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    • 1. 发明授权
    • Apparatus for quantitative solidification of molten salt by using vacuum transfer and dual vessel
    • 用于通过真空转移和双重容器定量凝固熔融盐的装置
    • US07703304B2
    • 2010-04-27
    • US11189657
    • 2005-07-26
    • Myeong Soo JeongJin Mok HurSoo Haeng ChoChung Seok SeoSeong Won Park
    • Myeong Soo JeongJin Mok HurSoo Haeng ChoChung Seok SeoSeong Won Park
    • C03B7/00C03B5/00B22D35/06
    • C01D15/04
    • Provided are an apparatus and method for manufacturing a solidified salt that is easy to treat in size and shape by using a vacuum transfer and a dual vessel. In the apparatus for quantitative solidification of a molten salt, a molten salt is introduced into a first vessel, and a second vessel is disposed inside the first vessel and quantitatively supplied with the molten salt. A molten-salt transferring unit quantitatively transfers the molten salt from the first vessel to the second vessel by vacuum pressure. A valve controls a discharge of the molten salt from the second vessel. A mold receives the molten salt from the second vessel and solidifies the molten salt. Accordingly, the molten salt can be stably discharged to the mold by quantitatively transferring the molten salt at vacuum pressure within the dual vessel, and a predetermined size and shape of the solidified salt can be manufactured, thereby processing and collecting the solidified salt safely.
    • 提供一种制造固化盐的装置和方法,其通过使用真空转移和双重容器容易地处理尺寸和形状。 在熔融盐定量固化装置中,将熔融盐引入第一容器中,将第二容器置于第一容器的内部并定量供给熔融盐。 熔融盐转移单元通过真空压力将熔融盐从第一容器定量转移到第二容器。 阀门控制来自第二容器的熔融盐的排放。 模具从第二容器接收熔融盐并使熔融盐固化。 因此,可以通过在双容器内以真空压力定量转移熔融盐,将熔融盐稳定地排出到模具中,并且可以制造预定尺寸和形状的固化盐,从而安全地加工和收集固化盐。
    • 2. 发明申请
    • Apparatus and method for quantitative solidification of molten salt by using vacuum transfer and dual vessel
    • 使用真空转移和双重容器定量凝固熔融盐的设备和方法
    • US20060179883A1
    • 2006-08-17
    • US11189657
    • 2005-07-26
    • Myeong Soo JeongJin Mok HurSoo Haeng ChoChung Seok SeoSeong Won Park
    • Myeong Soo JeongJin Mok HurSoo Haeng ChoChung Seok SeoSeong Won Park
    • C03B7/18C03B5/16C03B5/26
    • C01D15/04
    • Provided are an apparatus and method for manufacturing a solidified salt that is easy to treat in size and shape by using a vacuum transfer and a dual vessel. In the apparatus for quantitative solidification of a molten salt, a molten salt is introduced into a first vessel, and a second vessel is disposed inside the first vessel and quantitatively supplied with the molten salt. A molten-salt transferring unit quantitatively transfers the molten salt from the first vessel to the second vessel by vacuum pressure. A valve controls a discharge of the molten salt from the second vessel. A mold receives the molten salt from the second vessel and solidifies the molten salt. Accordingly, the molten salt can be stably discharged to the mold by quantitatively transferring the molten salt at vacuum pressure within the dual vessel, and a predetermined size and shape of the solidified salt can be manufactured, thereby processing and collecting the solidified salt safely.
    • 提供一种制造固化盐的装置和方法,其通过使用真空转移和双重容器容易地处理尺寸和形状。 在熔融盐定量固化装置中,将熔融盐引入第一容器中,将第二容器置于第一容器的内部并定量供给熔融盐。 熔融盐转移单元通过真空压力将熔融盐从第一容器定量转移到第二容器。 阀门控制来自第二容器的熔融盐的排放。 模具从第二容器接收熔融盐并使熔融盐固化。 因此,可以通过在双容器内以真空压力定量转移熔融盐,将熔融盐稳定地排出到模具中,并且可以制造预定尺寸和形状的固化盐,从而安全地加工和收集固化盐。
    • 4. 发明申请
    • Method for preparing tantalum or niobium powders used for manufacturing capacitors
    • 制造用于制造电容器的钽或铌粉末的方法
    • US20070295609A1
    • 2007-12-27
    • US11473605
    • 2006-06-23
    • Sang Mun JeongSung Bin ParkJong Hyeon LeeChung Seok SeoSeong Won ParkEung Ho Kim
    • Sang Mun JeongSung Bin ParkJong Hyeon LeeChung Seok SeoSeong Won ParkEung Ho Kim
    • C25C3/00
    • C25C3/26B22F9/20B22F2999/00C25C3/02C25C5/04
    • Disclosed relates to a method for preparing tantalum or niobium powders used for manufacturing capacitors in an electrolytic reducing reactor including an anode, a cathode and a molten salt, the method comprising: obtaining a tantalum or niobium oxide, expressed by Ta2O(5-y) or Nb2O(5-y) where y=2.5 to 4.5, from a tantalum pentoxide Ta2O5 or a niobium pentoxide Nb2O5 generated partially by an alkaline metal electrolytically reduced via a first electrolytic reducing reaction that reduces an alkaline metal oxide from a molten salt comprising at least one metal halogen compound, selected from the group consisting of alkaline metal and alkaline earth metal, and an alkaline metal oxide on the cathode; and preparing a tantalum or niobium powder by a first electrolytic reducing reaction that reduces at least one metal halogen compound selected from the group consisting of the alkaline metal oxide and the alkaline earth metal on the cathode and by a second reducing reaction with the tantalum or niobium oxide, represented by Ta2O(5-y) or Nb2O(5-y) where y=2.5 to 4.5.
    • 本发明涉及一种制备用于在包括阳极,阴极和熔融盐的电解还原反应器中制造电容器的钽或铌粉末的方法,所述方法包括:获得由Ta 2表示的钽或铌氧化物, (5-y)或Nb 2 O(5-y)其中y = 2.5至4.5,从五氧化二钽 或通过碱金属部分地生成的五氧化二铌Nb 2 O 5 O 3,其通过电解还原的碱金属 第一电解还原反应,其从包含至少一种选自碱金属和碱土金属的金属卤素化合物和阴极上的碱金属氧化物的熔融盐中降低碱金属氧化物; 并通过第一次电解还原反应来制备钽或铌粉末,该反应在阴极上还原至少一种选自碱金属氧化物和碱土金属的金属卤素化合物,并通过与钽或铌的第二次还原反应 氧化物,由Ta 2 O(5-y)或Nb 2 O(5-y)表示,其中 y = 2.5〜4.5。