 , B01D71/52 , B01D71/62 , B01D71/64 , B01D71/66 , B01D71/72 , C01B13/0251 , C01B21/0444 , C08G64/10 , C08G75/06 , C08G75/26 , C08L71/12 , C01B2210/0046 , C01B2210/0062 , Y02P20/129
摘要： This invention relates to a method of and apparatus for separating component gases in a gas mixture employing a glassy polymer membrane at temperatures of 5.degree. C. or less so as to achieve superior separation of gas components.
摘要翻译：本发明涉及一种在5℃或更低的温度下使用玻璃状聚合物膜分离气体混合物中的组分气体的方法和装置，以实现气体组分的优异分离。

4. 发明授权

US5837032A Gas separations utilizing glassy polymer membranes at sub-ambient temperatures 失效
标题翻译：在低于环境温度下使用玻璃状聚合物膜的气体分离
公开(公告)号：US5837032A
公开(公告)日：1998-11-17
申请号：US382032
申请日：1995-02-10
申请人： David J. Moll , Alan F. Burmester , Thomas C. Young , Kent B. McReynolds , James E. Clark , Charles Z. Hotz , Ritchie A. Wessling , George J. Quarderer , Ronald M. Lacher , Thomas O. Jeanes , Henry N. Beck , Stephen E. Bales , Bethanne L. Smith
发明人： David J. Moll , Alan F. Burmester , Thomas C. Young , Kent B. McReynolds , James E. Clark , Charles Z. Hotz , Ritchie A. Wessling , George J. Quarderer , Ronald M. Lacher , Thomas O. Jeanes , Henry N. Beck , Stephen E. Bales , Bethanne L. Smith
IPC分类号： B01D53/22 , B01D53/26 , B01D69/02 , B01D71/48 , B01D71/50 , B01D71/52 , B01D71/62 , B01D71/64 , B01D71/66 , B01D71/72 , C01B13/02 , C01B21/04 , C08G64/10 , C08G75/06 , C08G75/26 , C08L71/12
CPC分类号： C01B13/0251 , B01D53/22 , B01D53/228 , B01D53/268 , B01D69/02 , B01D71/48 , B01D71/50 , B01D71/52 , B01D71/62 , B01D71/64 , B01D71/66 , B01D71/72 , C01B21/0444 , C08G64/10 , C08G75/06 , C08G75/26 , C08L71/12 , C01B2210/0046 , C01B2210/0062
摘要： This invention relates to a method of an apparatus and method for separating component gases in a gas mixture employing a glassy polymer membrane at temperatures at or slightly above the freezing point of any liquid present so as to achieve superior separator of gas components. The composition of certain monomers and polymers are claimed.
摘要翻译： PCT No.PCT / US93 / 07696 Sec。 371日期1995年2月10日 102（e）1995年2月10日PCT PCT 1993年8月13日PCT公布。出版物WO94 / 04250 日本特开1994年3月3日本发明涉及一种使用玻璃状聚合物膜在气体混合物中分离组分气体的装置和方法的方法，所述气体混合物在存在的任何液体的冰点处或稍高于所存在的任何液体的冰点处，以便获得优异的气体分离器组件。要求某些单体和聚合物的组成。

5. 发明授权

US5679133A Gas separations utilizing glassy polymer membranes at sub-ambient temperatures 失效
标题翻译：在低于环境温度下使用玻璃状聚合物膜的气体分离
公开(公告)号：US5679133A
公开(公告)日：1997-10-21
申请号：US292771
申请日：1994-08-18
申请人： David J. Moll , Alan F. Burmester , Thomas C. Young , Kent B. McReynolds , James E. Clark , Charles Z. Hotz , Ritchie A. Wessling , George J. Quarderer , Ronald M. Lacher , Stephen E. Bales , Henry Nelson Beck , Thomas O. Jeanes , Bethanne L. Smith
发明人： David J. Moll , Alan F. Burmester , Thomas C. Young , Kent B. McReynolds , James E. Clark , Charles Z. Hotz , Ritchie A. Wessling , George J. Quarderer , Ronald M. Lacher , Stephen E. Bales , Henry Nelson Beck , Thomas O. Jeanes , Bethanne L. Smith
IPC分类号： B01D53/22 , B01D53/26 , B01D63/00 , B01D69/02 , B01D71/48 , B01D71/50 , B01D71/52 , B01D71/62 , B01D71/64 , B01D71/66 , B01D71/72 , C01B13/02 , C01B21/04 , C08G64/10 , C08G75/06 , C08G75/26 , C08L67/00 , C08L67/03 , C08L69/00 , C08L71/12
CPC分类号： B01D71/48 , B01D53/22 , B01D53/228 , B01D53/268 , B01D69/02 , B01D71/50 , B01D71/52 , B01D71/62 , B01D71/64 , B01D71/66 , B01D71/72 , C01B13/0251 , C01B21/0444 , C08G64/10 , C08G75/06 , C08G75/26 , C08L71/12 , C01B2210/0046 , C01B2210/0062 , Y02P20/129
摘要： This invention relates to a method of and apparatus for separating component gases in a gas mixture employing a glassy polymer membrane at temperatures of 5.degree. C. or less so as to achieve superior separation of gas components.
摘要翻译：本发明涉及一种在5℃或更低的温度下使用玻璃状聚合物膜分离气体混合物中的组分气体的方法和装置，以实现气体组分的优异分离。

6. 发明授权

US5516877A Crosslinkable carbonate polymers of dihydroxyaryl fluorene 失效
标题翻译：二羟基芳基芴的交联碳酸酯聚合物
公开(公告)号：US5516877A
公开(公告)日：1996-05-14
申请号：US291211
申请日：1994-08-16
申请人： Stephen E. Bales , James P. Godschalx , Philip C. Yang , Matthew T. Bishop , Maurice J. Marks
发明人： Stephen E. Bales , James P. Godschalx , Philip C. Yang , Matthew T. Bishop , Maurice J. Marks
IPC分类号： C08G64/14 , C08G64/00
CPC分类号： C08G64/14
摘要： There are disclosed carbonate polymers of dihydroxyaryl fluorene having crosslinkable moieties. There are also disclosed such polymers in the form of composites. The polymers of this invention are capable of being crosslinked by activation of the crosslinkable moieties. Once crosslinked, these polymers demonstrate an excellent combination of properties including resistance to melting at high temperatures, solvent resistance, optical clarity, impact resistance, and physical strength.
摘要翻译：公开了具有可交联部分的二羟基芳基芴的碳酸酯聚合物。还公开了复合材料形式的这种聚合物。本发明的聚合物能够通过可交联部分的活化而交联。一旦交联，这些聚合物表现出包括耐高温熔融性，耐溶剂性，光学透明度，耐冲击性和物理强度的优异的组合。

7. 发明授权

US5045610A Blend of copolyestercarbonate polymer derived from diaryl dicarboxylic acid 失效
标题翻译：由二芳基二羧酸衍生的共聚酯碳酸酯聚合物的共混物
公开(公告)号：US5045610A
公开(公告)日：1991-09-03
申请号：US401213
申请日：1989-08-31
申请人： Stephen E. Bales , Kenneth A. Burdett , Guo-Shuh J. Lee
发明人： Stephen E. Bales , Kenneth A. Burdett , Guo-Shuh J. Lee
IPC分类号： C08G63/64 , C08L69/00 , C08L101/00
CPC分类号： C08L69/005 , C08G63/64 , C08L101/00
摘要： This invention relates to copolyestercarbonate polymers which are prepared with diaryl dicarboxylic acid compounds, particularly biphenyldicarboxylic acid compounds. Such copolyestercarbonate polymers show good physical properties including high glass transition temperatures and low ultraviolet radiation sensitivity. The thermoplastic copolymestercarbonates can be used to prepare films or molded articles or blended with other thermoplastic resins to give thermoplastic polymer blends for molding purposes.
摘要翻译：本发明涉及用二芳基二羧酸化合物，特别是联苯二羧酸化合物制备的共聚酯碳酸酯聚合物。这种共聚酯碳酸酯聚合物显示出良好的物理性质，包括高玻璃化转变温度和低紫外线辐射敏感性。热塑性共聚酯碳酸酯可用于制备膜或模塑制品或与其它热塑性树脂共混以得到用于模制目的的热塑性聚合物共混物。

8. 发明授权

US4388455A Process for preparing ester carbonate copolymers 失效
标题翻译：制备碳酸酯共聚物的方法
公开(公告)号：US4388455A
公开(公告)日：1983-06-14
申请号：US378693
申请日：1982-05-17
申请人： Stephen E. Bales
发明人： Stephen E. Bales
IPC分类号： C08G63/00 , C08G63/20 , C08G63/64 , C08G64/20
CPC分类号： C08G63/64
摘要： Ordered ester/carbonate copolymers having improved properties at higher solids are provided by (1) contacting a dihydric organic compound such as bisphenol-A with a diacid halide such as terephthaloyl chloride and a carbonate precursor such as phosgene under conditions sufficient to form an ester/carbonate oligomer and (2) contacting the oligomer with additional carbonate precursor to produce the desired ordered ester/carbonate copolymer.
摘要翻译：通过（1）在足以形成酯/酯的条件下使二羟基有机化合物如双酚A与二酰卤如对苯二甲酰氯和碳酸酯前体例如光气接触来提供在较高固体下具有改进性能的有序酯/碳酸酯共聚物，碳酸酯低聚物和（2）使低聚物与另外的碳酸酯前体接触以产生所需的有序酯/碳酸酯共聚物。

9. 发明授权

US4840646A Tetrabromo bisphenol based polyestercarbonate membranes and method of using 失效
标题翻译：四溴双酚基聚碳酸酯膜及其使用方法
公开(公告)号：US4840646A
公开(公告)日：1989-06-20
申请号：US221483
申请日：1988-07-19
申请人： Joginder N. Anand , Stephen E. Bales , Darrell C. Feay , Thomas O. Jeanes
发明人： Joginder N. Anand , Stephen E. Bales , Darrell C. Feay , Thomas O. Jeanes
IPC分类号： B01D53/22 , B01D71/48 , B01D71/50 , C08G63/682
CPC分类号： C08G63/682 , B01D53/22 , B01D71/48 , B01D71/50
摘要： The invention is a membrane comprising a dense skin of a polyestercarbonate, wherein the diphenolic residue in the backbone of the polyestercarbonate is a tetrabromo diphenolic residue, wherein the membrane has a separation factor for oxygen and nitrogen of 6.5 or greater at about 24.degree. C. In another aspect, the invention is a method of separating oxygen from a mixture of gases comprising nitrogen and oxygen, wherein the method comprises (a) contacting the gas mixture with a thin, non-porous membrane comprising a polyestercarbonate described hereinbefore under conditions such that the oxygen selectively permeates through the membrane to the other side of the membrane; and (b) removing the permeated oxygen from the other side of the membrane, wherein separation factor for the oxygen and nitrogen is 6.5 or greater at about 24.degree. C. The membranes of this invention demonstrate surprisingly high separation factors for oxygen and nitrogen separations. The membranes of this invention have good mechanical properties and therefore are useful under more extreme conditions, for example temperature and pressure, than many commercially used membranes.
摘要翻译：本发明是一种包含聚酯碳酸酯致密表皮的膜，其中聚酯碳酸酯主链中的二酚残基是四溴二酚残基，其中该膜在约24℃下具有6.5或更高的氧和氮分离因子。在另一方面，本发明是从包含氮和氧的气体混合物中分离氧的方法，其中所述方法包括（a）使气体混合物与包含上述聚酯碳酸酯的薄的非多孔膜接触，条件是使得氧选择性地渗透膜到膜的另一侧; 和（b）从膜的另一侧除去渗透的氧气，其中在约24℃下氧和氮的分离因子为6.5或更大。本发明的膜表现出惊人的高分离因子用于氧气和氮气的分离。本发明的膜具有良好的机械性能，因此在许多商业使用的膜的更极端条件下，例如温度和压力下是有用的。

10. 发明授权

US4330662A Ordered copolyestercarbonate resins 失效
标题翻译：有序共聚酯碳酸酯树脂
公开(公告)号：US4330662A
公开(公告)日：1982-05-18
申请号：US200759
申请日：1980-10-27
申请人： Stephen E. Bales
发明人： Stephen E. Bales
IPC分类号： C08G63/00 , C08G63/64 , C08G63/12
CPC分类号： C08G63/64
摘要： Ordered copolyestercarbonate resins having repeating units of the formula: ##STR1## wherein a portion of R.sup.1 is meta-phenylene and a portion of R.sub.1 is para-phenylene and R is independently an aromatic hydrocarbylene or inertly substituted aromatic hydrocarbylene, e.g., ##STR2## exhibit physical properties such as heat resistance, clarity and impact strength that are superior to the comparable properties of corresponding random copolymers. They exhibit melt processability that is superior to the melt processability of corresponding copolyestercarbonates wherein R.sup.1 is entirely para-phenylene. They exhibit heat resistance, notch sensitivity and low temperature impact resistance that are superior to comparable properties of corresponding copolyestercarbonates wherein R.sup.1 is entirely meta-phenylene. Such resins are useful for making transparent tough films and molded articles having high heat resistance.
摘要翻译：具有下式重复单元的有序共聚酯碳酸酯树脂：其中R1的一部分是间亚苯基，R 1的一部分是对亚苯基，R独立地是芳族亚烃基或惰性取代的芳族亚烃基，例如，诸如耐热性，透明度和冲击强度的物理性能优于相应无规共聚物的可比性能。它们表现出优于相应的共聚酯碳酸酯的熔融加工性的熔融加工性，其中R1是完全对亚苯基。它们表现出耐热性，切口灵敏度和耐低温冲击性，其优于相应的共聚酯碳酸酯的性能，其中R1完全是间 - 亚苯基。这种树脂可用于制造具有高耐热性的透明韧性薄膜和模制品。

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