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1. 发明授权

US3974211A Method of manufacturing methallyl sulfonate 失效
标题翻译：甲代烯丙基磺酸盐的制备方法
公开(公告)号：US3974211A
公开(公告)日：1976-08-10
申请号：US539413
申请日：1975-01-08
申请人： Osamu Okumura , Katsumi Yaguchi , Ikuo Adachi , Masuzo Nagayama
发明人： Osamu Okumura , Katsumi Yaguchi , Ikuo Adachi , Masuzo Nagayama
IPC分类号： G01S1/32 , C07C143/16
CPC分类号： C07C309/00
摘要： A method of manufacturing methallyl sulfonate, which comprises: forming a sulfur trioxide-dialkyl sulfoxide complex by effecting reaction between sulfur trioxide and dialkyl sulfoxide as mixed at the ratio of more than 0.8 mol of the latter to 1 mol of the former in the presence of an inert solvent; effecting reaction between said complex and isobutylene, in an amount of 0.9-1.2 mols of isobutylene per 1 mol of sulfur trioxide, by applying a temperature in the range of 10.degree.-80.degree.C; and neutralizing the reaction product with a base.
摘要翻译：一种制备甲代烯丙基磺酸盐的方法，其包括：通过在三氧化硫和二烷基亚砜之间的反应中形成三氧化硫 - 二烷基亚砜络合物，所述三氧化硫和二烷基亚砜在后者的比例大于0.8摩尔与前者的摩尔比为1摩尔的情况下，惰性溶剂; 通过施加10〜80℃的温度，使所述络合物和异丁烯之间的反应以每1摩尔三氧化硫0.9-1.2摩尔的异丁烯的量进行反应; 并用碱中和反应产物。

2. 发明授权

US3951877A Heavy-duty granular detergent composition with sodium citrate builder 失效
标题翻译：具有柠檬酸钠助洗剂的重型颗粒洗涤剂组合物
公开(公告)号：US3951877A
公开(公告)日：1976-04-20
申请号：US378922
申请日：1973-07-13
申请人： Osamu Okumura , Kazuo Ohbu , Mitsuharu Kachi , Masuzo Nagayama
发明人： Osamu Okumura , Kazuo Ohbu , Mitsuharu Kachi , Masuzo Nagayama
IPC分类号： B01J2/28 , C11D1/02 , C11D3/02 , C11D3/20 , C11D3/08 , C11D1/14 , C11D1/22 , C11D3/04
CPC分类号： C11D17/06 , C11D1/02 , C11D3/046 , C11D3/2086
摘要： A heavy-duty granular detergent composition consisting of 10 to 60 wt. percent of sodium citrate, 5 to 40 wt. percent of non-soap anionic surfactants, 0.1 to 10 wt. percent of inorganic aluminum salts and additives for use in conventional detergents, the weight ratio of the citrate to the surfactants being 1/5 to 10/1.
摘要翻译：一种重垢颗粒洗涤剂组合物，其由10至60wt。柠檬酸钠的百分比为5〜40wt。百分比的非皂阴离子表面活性剂，0.1-10重量％百分比的用于常规洗涤剂的无机铝盐和添加剂，柠檬酸盐与表面活性剂的重量比为1/5至10/1。

3. 发明授权

US3969375A Method of manufacturing salt of .alpha.-sulfofatty acid ester 失效
标题翻译：制备{60-磺基酸酯的盐的方法
公开(公告)号：US3969375A
公开(公告)日：1976-07-13
申请号：US524709
申请日：1974-11-18
申请人： Osamu Okumura , Takenobu Sakatani , Kazuo Ohbu , Masuzo Nagayama
发明人： Osamu Okumura , Takenobu Sakatani , Kazuo Ohbu , Masuzo Nagayama
IPC分类号： C07C67/00 , C07C301/00 , C07C303/06 , C07C303/32 , C07C309/17 , C11D1/28 , C07C143/12
CPC分类号： C07C303/06
摘要： A neutralized product containing salt of .alpha.-sulfofatty acid ester in high concentration can be produced by the method comprising the steps of (1) sulfonating fatty acid ester by contacting a gaseous mixture of sulfur trioxide (SO.sub.3) and an inert gas containing 1 - 15% by volume of SO.sub.3 with a film of a fatty acid ester, said ester having the formula RCH.sub.2 COOR' (wherein R is alkyl having 8 - 18 carbon atoms and R' is alkyl having 1 - 5 carbon atoms), under the conditions that the molar ratio of SO.sub.3 to said fatty acid ester is in the range of 1.0 - 1.5, the temperature is in the range of 50.degree. - 85.degree.C and the time of contact is in the range of 0.5 - 30 seconds; (2) contacting a film of the reaction product obtained by step (1) into contact with said gaseous mixture, under the conditions of a temperature in the range of 95 - 150.degree.C and a time of contact in the range of 3 - 120 seconds; and (3) instantly neutralizing the reaction product obtained by step (2) with a base selected from the group consisting of an aqueous solution of alkali metal hydroxide, ammonia water and ethanol amine while retaining the condition that the pH value is in the range of 6 - 10 and the temperature is less than 70.degree.C. This neutralized product is usable as the active ingredient a detergent without subjecting it to any further treatment.
摘要翻译：含有高浓度的α-磺基脂肪酸酯的中和产物可以通过以下方法制备：（1）通过使三氧化硫（SO 3）和含有1-15的惰性气体的气体混合物脂肪酸酯膜的SO 3体积％，所述具有式RCH 2 COOR'的酯（其中R是具有8-18个碳原子的烷基，R'是具有1-5个碳原子的烷基），在 SO 3与所述脂肪酸酯的摩尔比在1.0-1.5的范围内，温度在50-85℃的范围内，接触时间在0.5-30秒的范围内; （2）使步骤（1）获得的反应产物的膜与所述气体混合物接触，在95-150℃的温度和3〜120℃范围内的接触时间秒; 和（3）用碱金属氢氧化物水溶液，氨水和乙醇胺立即中和由步骤（2）获得的反应产物与碱金属氢氧化物，氨水和乙醇胺的水溶液，同时保持pH值在 6-10，温度低于70℃。该中和产物可用作活性成分，不用进行任何进一步的处理。

4. 发明授权

US3974194A Method of separating cobalt catalyst from a liquid polyol ester product 失效
标题翻译：从液体多元醇酯产物中分离钴催化剂的方法
公开(公告)号：US3974194A
公开(公告)日：1976-08-10
申请号：US510590
申请日：1974-09-30
申请人： Hiroshi Isa , Takeo Inagaki , Yasuhiro Kiyonaga , Masuzo Nagayama
发明人： Hiroshi Isa , Takeo Inagaki , Yasuhiro Kiyonaga , Masuzo Nagayama
IPC分类号： C07C69/24 , B01J23/94 , B01J31/40 , B01J38/00 , C07B61/00 , C07C67/38 , C07C69/28 , C07C69/30 , C07C69/33 , C09F5/08
CPC分类号： B01J31/0244 , B01J23/94 , B01J31/20 , B01J31/403 , C07C67/38 , C07C67/54 , B01J2231/321 , B01J2531/0208 , B01J2531/845 , B01J31/04 , Y02P20/584
摘要： In the method of manufacturing liquid polyol esters of carboxylic acid by making an olefin having 3 or more carbon atoms, carbon monoxide and polyhydric alcohol react with one another in the presence of a cobalt compound catalyst, the steps comprising heating the thus reacted mixture to distill out unreacted olefin and so forth, thereafter cooling the distillation residue and separating it into the ester of polyhydric alcohol and the cobalt compound.
摘要翻译：在通过制备具有3个或更多个碳原子的烯烃制备羧酸的液体多元醇酯的方法中，一氧化碳和多元醇在钴化合物催化剂的存在下彼此反应，步骤包括将如此反应的混合物加热至蒸馏除去未反应的烯烃等，然后冷却蒸馏残渣并将其分离成多元醇和钴化合物的酯。

5. 发明授权

US3947507A Method of producing liquid olefin polymer 失效
标题翻译：制备液态烯烃聚合物的方法
公开(公告)号：US3947507A
公开(公告)日：1976-03-30
申请号：US446017
申请日：1974-02-26
申请人： Hiroshi Isa , Hiroshi Mandai , Toshiyuki Ukigai , Anri Tominaga , Ryozo Taniyasu , Masuzo Nagayama
发明人： Hiroshi Isa , Hiroshi Mandai , Toshiyuki Ukigai , Anri Tominaga , Ryozo Taniyasu , Masuzo Nagayama
IPC分类号： C07C2/30 , C08F4/16 , C08F10/00 , C07C3/18 , C07C3/21
CPC分类号： C07C2/30 , C08F10/00 , C07C2527/08 , C07C2527/125 , C07C2527/126 , C07C2527/135 , C07C2531/12 , C07C2531/26
摘要： A method for producing a liquid olefin polymer which comprises polymerizing an .alpha.-olefin having 6 - 14 carbon atoms or mixtures thereof, in the presence of a catalyst consisting of an alkali metal hydride, a halide of an element selected from boron and aluminum and a titanium halide, or a catalyst in which metallic lithium or sodium is added to those catalyst ingredients.
摘要翻译：一种制备液体烯烃聚合物的方法，其包括在由碱金属氢化物，选自硼和铝的元素的卤化物和选自硼和铝的催化剂的存在下，将具有6-14个碳原子的α-烯烃或其混合物聚合，卤化钛或其中向这些催化剂成分中加入金属锂或钠的催化剂。

6. 发明授权

US3953361A Method of manufacturing granular solid catalyst 失效
标题翻译：颗粒状固体催化剂的制备方法
公开(公告)号：US3953361A
公开(公告)日：1976-04-27
申请号：US527644
申请日：1974-11-27
申请人： Hiroshi Isa , Toshiyuki Ukigai , Anry Tominaga , Ryozo Taniyasu , Masuzo Nagayama
发明人： Hiroshi Isa , Toshiyuki Ukigai , Anry Tominaga , Ryozo Taniyasu , Masuzo Nagayama
IPC分类号： B01J31/22 , B01J37/04 , C07B61/00 , C07C1/00 , C07C2/22 , C07C2/32 , C07C11/02 , C07C67/00 , C08F4/00 , C08F4/06 , C08F4/12 , C08F10/00 , B01J31/02
CPC分类号： B01J31/2208 , B01J31/2291 , B01J37/04 , C07C2/22 , C08F10/00 , B01J2231/12 , B01J2531/31 , B01J27/125 , B01J31/26 , C07C2527/125 , C07C2527/126 , C07C2531/02 , C07C2531/26
摘要： A method of manufacturing granular solid catalyst, comprising the process of mixing more than 1 mole of olefin and 1.0 - 1.2 mole of ketone having 4 or more carbon atoms relative to 1 mole of aluminum halide and effecting reaction at a temperature of more than 60.degree.C.
摘要翻译：一种制备粒状固体催化剂的方法，包括相对于1摩尔铝卤化物混合大于1摩尔烯烃和1.0-1.2摩尔具有4个或更多个碳原子的酮的方法，并在大于60℃的温度下进行反应 C。

7. 发明授权

US3946055A Method of manufacturing carboxylic acid or ester thereof 失效
标题翻译：制备羧酸或其酯的方法
公开(公告)号：US3946055A
公开(公告)日：1976-03-23
申请号：US510732
申请日：1974-09-30
申请人： Hiroshi Isa , Takeo Inagaki , Yasuhiro Kiyonaga , Masuzo Nagayama
发明人： Hiroshi Isa , Takeo Inagaki , Yasuhiro Kiyonaga , Masuzo Nagayama
IPC分类号： C07C69/22 , B01J23/00 , B01J31/00 , C07B61/00 , C07C51/00 , C07C51/14 , C07C53/00 , C07C53/126 , C07C67/00 , C07C67/38 , C07C69/017 , C11C3/02 , C11C1/00
CPC分类号： C07C51/14 , C07C67/38
摘要： In the method of manufacturing carboxylic acids or esters thereof by reacting olefin, carbon monoxide and alcohol or water in the presence of catalyst prepared in advance by heating a cobalt compound and pyridine or at least one pyridine base selected from the group of mono-, di- and tri-alkyl (having 1.about.3 carbon atoms)-substituted pyridines under the pressure of carbon monoxide.
摘要翻译：在通过在预先通过加热钴化合物和吡啶或至少一种选自单，二，二的吡啶碱的催化剂存在下，使烯烃，一氧化碳和醇或水反应来制造羧酸或其酯的方法中， - 和三烷基（具有1个差异3个碳原子） - 取代的吡啶在一氧化碳的压力下。

8. 发明授权

US4031158A Method for preparation of polyolefin oil 失效
标题翻译：聚烯烃油的制备方法
公开(公告)号：US4031158A
公开(公告)日：1977-06-21
申请号：US707614
申请日：1976-07-22
申请人： Hiroshi Isa , Toshiyuki Ukigai , Anri Tominaga , Ryozo Taniyasu , Masuzo Nagayama
发明人： Hiroshi Isa , Toshiyuki Ukigai , Anri Tominaga , Ryozo Taniyasu , Masuzo Nagayama
IPC分类号： C08F4/00 , C07C1/00 , C07C2/22 , C07C11/02 , C07C67/00 , C08F4/06 , C08F10/00 , C08F10/14 , C10M107/10 , C10N30/02 , C10N40/08 , C10N40/12 , C10N40/25 , C10N60/02 , C07C3/18
CPC分类号： C08F10/14
摘要： A method of preparing a polyolefin oil in the present invention comprises polymerizing an olefin having 6 or more carbon atoms in the presence of a mixture of a polyhydric alcohol derivative and an aluminum halide, said derivative being obtained by replacing hydrogen atoms of all the hydroxyl groups of the polyhydric alcohol by alkyl groups having 1-20 carbon atoms. The thus prepared polyolefin oil scarcely contains halogen, and it has a wide range of use such as, for instance, a lubricant, a cosmetic base, a textile finishing agent, etc.
摘要翻译：在本发明中制备聚烯烃油的方法包括在多元醇衍生物和卤化铝的混合物的存在下聚合具有6个或更多个碳原子的烯烃，所述衍生物是通过取代所有羟基的氢原子的多元醇通过具有1-20个碳原子的烷基。由此制备的聚烯烃油几乎不含有卤素，并且具有广泛的用途，例如润滑剂，化妆品基质，纺织整理剂等。

9. 发明授权

US3952071A Method for preparation of olefin oligomer 失效
标题翻译：烯烃低聚物的制备方法
公开(公告)号：US3952071A
公开(公告)日：1976-04-20
申请号：US538965
申请日：1975-01-06
申请人： Hiroshi Isa , Toshiyuki Ukigai , Anri Tominaga , Ryozo Taniyasu , Masuzo Nagayama
发明人： Hiroshi Isa , Toshiyuki Ukigai , Anri Tominaga , Ryozo Taniyasu , Masuzo Nagayama
IPC分类号： C08F4/00 , A61K8/30 , A61K8/72 , A61K8/81 , A61K9/06 , B01J31/00 , C07B61/00 , C07C1/00 , C07C2/22 , C07C11/02 , C07C67/00 , C08F4/06 , C08F10/00 , C08F10/14 , C07C3/18
CPC分类号： C07C2/22 , C08F10/00 , C07C2527/125 , C07C2527/126 , C07C2531/02
摘要： An olefin oligomer having a low viscosity and a high viscosity index can be prepared by polymerizing an olefin having 6 or more carbon atoms in the presence of a mixture of a polyhydric alcohol derivative and an aluminum halide, said derivative being obtained by replacing the hydrogen atoms of all the hydroxyl groups of the polyhydric alcohol by either acyl groups exclusively or by acyl group and alkyl groups both of said groups having 1 - 20 carbon atoms. The thus prepared olefin oligomer scarcely contains halogen, and it has a wide range of uses such as, for instance, a lubricant, a cosmetic base, etc.
摘要翻译：具有低粘度和高粘度指数的烯烃低聚物可以通过在多元醇衍生物和卤化铝的混合物存在下聚合具有6个或更多个碳原子的烯烃来制备，所述衍生物是通过将氢原子的多羟基醇的所有羟基通过酰基独立地或通过酰基和烷基，所述基团都具有1-20个碳原子。如此制备的烯烃低聚物几乎不含有卤素，并且具有广泛的用途，例如润滑剂，化妆品基料等。

10. 发明授权

US3947509A Method for preparation of hydrocarbon liquid polymers 失效
标题翻译：烃类液体聚合物的制备方法
公开(公告)号：US3947509A
公开(公告)日：1976-03-30
申请号：US549864
申请日：1975-02-14
申请人： Hiroshi Isa , Toshiyuki Ukigai , Anri Tominaga , Ryozo Taniyasu , Masuzo Nagayama
发明人： Hiroshi Isa , Toshiyuki Ukigai , Anri Tominaga , Ryozo Taniyasu , Masuzo Nagayama
IPC分类号： C08F4/00 , A61K8/30 , B01J31/00 , C07B61/00 , C07C1/00 , C07C2/20 , C07C2/22 , C07C2/26 , C07C11/02 , C07C67/00 , C08F4/06 , C08F10/00 , C08F10/14 , C10M107/10 , C10M169/00 , C10N30/02 , C10N40/04 , C10N40/12 , C10N40/30 , C07C9/00 , C10M1/16
CPC分类号： C10M3/00 , C07C2/22 , C07C2527/126 , C07C2531/02 , C07C2531/26 , C10M2205/00 , C10M2205/028
摘要： A method of effecting polymerization of olefins having 6 or more carbon atoms or mixtures of such olefins (hereinafter referred to as the feed olefin), to produce a hydrocarbon liquid polymer which comprises mixing a catalyst composed of aluminum chloride, ketone having 4 or more carbon atoms and olefin catalyst constituent with 0.01 to 0.3 mole of ester, ether or alcohol per mole of said aluminum chloride and effecting the polymerization of the feed olefin at a reaction temperature of more than 60.degree.C.
摘要翻译：一种使具有6个或更多个碳原子的烯烃或这种烯烃的混合物（以下称为进料烯烃）进行聚合的方法来制备烃液体聚合物，其包括将由氯化铝组成的催化剂，具有4个或更多个碳的酮原子和烯烃催化剂组分，每摩尔所述氯化铝具有0.01至0.3摩尔的酯，醚或醇，并在大于60℃的反应温度下进行进料烯烃的聚合。

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