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1. 发明授权

US5837032A Gas separations utilizing glassy polymer membranes at sub-ambient temperatures 失效
标题翻译：在低于环境温度下使用玻璃状聚合物膜的气体分离
公开(公告)号：US5837032A
公开(公告)日：1998-11-17
申请号：US382032
申请日：1995-02-10
申请人： David J. Moll , Alan F. Burmester , Thomas C. Young , Kent B. McReynolds , James E. Clark , Charles Z. Hotz , Ritchie A. Wessling , George J. Quarderer , Ronald M. Lacher , Thomas O. Jeanes , Henry N. Beck , Stephen E. Bales , Bethanne L. Smith
发明人： David J. Moll , Alan F. Burmester , Thomas C. Young , Kent B. McReynolds , James E. Clark , Charles Z. Hotz , Ritchie A. Wessling , George J. Quarderer , Ronald M. Lacher , Thomas O. Jeanes , Henry N. Beck , Stephen E. Bales , Bethanne L. Smith
IPC分类号： B01D53/22 , B01D53/26 , B01D69/02 , B01D71/48 , B01D71/50 , B01D71/52 , B01D71/62 , B01D71/64 , B01D71/66 , B01D71/72 , C01B13/02 , C01B21/04 , C08G64/10 , C08G75/06 , C08G75/26 , C08L71/12
CPC分类号： C01B13/0251 , B01D53/22 , B01D53/228 , B01D53/268 , B01D69/02 , B01D71/48 , B01D71/50 , B01D71/52 , B01D71/62 , B01D71/64 , B01D71/66 , B01D71/72 , C01B21/0444 , C08G64/10 , C08G75/06 , C08G75/26 , C08L71/12 , C01B2210/0046 , C01B2210/0062
摘要： This invention relates to a method of an apparatus and method for separating component gases in a gas mixture employing a glassy polymer membrane at temperatures at or slightly above the freezing point of any liquid present so as to achieve superior separator of gas components. The composition of certain monomers and polymers are claimed.
摘要翻译： PCT No.PCT / US93 / 07696 Sec。 371日期1995年2月10日 102（e）1995年2月10日PCT PCT 1993年8月13日PCT公布。出版物WO94 / 04250 日本特开1994年3月3日本发明涉及一种使用玻璃状聚合物膜在气体混合物中分离组分气体的装置和方法的方法，所述气体混合物在存在的任何液体的冰点处或稍高于所存在的任何液体的冰点处，以便获得优异的气体分离器组件。要求某些单体和聚合物的组成。

2. 发明授权

US5246647A Process of making microporous hollow fiber or film membrane of poly(phenylene sulfide) (PPS) 失效
标题翻译：制造聚苯硫醚（PPS）的微孔中空纤维或膜膜的方法
公开(公告)号：US5246647A
公开(公告)日：1993-09-21
申请号：US746756
申请日：1991-08-19
申请人： Henry N. Beck , Robert D. Mahoney , Hawk S. Wan , Chieh-Chun Chau , Timothy M. Finney , Ritchie A. Wessling , Jiro Kawamoto , Mark F. Sonnenschein
发明人： Henry N. Beck , Robert D. Mahoney , Hawk S. Wan , Chieh-Chun Chau , Timothy M. Finney , Ritchie A. Wessling , Jiro Kawamoto , Mark F. Sonnenschein
IPC分类号： B01D53/22 , B01D67/00 , B01D71/66 , C08J3/09 , C08J9/26 , C08J9/28 , D01F6/76
CPC分类号： B01D53/228 , B01D67/0018 , B01D67/0027 , B01D67/003 , B01D71/66 , C08J3/091 , C08J9/26 , C08J9/28 , D01F6/765 , B01D2323/22 , C08J2201/046 , C08J2201/052 , C08J2381/02
摘要： The present invention relates to a process for preparing a microporous permselective membrane from a poly(phenylene sulfide) (PPS) polymer, an organic compound which substantially solubilizes the PPS below its melting point to form a homogenous mixture, heating the resulting mixture, extruding or casting the mixture into a membrane (fiber or film), quenching or coagulating the membrane, and leaching the membrane, while optionally drawing the membrane before, during, after leaching, or a combination thereof. In one embodiment, the solvent optionally includes an organic non-solvent to assist in obtaining the desired microporsity. The permselective polymers are useful to separate gaseous or liquid components from a mixture of components.
摘要翻译：本发明涉及一种由聚（苯硫醚）（PPS）聚合物制备微孔渗透选择膜的方法，该有机化合物基本上将PPS溶解在其熔点以下以形成均匀混合物，加热得到的混合物，挤出或将混合物浇注到膜（纤维或膜）中，淬火或凝结膜并浸出膜，同时任选地在浸出之前，浸出期间，浸出后或其组合时拉伸膜。在一个实施方案中，溶剂任选地包括有机非溶剂以帮助获得所需的微孔性。选择性聚合物可用于从组分混合物中分离气态或液体组分。

3. 发明授权

US5064580A Process for making microporous membranes from poly(etheretherketone)-type polymers 失效
标题翻译：由聚（醚醚酮）型聚合物制备微孔膜的方法
公开(公告)号：US5064580A
公开(公告)日：1991-11-12
申请号：US380058
申请日：1989-07-14
申请人： Henry N. Beck , Richard A. Lundgard , Robert D. Mahoney
发明人： Henry N. Beck , Richard A. Lundgard , Robert D. Mahoney
IPC分类号： B01D67/00 , B01D69/08 , B01D71/52 , C08J3/09 , C08J5/18 , C08J9/28 , C08L71/08 , C08L71/10 , D01D5/24 , D01D5/247 , D01F6/66
CPC分类号： D01F6/665 , B01D67/0009 , B01D67/0027 , B01D67/003 , B01D69/02 , B01D69/08 , B01D69/081 , B01D69/085 , B01D69/088 , B01D71/52 , C08J3/091 , C08J5/18 , C08J9/28 , D01D5/24 , D01D5/247 , B01D2323/08 , B01D2323/12 , C08J2201/052 , C08J2371/00
摘要： A method of preparing a microporous membrane from unsulfonated poly(etheretherketone)-type polymers.
摘要翻译：从未磺化的聚（醚醚酮）型聚合物制备微孔膜的方法。

4. 发明授权

US4772392A Process for preparing POWADIR membranes from tetrahalobisphenol A polycarbonates 失效
标题翻译：从四卤双酚A聚碳酸酯制备POWADIR膜的方法
公开(公告)号：US4772392A
公开(公告)日：1988-09-20
申请号：US118119
申请日：1987-11-06
申请人： Edgar S. Sanders, Jr. , Daniel O. Clark , John A. Jensvold , Henry N. Beck , G. Glenn Lipscomb, II , Frederick L. Coan
发明人： Edgar S. Sanders, Jr. , Daniel O. Clark , John A. Jensvold , Henry N. Beck , G. Glenn Lipscomb, II , Frederick L. Coan
IPC分类号： B01D67/00 , B01D69/02 , B01D69/08 , B01D71/50 , C01B3/50 , C01B13/02 , C08G64/10 , B01D13/01
CPC分类号： B01D67/0009 , B01D69/02 , B01D69/08 , B01D69/087 , B01D71/50 , C01B13/0255 , C01B3/503 , C08G64/10 , B01D2323/08 , B01D2323/12 , B01D2325/022 , C01B2203/0405 , C01B2203/048 , C01B2210/0046 , Y10S264/48
摘要： The invention is a process for the preparation of a POWADIR membrane comprising bisphenol-based polycarbonates wherein at least 25 percent by weight of the bisphenol moieties are tetrahalogenated wherein the halogen is Cl or Br, and the membrane prepared by such process. The process generally comprises: forming a mixture comprising (i) a bisphenol-based polycarbonate wherein at least 25 percent by weight of the bisphenol moieties are tetrahalogenated, wherein the halogen is Cl or Br, (ii) a solvent for such polycarbonate, and (iii) a non-solvent for such polycarbonate, wherein the mixture has a sufficient viscosity to allow extrusion at temperatures at which the mixture is homogeneous; heating the mixture to a temperature at which the mixture is a homogeneous fluid and extrudable; extruding the heated mixture into a shape suitable for membrane use; passing the formed membrane through a quench zone wherein the mixture undergoes phase separation, and the major portion of the solvent and non-solvent are removed from the formed membrane; wherein the membrane formed is a POWADIR membrane with a discriminating region capable of separating oxygen from nitrogen.
摘要翻译：本发明是一种制备包含双酚基聚碳酸酯的POWADIR膜的方法，其中至少25重量％的双酚部分是四卤化的，其中卤素是Cl或Br，以及通过这种方法制备的膜。该方法通常包括：形成混合物，其包含（i）双酚基聚碳酸酯，其中至少25重量％的双酚部分是四卤代的，其中卤素是Cl或Br，（ii）这种聚碳酸酯的溶剂和（ iii）用于这种聚碳酸酯的非溶剂，其中混合物具有足够的粘度以允许在混合物均匀的温度下挤出; 将混合物加热到混合物是均匀流体并可挤出的温度; 将加热的混合物挤出成适于膜使用的形状; 将形成的膜通过骤冷区，其中混合物经历相分离，并且从形成的膜中除去主要部分的溶剂和非溶剂; 其中所形成的膜是具有能够将氮与氮分离的鉴别区的POWADIR膜。

5. 发明授权

US4980101A Anisotropic microporous syndiotactic polystyrene membranes and a process for preparing the same 失效
标题翻译：各向异性微孔间同立构聚苯乙烯膜及其制备方法
公开(公告)号：US4980101A
公开(公告)日：1990-12-25
申请号：US381432
申请日：1989-07-14
申请人： Henry N. Beck , Robert D. Mahoney , Hawk S. Wan , Richard A. Lundgard
发明人： Henry N. Beck , Robert D. Mahoney , Hawk S. Wan , Richard A. Lundgard
IPC分类号： B01D67/00 , B01D71/28
CPC分类号： B01D71/28 , B01D67/0009 , B01D67/0011 , B01D67/0027 , B01D67/003 , B01D67/0083 , B01D69/088 , B01D2323/12
摘要： This invention relates to semi-permeable anisotropic syndiotatic polystyrene microporous membranes and a process for preparing such membranes.
摘要翻译：本发明涉及半渗各向异性间同聚苯乙烯微孔膜及其制备方法。

6. 发明授权

US4962131A Composition useful in process for preparing powadir membranes from tetrahalobisphenol a polycarbonates 失效
标题翻译：用于从四卤双酚聚碳酸酯制备powadir膜的方法中的组合物
公开(公告)号：US4962131A
公开(公告)日：1990-10-09
申请号：US118141
申请日：1987-11-06
申请人： Henry N. Beck , Edgar S. Sanders, Jr. , G. Glenn Lipscomb, II
发明人： Henry N. Beck , Edgar S. Sanders, Jr. , G. Glenn Lipscomb, II
IPC分类号： B01D53/22 , C01B13/02 , C08G64/10
CPC分类号： C08G64/10 , B01D53/22 , C01B13/0255 , C01B2210/0046
摘要： The invention is a composition useful for the preparation of POWADIR membranes of a bisphenol-based polycarbonate wherein at least 25 percent by weight of the bisphenol moieties are tetrahalogenated, wherein the halogen is Cl or Br, the composition comprising (i) a bisphenol-based polycarbonate wherein at least 25 percent by weight of the bisphenol moieties are tetrahalogenated, wherein the halogen is Cl or Br, (ii) a solvent for such polycarbonate, and (iii) a non-solvent for such polycarbonate. The composition is useful for extruding membranes wherein the membranes formed are POWADIR membranes with a discriminating region capable of separating oxygen from nitrogen.The composition of this invention allows the formation of membranes with excellent physical properties, good separation factors for oxygen and nitrogen, with excellent fluxes.
摘要翻译：本发明是一种可用于制备双酚基聚碳酸酯的POWADIR膜的组合物，其中至少25重量％的双酚部分是四卤化的，其中卤素是Cl或Br，组合物包含（i）双酚基聚碳酸酯，其中至少25重量％的双酚部分是四卤代的，其中卤素是Cl或Br，（ii）这种聚碳酸酯的溶剂，和（iii）这种聚碳酸酯的非溶剂。该组合物可用于挤出膜，其中形成的膜是具有能够从氮分离氧的鉴别区的POWADIR膜。本发明的组合物允许形成具有优异物理性能，良好的氧和氮分离因子的膜，具有优异的通量。

7. 发明授权

US5071917A High strength fibers of stereoregular polystrene 失效
标题翻译：立体定向聚苯乙烯的高强度纤维
公开(公告)号：US5071917A
公开(公告)日：1991-12-10
申请号：US569492
申请日：1990-08-20
申请人： David R. Pederson , Peter E. Pierini , Henry N. Beck , Mark J. Semer
发明人： David R. Pederson , Peter E. Pierini , Henry N. Beck , Mark J. Semer
IPC分类号： D01F6/22
CPC分类号： D01F6/22
摘要： The invention is a crystalline fiber comprising syndiotactic polystyrene, or a mixture. Preferably the fiber is a high strength fiber isotactic polystyrene and syndiotactic polystyrene wherein the fiber is monoaxially oriented, has a tensile strength of about 10,000 psi or greater, and a modulus of about 1,000,000 psi or greater.In another aspect the invention is a process for the preparation of fibers of syndiotactic polystyrene, or a mixture of isotactic polystyrene and syndiotactic polystyrene which comprises:A. contacting syndiotactic polystyrene, or a mixture of isotactic polystyrene and syndiotactic polystyrene with a solvent for the polystyrene at elevated temperatures under conditions such that a homogenous solution is formed which has sufficient viscosity to be extruded;B. extruding the solution through an orifice to form a fiber at elevated temperatures;C. quenching the fiber by passing the fiber through one or more zones under conditions such that the fiber solidifies;D. removing the solvent for the polystyrene from the fiber; andE. cooling the fiber to ambient temperature.In the embodiment where it is desirable to prepare high strength fibers, the fibers are further exposed to the following process steps:F. heating the fiber to a temperature above the glass transition temperature of the polystyrene;G. redrawing the fiber to elongate the fiber, maximize crystallinity, and induce monoaxial orientation of the polystyrene in the fiber.
摘要翻译：本发明是包含间同立构聚苯乙烯或混合物的结晶纤维。优选地，纤维是高强度纤维全同立构聚苯乙烯和间同立构聚苯乙烯，其中纤维是单轴取向的，具有约10,000psi或更大的拉伸强度和约1,000,000psi或更大的模量。另一方面，本发明是制备间同立构聚苯乙烯纤维或全同立构聚苯乙烯与间同立构聚苯乙烯的混合物的方法，其包括：A.将间同立构聚苯乙烯或全同立构聚苯乙烯与间同立构聚苯乙烯的混合物与聚苯乙烯溶剂在升高的温度下，在形成具有足够的待挤出粘度的均匀溶液的条件下， B.通过孔口挤出溶液以在升高的温度下形成纤维; C.通过在纤维固化的条件下使纤维通过一个或多个区域淬火纤维; D.从纤维中去除聚苯乙烯的溶剂; 和E.将纤维冷却至环境温度。在需要制备高强度纤维的实施方案中，纤维进一步暴露于以下工艺步骤：F.将纤维加热到高于聚苯乙烯的玻璃化转变温度的温度; G.重新拉伸纤维以拉长纤维，使结晶度最大化，并诱导纤维中聚苯乙烯的单轴取向。

8. 发明授权

US5057600A Process for forming an article comprising poly(etheretherketone) (PEEK) type polymers 失效
标题翻译：用于形成包含聚（醚醚酮）（PEEK）型聚合物的制品的方法
公开(公告)号：US5057600A
公开(公告)日：1991-10-15
申请号：US107699
申请日：1987-10-09
申请人： Henry N. Beck , Richard A. Lundgard
发明人： Henry N. Beck , Richard A. Lundgard
IPC分类号： C08J3/09
CPC分类号： C08J3/091 , C08J2371/00
摘要： The present invention relates to a process for the production of an article comprising a polymer itself comprising poly(etheretherketone), which process comprises:A. contacting poly(etheretherketone) with at least one organic compound, consisting essentially of carbon and hydrogen, and optionally oxygen, nitrogen, sulfur, halogen, or mixtures thereof having a molecular weight of between about 160 and 450 daltons and having at least one six membered aromatic ring structure, which compound is stable at a temperature of between 240.degree. and 400.degree. C. at ambient pressure, at a temperature of between about 240.degree. and 400.degree. C. at ambient pressure for a time effective to dissolve greater than about 10 percent by weight of the poly(etheretherketone) present;B. forming the solution of poly(etheretherketone) and solvent of step (A) into a desired article configuration;C. removing the solvent; andD. recovering the article comprising poly(etheretherketone) formed thereby. PEEK is a useful material for articles needing high temperature and solvent resistant properties. PEEK is also useful in the formation of membranes, hollow fibers and solid fibers which are porous, permeable, semipermeable or selectively permeable.
摘要翻译：本发明涉及制备包含聚合物本身的制品的方法，该聚合物本身包含聚（醚醚酮），该方法包括：A.将聚（醚醚酮）与至少一种基本上由碳和氢组成的有机化合物和任选地氧，氮，硫，卤素或其混合物，其分子量为约160至450道尔顿且具有至少一个六元芳族环结构，该化合物在240-400℃的温度下是稳定的环境压力，在约240-400℃的温度下，在环境压力下，有效地溶解存在的聚（醚醚酮）的大于约10重量％的时间; B.将步骤（A）的聚（醚醚）溶剂和溶剂形成所需的制品构型; C.除去溶剂; 和D.回收包含由其形成的聚（醚醚酮）的制品。 PEEK是需要耐高温和耐溶剂性能的物品的有用材料。 PEEK也可用于形成多孔，可渗透，半渗透或选择性渗透的膜，中空纤维和固体纤维。

9. 发明授权

US5015275A Isotropic microporous syndiotactic polystyrene membranes and processes for preparing the same 失效
标题翻译：各向同性微孔间同立构聚苯乙烯膜及其制备方法
公开(公告)号：US5015275A
公开(公告)日：1991-05-14
申请号：US380227
申请日：1989-07-14
申请人： Henry N. Beck , Robert D. Mahoney , Hawk S. Wan , Richard A. Lundgard
发明人： Henry N. Beck , Robert D. Mahoney , Hawk S. Wan , Richard A. Lundgard
IPC分类号： B01D67/00 , B01D71/28
CPC分类号： B01D71/28 , B01D67/0009 , B01D67/0027 , B01D67/003 , B01D2323/08 , B01D2323/12 , B01D2325/02
摘要： This invention relates to semi-permeable isotropic syndiotactic polystyrene microporous membranes and processes for preparing such membranes.
摘要翻译：本发明涉及半渗各向同性间同立构聚苯乙烯微孔膜及其制备方法。

10. 发明授权

US4976901A Microporous membranes from isotactic polystyrene and syndiotactic polystyrene 失效
标题翻译：来自全同立构聚苯乙烯和间同立构聚苯乙烯的微孔膜
公开(公告)号：US4976901A
公开(公告)日：1990-12-11
申请号：US477363
申请日：1990-02-08
申请人： Henry N. Beck , Robert D. Mahoney
发明人： Henry N. Beck , Robert D. Mahoney
IPC分类号： B01D67/00 , B01D71/28
CPC分类号： B01D71/28 , B01D67/0009 , B01D67/0011 , B01D67/0016 , B01D67/0027 , B01D67/003 , B01D2323/08 , B01D2323/12 , B01D2325/20
摘要： This invention relates to novel semi-permeable isotropic or anisotropic microporous membranes fabricated from a mixture of isotactic polystyrene and syndiotactic polystyrene and a method of producing such membranes.
摘要翻译：本发明涉及由全同立构聚苯乙烯和间同立构聚苯乙烯的混合物制备的新型半渗各向同性或各向异性微孔膜及其制备方法。

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