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1. 发明申请

US20120149551A1 TWO-LAYER CATALYST, PROCESS FOR PREPARING SAME AND USE FOR THE MANUFACTURE OF NANOTUBES 审中-公开
标题翻译：两层催化剂，其制备方法和用于制备纳米管的方法
公开(公告)号：US20120149551A1
公开(公告)日：2012-06-14
申请号：US13391100
申请日：2010-08-16
申请人： Patrice Gaillard , Serge Bordere , Philippe Serp , Brigitte Caussat , Julien Beausoleil
发明人： Patrice Gaillard , Serge Bordere , Philippe Serp , Brigitte Caussat , Julien Beausoleil
IPC分类号： D01F9/127 , B01J23/881 , B01J21/04 , B01J21/18 , B01J21/08 , B01J21/06 , B01J29/04 , D01F9/12 , H01B1/24 , B01J23/85 , B01J21/10 , B82Y30/00 , B82B1/00 , B82B3/00
CPC分类号： B01J37/0244 , B01J21/04 , B01J23/85 , B01J23/881 , B01J35/023 , B01J37/0205 , B82Y30/00 , B82Y40/00 , C01B32/162
摘要： A catalyst material for preparing nanotubes, especially carbon nanotubes, said material being in the form of solid particles, said particles including a porous substrate supporting two superposed catalytic layers, a first layer, directly positioned on the substrate, including at least one transition metal from column VIB of the Periodic Table, preferably molybdenum, and a second catalytic layer, positioned on the first layer, comprising iron. Also, a process for preparing same and to a process for the synthesis of nanotubes using this catalyst material.
摘要翻译：一种用于制备纳米管，特别是碳纳米管的催化剂材料，所述材料为固体颗粒的形式，所述颗粒包括支撑两个重叠的催化层的多孔基材，直接位于基材上的第一层，包括至少一种过渡金属周期表的VIB柱，优选钼，以及位于第一层上的第二催化剂层，包含铁。另外，其制备方法和使用该催化剂材料合成纳米管的方法。

2. 发明申请

US20110123429A1 Process for Producing Carbon Nanotubes from Renewable Raw Materials 审中-公开
标题翻译：从可再生原料生产碳纳米管的工艺
公开(公告)号：US20110123429A1
公开(公告)日：2011-05-26
申请号：US13017601
申请日：2011-01-31
申请人： Serge Bordere , Daniel Cochard , Eric Dutilh , Patrice Gaillard , André Lozowski , Dominique Plee
发明人： Serge Bordere , Daniel Cochard , Eric Dutilh , Patrice Gaillard , André Lozowski , Dominique Plee
IPC分类号： D01F9/12 , B82Y30/00 , B82Y40/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/162
摘要： A subject of the present invention is a process for producing carbon nanotubes, the process comprising: a) the synthesis of alcohol(s) by fermentation of at least one vegetable matter and optionally the purification of the product obtained; b) the dehydration of the alcohol or alcohols obtained in a) in order to produce, in a first reactor, a mixture of alkene(s) and water and optionally the purification of the product obtained; c) the introduction, in particular the introduction into a fluidized bed, in a second reactor, of a powdery catalyst at a temperature ranging from 450 to 850° C., this catalyst comprising at least one catalytic metal supported by an inert solid substrate, the grains of catalyst having a d50 of less than 300 μm; d) bringing the alkene produced in b) into contact with the powdery catalyst of stage c), optionally in a fluidized bed, in order to form carbon nanotubes and hydrogen on the surface of said catalyst by catalytic decomposition of said alkene; e) the recovery of the carbon nanotubes produced in d). The invention also relates to nanotubes capable of being obtained according to the abovementioned process, which can be advantageously used in all the known fields of application of carbon nanotubes.
摘要翻译：本发明的主题是一种生产碳纳米管的方法，该方法包括：a）通过至少一种植物物质的发酵和任选的所得产物的纯化来合成醇; b）在a）中获得的醇或醇的脱水，以便在第一反应器中产生烯烃和水的混合物，并任选地纯化获得的产物; c）引入，特别是在第二反应器中引入粉末状催化剂在450-850℃的温度下引入流化床，该催化剂包含至少一种由惰性固体基质负载的催化金属， d50小于300μm的催化剂颗粒; d）使b）中产生的烯烃与阶段c）的粉末催化剂任选地在流化床中接触，以便通过所述烯烃的催化分解在所述催化剂的表面上形成碳纳米管和氢; e）在d）中生产的碳纳米管的回收。本发明还涉及能够根据上述方法获得的纳米管，其可有利地用于所有已知的碳纳米管应用领域。

3. 发明申请

US20090134363A1 METHOD FOR SYNTHESIS OF CARBON NANOTUBES 失效
标题翻译：合成碳纳米管的方法
公开(公告)号：US20090134363A1
公开(公告)日：2009-05-28
申请号：US12158436
申请日：2006-12-22
申请人： Serge Bordere , Patrice Gaillard , Carole Baddour
发明人： Serge Bordere , Patrice Gaillard , Carole Baddour
IPC分类号： D01F9/12 , C08K3/04 , H01B1/24 , B01J19/00 , B82B1/00 , B82B3/00
CPC分类号： H01C17/0652 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/30 , C01P2004/03 , C01P2004/13 , C01P2004/50 , C08K3/04 , C09C1/48 , C09C1/56 , C09D5/24 , C09D7/61 , C09D7/69 , H01G9/058 , H01G11/36 , Y02E60/13
摘要： The invention relates to a method for synthesis of carbon nanotubes of the highest carbon purity by the process of vapour phase chemical deposition. The nanotubes produced can be used to advantage in all know applications of carbon nanotubes.
摘要翻译：本发明涉及一种通过气相化学沉积方法合成具有最高碳纯度的碳纳米管的方法。所生产的纳米管可用于碳纳米管的所有知识应用中。

4. 发明申请

US20090008610A1 PROCESS FOR PRODUCING CARBON NANOTUBES FROM RENEWABLE RAW MATERIALS 有权
标题翻译：从可再生原料生产碳纳米管的方法
公开(公告)号：US20090008610A1
公开(公告)日：2009-01-08
申请号：US12062687
申请日：2008-04-04
申请人： Serge Bordere , Daniel Cochard , Eric Dutilh , Patrice Gaillard , Andre Lozowski , Dominique Plee
发明人： Serge Bordere , Daniel Cochard , Eric Dutilh , Patrice Gaillard , Andre Lozowski , Dominique Plee
IPC分类号： D01F9/12 , H01B1/24
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/162
摘要： A subject of the present invention is a process for producing carbon nanotubes, the process comprising: a) the synthesis of alcohol(s) by fermentation of at least one vegetable matter and optionally the purification of the product obtained; b) the dehydration of the alcohol or alcohols obtained in a) in order to produce, in a first reactor, a mixture of alkene(s) and water and optionally the purification of the product obtained; c) the introduction, in particular the introduction into a fluidized bed, in a second reactor, of a powdery catalyst at a temperature ranging from 450 to 850° C., this catalyst comprising at least one catalytic metal supported by an inert solid substrate, the grains of catalyst having a d50 of less than 300 μm; d) bringing the alkene produced in b) into contact with the powdery catalyst of stage c), optionally in a fluidized bed, in order to form carbon nanotubes and hydrogen on the surface of said catalyst by catalytic decomposition of said alkene; e) the recovery of the carbon nanotubes produced in d). The invention also relates to nanotubes capable of being obtained according to the abovementioned process, which can be advantageously used in all the known fields of application of carbon nanotubes.
摘要翻译：本发明的主题是一种生产碳纳米管的方法，该方法包括：a）通过至少一种植物物质的发酵和任选的所得产物的纯化来合成醇; b）在a）中获得的醇或醇的脱水，以便在第一反应器中产生烯烃和水的混合物，并任选地纯化获得的产物; c）引入，特别是在第二反应器中引入粉末状催化剂在450-850℃的温度下引入流化床，该催化剂包含至少一种由惰性固体基质负载的催化金属， d50小于300μm的催化剂颗粒; d）使b）中产生的烯烃与阶段c）的粉末催化剂任选地在流化床中接触，以便通过所述烯烃的催化分解在所述催化剂的表面上形成碳纳米管和氢; e）在d）中生产的碳纳米管的回收。本发明还涉及能够根据上述方法获得的纳米管，其可有利地用于所有已知的碳纳米管应用领域。

5. 发明授权

US08911701B2 Process for fabricating carbon nanotubes and apparatus for implementing the process 有权
标题翻译：制造碳纳米管的方法和用于实施该方法的装置
公开(公告)号：US08911701B2
公开(公告)日：2014-12-16
申请号：US13424784
申请日：2012-03-20
申请人： Patrice Gaillard , Serge Bordere
发明人： Patrice Gaillard , Serge Bordere
IPC分类号： C07B31/00 , C01B31/02 , B82Y30/00 , B82Y40/00
CPC分类号： C01B31/024 , B82Y30/00 , B82Y40/00 , C01B32/164 , Y10S977/843
摘要： An industrial process and an apparatus for fabricating carbon nanotubes (CNTs) is provided, comprising synthesis of the carbon nanotubes by decomposing a carbon source brought into contact, in a fluidized-bed reactor, whereby the carbon nanotubes synthesized in the reactor and fixed onto the grains of catalytic substrate in the form of an entangled three-dimensional network, forming agglomerates constituting the CNT powder, are recovered sequentially by discharging them while hot, that is to say at the reaction temperature for synthesizing the CNTs, at the foot of the reactor, the sequence in which the discharges are carried out corresponding to the frequency of filling of the reactor.
摘要翻译：提供了一种用于制造碳纳米管（CNT）的工业方法和装置，其包括通过在流化床反应器中分解接触的碳源来合成碳纳米管，由此将在反应器中合成的碳纳米管固定在形成构成CNT粉末的聚集体的缠结三维网络形式的催化底物颗粒通过在反应器底部的热，即在合成CNT的反应温度下排出，依次回收，对应于反应堆的填充频率进行排放的顺序。

6. 发明申请

US20080135816A1 Method For Synthesis Of Carbon Nanotubes 有权
标题翻译：碳纳米管的合成方法
公开(公告)号：US20080135816A1
公开(公告)日：2008-06-12
申请号：US11814811
申请日：2006-02-03
申请人： Serge Bordere , Daniel Cochard , Eric Duthilh , Patrice Gaillard , Dominique Plee
发明人： Serge Bordere , Daniel Cochard , Eric Duthilh , Patrice Gaillard , Dominique Plee
IPC分类号： D01F9/12 , H01B1/06 , C08K3/04
CPC分类号： B01J8/24 , B01J21/04 , B01J23/745 , B01J35/006 , B01J35/023 , B01J35/10 , B01J35/1019 , B01J35/108 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , C01B2202/06 , C30B7/00 , C30B7/005 , C30B29/605
摘要： The present invention relates to a process for preparing CNTs by bringing a carbon source into contact with a multivalent metal and/or metal-oxide-based catalyst deposited on an inorganic substrate having a BET specific surface area of greater than 50 m2/g.The CNTs obtained may be used as agents for improving the mechanical and electrical conductivity properties in polymeric compositions.
摘要翻译：本发明涉及通过使碳源与沉积在BET比表面积大于50m 2的无机基材上的多价金属和/或金属氧化物系催化剂接触来制备CNT的方法 / g。所获得的CNT可以用作改善聚合物组合物中机械和电导率性能的试剂。

7. 发明申请

US20090194189A1 METHOD FOR SAFE FILLING WITH CARBON NANOTUBES, FILLING SYSTEM AND INDUSTRIAL PLANT EMPLOYING THIS METHOD 有权
标题翻译：使用碳纳米管进行安全填充的方法，填充系统和使用本方法的工业设备
公开(公告)号：US20090194189A1
公开(公告)日：2009-08-06
申请号：US12361652
申请日：2009-01-29
申请人： Serge Bordere , Patrice Gaillard
发明人： Serge Bordere , Patrice Gaillard
IPC分类号： B65B1/04 , B65B1/16 , B65B1/30 , B65B57/00
CPC分类号： B65B1/16 , B65B1/28 , B65G69/182 , B65G69/183 , Y10T137/87925
摘要： The invention relates to a method for filling a receptacle (200) with carbon nanotubes from another receptacle (106) whereby the CNTs are passed from one receptacle to the other by means of a coupling (300) comprising a double-valve device (30), each valve being coupled to one of the receptacles, the valves (31, 32) closing independently and tightly and being openable only when they are coupled to one another.
摘要翻译：本发明涉及一种用于从另一容器（106）向碳纳米管填充容器（200）的方法，由此通过包括双阀装置（30）的联接器（300）使CNT从一个容器传递到另一容器，每个阀联接到所述容器之一，所述阀（31,32）独立且紧密地封闭，并且只有当它们彼此联接时才可打开。

8. 发明授权

US08561652B2 Method for safe filling with carbon nanotubes, filling system and industrial plant employing this method 有权
标题翻译：采用这种方法安全填充碳纳米管，灌装系统和工厂的方法
公开(公告)号：US08561652B2
公开(公告)日：2013-10-22
申请号：US12361652
申请日：2009-01-29
申请人： Serge Bordere , Patrice Gaillard
发明人： Serge Bordere , Patrice Gaillard
IPC分类号： B65B1/04 , F16L37/28
CPC分类号： B65B1/16 , B65B1/28 , B65G69/182 , B65G69/183 , Y10T137/87925
摘要： The invention relates to a method for filling a receptacle (200) with carbon nanotubes from another receptacle (106) whereby the CNTs are passed from one receptacle to the other by means of a coupling (300) comprising a double-valve device (30), each valve being coupled to one of the receptacles, the valves (31, 32) closing independently and tightly and being openable only when they are coupled to one another.
摘要翻译：本发明涉及一种用于从另一容器（106）向碳纳米管填充容器（200）的方法，由此通过包括双阀装置（30）的联接器（300）使CNT从一个容器传递到另一容器，每个阀联接到所述容器之一，所述阀（31,32）独立且紧密地封闭，并且只有当它们彼此联接时才可打开。

9. 发明申请

US20110121241A1 Process for Producing Carbon Nanotubes from Renewable Raw Materials 审中-公开
公开(公告)号：US20110121241A1
公开(公告)日：2011-05-26
申请号：US13017594
申请日：2011-01-31
申请人： Serge Bordere , Daniel Cochard , Eric Dutilh , Patrice Gaillard , André Lozowski , Dominique Plee
发明人： Serge Bordere , Daniel Cochard , Eric Dutilh , Patrice Gaillard , André Lozowski , Dominique Plee
IPC分类号： H01B1/04 , D01F9/12 , B82Y30/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/162
摘要： A subject of the present invention is a process for producing carbon nanotubes, the process comprising: a) the synthesis of alcohol(s) by fermentation of at least one vegetable matter and optionally the purification of the product obtained; b) the dehydration of the alcohol or alcohols obtained in a) in order to produce, in a first reactor, a mixture of alkene(s) and water and optionally the purification of the product obtained; c) the introduction, in particular the introduction into a fluidized bed, in a second reactor, of a powdery catalyst at a temperature ranging from 450 to 850° C., this catalyst comprising at least one catalytic metal supported by an inert solid substrate, the grains of catalyst having a d50 of less than 300 μm; d) bringing the alkene produced in b) into contact with the powdery catalyst of stage c), optionally in a fluidized bed, in order to form carbon nanotubes and hydrogen on the surface of said catalyst by catalytic decomposition of said alkene; e) the recovery of the carbon nanotubes produced in d). The invention also relates to nanotubes capable of being obtained according to the abovementioned process, which can be advantageously used in all the known fields of application of carbon nanotubes.

10. 发明授权

US07622059B2 Method for synthesis of carbon nanotubes 失效
标题翻译：合成碳纳米管的方法
公开(公告)号：US07622059B2
公开(公告)日：2009-11-24
申请号：US12158436
申请日：2006-12-22
申请人： Serge Bordere , Patrice Gaillard , Carole Baddour
发明人： Serge Bordere , Patrice Gaillard , Carole Baddour
IPC分类号： H01B1/04 , C01B31/02
CPC分类号： H01C17/0652 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/30 , C01P2004/03 , C01P2004/13 , C01P2004/50 , C08K3/04 , C09C1/48 , C09C1/56 , C09D5/24 , C09D7/61 , C09D7/69 , H01G9/058 , H01G11/36 , Y02E60/13
摘要： The invention relates to a method for synthesis of carbon nanotubes of the highest carbon purity by the process of vapour phase chemical deposition. The nanotubes produced can be used to advantage in all know applications of carbon nanotubes.
摘要翻译：本发明涉及一种通过气相化学沉积方法合成具有最高碳纯度的碳纳米管的方法。所生产的纳米管可用于碳纳米管的所有知识应用中。

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