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1. 发明授权

US6017996A Method for the continuous manufacturing of silicone rubber composition 失效
标题翻译：连续制造硅橡胶组合物的方法
公开(公告)号：US6017996A
公开(公告)日：2000-01-25
申请号：US151120
申请日：1998-09-10
申请人： Mitsuo Hamada , Tomoo Kinoshita , Kaoru Kunimatsu
发明人： Mitsuo Hamada , Tomoo Kinoshita , Kaoru Kunimatsu
IPC分类号： B29B7/00 , B29B7/40 , B29B7/90 , B29B11/14 , B29C47/00 , B29C47/64 , C08J3/20 , C08K3/34 , C08L83/04 , C08K5/54
CPC分类号： C08J3/203 , B29B7/402 , B29B7/421 , B29B7/428 , B29B7/90 , B29C47/605 , B29C47/00 , B29C47/0009 , B29K2083/00 , B29K2105/16 , C08J2383/04
摘要： A method for manufacturing of a silicone rubber base composition in a mass-like form, comprises:(A) preparing a freely flowable powdered silicone rubber composition comprising(a) a cross-linkable polydiorganosiloxane with a viscosity of at least 1.times.10.sup.5 mPa.s at 25.degree. C. and(b) an inorganic filler, and(B) continuously kneading and massing the powdered silicone rubber composition in a multiple-stage siding shear-type single-screw extruder.This method provides for continuous preparation of a silicone rubber base compound without the use of a dual-screw mixer-extruder having a large length to diameter ratio, without abrasive wear of screws and cylinders with such inorganic fillers as diatomaceous earth power, quartz or a similar large-grain and hard powders, without blackening of the mixed silicone rubber composition, and without production problems associated with the use of large quantities of fumed silica, sedimentary silica, or a similar reinforcing silica.
摘要翻译：制造质量状的硅橡胶基础组合物的方法包括：（A）制备可自由流动的粉状硅橡胶组合物，其包含（a）粘度为至少1×10 5 mPa.s的交联聚二有机硅氧烷， 25℃，（b）无机填料，（B）在多层壁板式剪切式单螺杆挤出机中连续混炼和组合粉状硅橡胶组合物。该方法提供连续制备硅橡胶基础化合物而不使用具有大直径比的双螺杆混合机 - 挤出机，而不会使用诸如硅藻土功率，石英或石英的无机填料的螺杆和圆筒的磨损类似的大颗粒和硬粉末，而不使混合的硅橡胶组合物变黑，并且与使用大量热解法二氧化硅，沉积二氧化硅或类似的增强二氧化硅有关的生产问题。

2. 发明授权

US6013701A Method for the continuous manufacturing of silicone rubber composition 失效
标题翻译：连续制造硅橡胶组合物的方法
公开(公告)号：US6013701A
公开(公告)日：2000-01-11
申请号：US174978
申请日：1998-10-19
申请人： Kaoru Kunimatsu , Tomoo Kinoshita , Mitsuo Hamada
发明人： Kaoru Kunimatsu , Tomoo Kinoshita , Mitsuo Hamada
IPC分类号： C08J3/20 , C08K3/36 , C08L83/04 , C08L83/07
CPC分类号： C08L83/04 , B29B7/402 , B29B7/421 , B29B7/428 , B29B7/90 , B29C47/0009 , B29C47/1045 , B29C47/366 , B29C47/385 , B29C47/6062 , B29K2083/005 , C08G77/06 , C08G77/20
摘要： A method for continuous preparation of a high consistency or liquid silicone rubber base does not cause abrasive wear of the extruder screw and of the extruder cylinder or blackening of the silicone rubber base even when the latter is admixed with such fillers as an inorganic filler in the form of a diatomaceous earth powder, quartz or a similar large-grained and hard substance, or with a fumed silica, sedimentary silica, or a similar reinforcing silica filler. The method comprises continuously kneading the following components in a multiple-stage shear type single-screw extruder: (A) a freely-flowable powdered silicone rubber mixture having its main components in the form of (a) a cross-linkable polydiorganosiloxane with a viscosity exceeding 1.times.10.sup.5 mPa.multidot.s at 25.degree. C. and (b) an inorganic filler, and (B) a high consistency silicone rubber base having its main components in the form of (a) a cross-linkable polydiorganosiloxane with a viscosity exceeding 1.times.10.sup.5 mPa.multidot.s at 25.degree. C. and (c) a reinforcing silica filler, or a liquid silicone rubber base having its main components in the form of (d) a cross-linkable polydiorganosiloxane with a viscosity below 1.times.10.sup.5 mPa.multidot.s at 25.degree. C. and (c) a reinforcing silica filler.
摘要翻译：连续制备高稠度或液体硅橡胶基体的方法不会引起挤出机螺杆和挤出机圆筒的磨损或硅橡胶基底的黑化，即使将后者与诸如无机填料的填料混合在一起硅藻土粉末，石英或类似的大颗粒和硬物质的形式，或与煅制二氧化硅，沉积二氧化硅或类似的增强二氧化硅填料形成。该方法包括在多级剪切式单螺杆挤出机中连续捏合以下组分：（A）可自由流动的粉状硅橡胶混合物，其主要成分为（a）可交联的聚二有机硅氧烷，其粘度在25℃下超过1×10 5 mPax，（b）无机填料，（B）高稠度硅橡胶基质，其主要成分为（a）可交联的聚二有机硅氧烷，其粘度在25℃时粘度超过1×10 5 mPax （c）增强二氧化硅填料或其主要组分为（d）可交联的聚二有机硅氧烷的液体硅橡胶基质，其粘度在25℃时粘度低于1×10 5 mPax，（c）a 增强二氧化硅填料。

3. 发明授权

US5409978A Method for the continuous preparation of heat-vulcanizing silicone rubber compounds 失效
标题翻译：连续制备热硫化硅橡胶化合物的方法
公开(公告)号：US5409978A
公开(公告)日：1995-04-25
申请号：US234212
申请日：1994-04-28
申请人： Mitsuo Hamada , Tomoo Kinoshita , Kaoru Kunimatsu , Teruyuki Nakagawa , Satoru Terashima
发明人： Mitsuo Hamada , Tomoo Kinoshita , Kaoru Kunimatsu , Teruyuki Nakagawa , Satoru Terashima
IPC分类号： B29B7/46 , B01F13/10 , B29B7/00 , B29B7/74 , B29B7/88 , B29B11/14 , C08J3/20 , C08L83/04 , C08K5/54
CPC分类号： C08J3/201 , B29B7/007 , B29B7/7466 , B29B7/7495 , B29B7/88 , B29C47/1081 , B29C47/366 , B29C47/802 , C08L83/04 , B01F13/1013 , B29K2083/00 , B29K2105/16 , C08G77/16 , C08G77/44 , C08G77/70 , C08J2383/04
摘要： The present invention relates to a method for the continuous preparation of heat-vulcanizing silicone rubber compounds. The method comprises continuous feeding of (A) 100 weight parts polydiorganosiloxane gum, (B) 5 to 100 weight parts reinforcing filler, and (C) up to 30 weight parts processing aid to a co-rotating twin-screw continuous compounding extruder. The components (A), (B), and (C) are continuously mixed in the extruder at a temperature in a range of about 200.degree. C. to 300.degree. C. The mixed components are then discharged, forming an extrudate. The extrudate is fed continuously to a counter-rotating twin-screw continuous compounding extruder, wherein the extrudate is continuously heat-treated at a temperature in a range of 150.degree. C. to 300.degree. C., forming the silicone rubber compound, which is then discharged from the counter-rotating twin-screw continuous compounding extruder.
摘要翻译：本发明涉及一种连续制备热硫化硅橡胶化合物的方法。该方法包括连续进料（A）100重量份聚二有机硅氧烷胶，（B）5至100重量份增强填料，和（C）至多30重量份的加工助剂至同向双螺杆连续混合挤出机。组分（A），（B）和（C）在挤出机中在约200℃至300℃的温度下连续混合。然后将混合的组分排出，形成挤出物。将挤出物连续供给到反向旋转的双螺杆连续复合挤出机中，其中挤出物在150℃至300℃的温度下连续热处理，形成硅橡胶化合物，其为然后从反向旋转双螺杆连续复合挤出机排出。

4. 发明授权

US5861460A Method for the continuous production of room-temperature-curable organopolysiloxane compositions 失效
标题翻译：连续生产室温可固化的有机聚硅氧烷组合物的方法
公开(公告)号：US5861460A
公开(公告)日：1999-01-19
申请号：US625568
申请日：1996-03-28
申请人： Mitsuo Hamada , Tomoo Kinoshita , Hideyuki Mori , Junya Yokoi
发明人： Mitsuo Hamada , Tomoo Kinoshita , Hideyuki Mori , Junya Yokoi
IPC分类号： B01F7/26 , B29B7/40 , B29B7/84 , C08G77/06 , C08K3/00 , C08K5/54 , C08K13/02 , C08L83/04 , C08L87/00
CPC分类号： C08K13/02 , B29B7/402 , B29B7/847 , B29C47/364 , B29C47/6087 , C08L83/04 , C08G77/06 , C08G77/16
摘要： A highly productive, continuous method for the production of room-temperature-curable organopolysiloxane compositions is obtained by continuously feeding 100 parts by weight of a diorganopolysiloxane with a viscosity at 25.degree. C. of 0.1 to 500 Pa.s that contains at least 2 silicon-bonded hydroxyl groups or hydrolyzable groups in each molecule; 1 to 30 parts by weight of an organosilane that contains at least 2 silicon-bonded hydrolyzable groups in each molecule, or the partial hydrolysis condensate thereof; 1 to 200 parts by weight of an inorganic filler in powder form, and 0 to 10 parts by weight of a cure-accelerating catalyst into a continuous mixing apparatus having starting material feed openings installed at its top, a discharge opening installed at its bottom, and a rotating disk installed within a casing and are therein mixed by the rotation of the said rotating disk, and in that the resulting mixture is thereafter continuously introduced into a vacuum mechanism- equipped degassing apparatus in which the water fraction present in the said mixture is removed under reduced pressure.
摘要翻译：通过连续供给100重量份的在25℃下的粘度为0.1至500Pa.s的二有机聚硅氧烷，其含有至少2个硅，得到用于制备室温可固化的有机基聚硅氧烷组合物的高产率连续方法每个分子中的双键羟基或可水解基团; 1〜30重量份在每个分子中含有至少2个硅键合的可水解基团的有机硅烷或其部分水解缩合物; 1〜200重量份的粉末状无机填料，0〜10重量份的固化促进催化剂，其具有安装在其顶部的起始原料供给开口的连续混合装置，安装在其底部的排出口，以及旋转盘，其安装在壳体内并通过所述旋转盘的旋转而混合，然后将所得混合物连续引入装有真空机构的脱气装置，其中存在于所述混合物中的水分为减压除去。

5. 发明授权

US07732519B2 Emulsion composition for silicone rubber, process for producing the same, and process for producing silicone rubber 有权
标题翻译：硅橡胶用乳液组合物及其制造方法以及硅橡胶的制造方法
公开(公告)号：US07732519B2
公开(公告)日：2010-06-08
申请号：US12536702
申请日：2009-08-06
申请人： Shinya Shirasaki , Tadanori Fukamachi , Mitsuo Hamada
发明人： Shinya Shirasaki , Tadanori Fukamachi , Mitsuo Hamada
IPC分类号： C08K3/34 , C08G77/04 , C08G77/12
CPC分类号： C08J3/03 , C08G77/06 , C08G77/12 , C08G77/20 , C08J2383/04 , C08L83/04 , C08L83/00 , C08L2666/54
摘要： A silicone rubber emulsion composition comprising (A) 100 parts diorganopolysiloxane having at least two silicon-bonded alkenyl groups, (E) 0 to 60 parts reinforcing silica filler, (B) 10 to 250 parts water containing a smectite clay, (C) 0.1 to 15 parts emulsifier, and (D) a cross-linking agent (e.g., an organohydrogenpolysiloxane) in an amount sufficient for cross-linking component (A) and a catalyst (e.g., a platinum-type catalyst). A method for preparing the aforementioned emulsion composition comprising mixing components (A) and (E) with other components in a high-speed stirrer-equipped mixer. A method of manufacturing a silicone rubber comprising either heating and dehydrating the aforementioned emulsion composition.
摘要翻译：一种硅橡胶乳液组合物，其包含（A）100份具有至少两个与硅键合的烯基的二有机聚硅氧烷，（E）0至60份增强二氧化硅填料，（B）10至250份含有蒙脱石粘土的水，（C）0.1 至（15）份的乳化剂和（D）交联剂（例如，有机氢聚硅氧烷），其量足以使交联组分（A）和催化剂（例如，铂型催化剂）。一种制备上述乳液组合物的方法，包括在具有高速搅拌器的混合器中将组分（A）和（E）与其它组分混合。包括加热和脱水上述乳液组合物的硅橡胶的制造方法。

6. 发明申请

US20090292056A1 Emulsion Composition For Silicone Rubber, Process For Producing The Same, And Process For Producing Silicone Rubber 有权
标题翻译：硅橡胶的乳液组合物，其生产方法和生产硅橡胶的方法
公开(公告)号：US20090292056A1
公开(公告)日：2009-11-26
申请号：US12536702
申请日：2009-08-06
申请人： Shinya Shirasaki , Tadanori Fukamachi , Mitsuo Hamada
发明人： Shinya Shirasaki , Tadanori Fukamachi , Mitsuo Hamada
IPC分类号： C08K3/34
CPC分类号： C08J3/03 , C08G77/06 , C08G77/12 , C08G77/20 , C08J2383/04 , C08L83/04 , C08L83/00 , C08L2666/54
摘要： A silicone rubber emulsion composition comprising (A) 100 parts diorganopolysiloxane having at least two silicon-bonded alkenyl groups, (E) 0 to 60 parts reinforcing silica filler, (B) 10 to 250 parts water containing a smectite clay, (C) 0.1 to 15 parts emulsifier, and (D) a cross-linking agent (e.g., an organohydrogenpolysiloxane) in an amount sufficient for cross-linking component (A) and a catalyst (e.g., a platinum-type catalyst). A method for preparing the aforementioned emulsion composition comprising mixing components (A) and (E) with other components in a high-speed stirrer-equipped mixer. A method of manufacturing a silicone rubber comprising either heating and dehydrating the aforementioned emulsion composition.
摘要翻译：一种硅橡胶乳液组合物，其包含（A）100份具有至少两个与硅键合的烯基的二有机聚硅氧烷，（E）0至60份增强二氧化硅填料，（B）10至250份含有蒙脱石粘土的水，（C）0.1 至（15）份的乳化剂和（D）交联剂（例如，有机氢聚硅氧烷），其量足以使交联组分（A）和催化剂（例如铂型催化剂）。一种制备上述乳液组合物的方法，包括在具有高速搅拌器的混合器中将组分（A）和（E）与其它组分混合。包括加热和脱水上述乳液组合物的硅橡胶的制造方法。

7. 发明申请

US20070166524A1 Porous carbon electrode substrate and its production method and carbon fiber paper 审中-公开
标题翻译：多孔碳电极基板及其生产方法和碳纤维纸
公开(公告)号：US20070166524A1
公开(公告)日：2007-07-19
申请号：US11723017
申请日：2007-03-15
申请人： Makoto Nakamura , Yoshihiko Hosako , Hidehiko Ohashi , Mitsuo Hamada , Kazushige Mihara
发明人： Makoto Nakamura , Yoshihiko Hosako , Hidehiko Ohashi , Mitsuo Hamada , Kazushige Mihara
IPC分类号： D04H1/00
CPC分类号： D21H13/50 , C04B35/83 , C04B2235/424 , C04B2235/48 , C04B2235/5212 , C04B2235/5248 , C04B2235/5256 , C04B2235/526 , C04B2235/5264 , C04B2235/602 , C04B2235/77 , C04B2235/94 , C04B2235/96 , D21H13/16 , D21H15/06 , D21H17/36 , D21H17/48 , D21H21/18 , D21H21/52 , H01M4/8605 , H01M4/96 , H01M8/0234 , H01M2008/1095 , Y02P70/56 , Y10T428/249924 , Y10T428/30
摘要： The present invention provides carbon fiber paper consisting of an organic high-molecular compound as a binder and carbon fibers, characterized in that the carbon fibers contain thin fibers with an average diameter smaller than 5 μm and an average fiber length of 3 to 10 mm; a porous carbon electrode substrate for a fuel cell having a thickness of 0.05 to 0.5 mm and a bulk density of 0.3 to 0.8 g/cm3, also having a bending strength of 10 MPa or higher and a deflection of 1.5 mm or more at the time of bending, measured by a three-point bending test in conditions of using a sample width of 1 cm, a strain rate of 10 mm/min, and a distance between supporting points of 2 cm; and a method of producing a porous carbon electrode substrate for a fuel cell by impregnating the carbon fiber paper with a thermosetting resin, curing the thermosetting resin by heating and pressing treatment, and then carbonizing the paper. The electrode substrate of the present invention is excellent in flexibility and bending strength and able to be rolled on a roll and thus has high productivity, and the carbon fiber paper of the present invention is suitable for producing the electrode substrate.
摘要翻译：本发明提供由作为粘合剂的有机高分子化合物和碳纤维组成的碳纤维纸，其特征在于，所述碳纤维含有平均直径小于5μm，平均纤维长度为3〜10mm的细纤维; 具有厚度为0.05〜0.5mm，体积密度为0.3〜0.8g / cm 3的燃料电池用多孔碳电极基板，其弯曲强度为10MPa以上，偏转在使用1cm的样品宽度，10mm / min的应变速度和2cm的支撑点之间的距离的条件下，通过三点弯曲试验测定弯曲时的1.5mm以上的1.5mm以上。以及通过用热固性树脂浸渍碳纤维纸来制造用于燃料电池的多孔碳电极基板的方法，通过加热和压制处理固化热固性树脂，然后碳化碳纸。本发明的电极基板的柔软性和弯曲强度优异，能够在辊上滚动，因此具有高生产率，本发明的碳纤维纸适用于制造电极基板。

8. 发明授权

US06353033B1 Method and apparatus for cutting high viscosity liquid material 失效
标题翻译：切割高粘度液体材料的方法和设备
公开(公告)号：US06353033B1
公开(公告)日：2002-03-05
申请号：US09628468
申请日：2000-07-31
申请人： Koichi Ozaki , Toru Imaizumi , Koichi Ishida , Toyohiko Yamadera , Mitsuo Hamada
发明人： Koichi Ozaki , Toru Imaizumi , Koichi Ishida , Toyohiko Yamadera , Mitsuo Hamada
IPC分类号： B01F1700
CPC分类号： B26F3/00 , F16K1/02 , F17D1/14 , Y10S516/924
摘要： Method and apparatus for cutting high viscosity liquid material, said apparatus comprising a cylinder divided into upper and lower tanks by a partition with a central discharge opening, a moveable and elevatable liquid supply pipe with a distal end positioned opposite the discharge opening, the liquid supply pipe being mounted so that it can be raised until its distal end contacts the partition around the discharge opening, and then lowered until there is no contact, means for raising and lowering the liquid supply pipe, the upper tank having peripheral injection ports for injecting a low viscosity liquid into the upper tank, means for feeding high viscosity liquid material into the lower tank and flowing it into the upper tank, means for feeding low viscosity liquid into the liquid supply pipe and for feeding low viscosity liquid into the peripheral injection ports, the high viscosity liquid material flowing from the lower tank into the upper tank when the liquid supply pipe is lowered, the high viscosity liquid material being pushed upwardly into the upper tank by the low viscosity liquid when the liquid supply pipe is raised, whereby the high viscosity liquid material being pushed upwardly in the upper tank is cut into blocks by the low viscosity liquid being injected into the upper tank.
摘要翻译：用于切割高粘度液体材料的方法和装置，所述装置包括通过具有中心排出口的分隔件分成上部和下部罐的圆筒，具有与排出口相对的远端的可移动和可升高的液体供应管，液体供应管被安装成可以升高直到其远端接触排放口周围的隔板，然后降低直到不接触，用于升高和降低液体供给管的装置，上部罐具有用于注入的周边注入口低粘度液体进入上部罐，用于将高粘度液体材料进入下部罐并将其流入上部罐的装置，用于将低粘度液体供给到液体供给管中并将低粘度液体供给到外部喷射口中的装置，当液体供应管较低时，高粘度液体材料从下槽流入上罐 d，当液体供应管升高时，高粘度液体材料被低粘度液体向上推入上罐，由此通过低粘度液体将在上槽中向上推的高粘度液体材料切成块注入上水箱。

9. 发明授权

US6117933A Silicone rubber particulate composition and methods for the preparation thereof 失效
标题翻译：硅橡胶颗粒组合物及其制备方法
公开(公告)号：US6117933A
公开(公告)日：2000-09-12
申请号：US337570
申请日：1999-06-22
申请人： Kouichi Ozaki , Norio Matsuda , Makoto Tanoue , Toyohiko Yamadera , Mitsuo Hamada
发明人： Kouichi Ozaki , Norio Matsuda , Makoto Tanoue , Toyohiko Yamadera , Mitsuo Hamada
IPC分类号： C08J3/12 , C08L83/04 , C08K5/09
CPC分类号： C08J3/12 , C08L83/04 , C08G77/12 , C08G77/16 , C08G77/20 , C08J2383/04
摘要： A silicone rubber particulate composition useful as an additive for cosmetics, rubbers, resins and paints is disclosed, said composition comprising:(A) a silicone rubber particulate having an average particle size of 0.1 to 1,000 .mu.m;(B) a water-absorptive resin particulate having a water-free average particle size of 0.1 to 1,000 .mu.m; and(C) water,wherein said component (B) is present at a level of 0.01 to 5 weight percent measured on a water-free basis relative to component (A) and said water is present at a level of 10 to 10,000 weight parts for each 100 weight parts of component (B).
摘要翻译：公开了一种可用作化妆品，橡胶，树脂和油漆的添加剂的硅橡胶颗粒组合物，所述组合物包含：（A）平均粒度为0.1-1000μm的硅橡胶颗粒; （B）无水平均粒径为0.1〜1000μm的吸水性树脂粒子; 和（C）水，其中所述组分（B）以相对于组分（A）在无水基础下测量的0.01至5重量％的水平存在，并且所述水以10至10,000重量份的量存在对于每100重量份组分（B）。

10. 发明授权

US4985483A Fluororubber composition containing dispersed particles of cured silicone material 失效
标题翻译：含有固化的硅氧烷材料的分散颗粒的氟橡胶组合物
公开(公告)号：US4985483A
公开(公告)日：1991-01-15
申请号：US411136
申请日：1989-09-22
申请人： Masayuki Saito , Keiji Yoshida , Mitsuo Hamada
发明人： Masayuki Saito , Keiji Yoshida , Mitsuo Hamada
IPC分类号： C08K5/54 , C08K5/5435 , C08L27/12 , C08L27/16 , C08L83/04 , C08L83/07 , C08L83/08 , C08L87/00 , C09J127/12 , C09J183/07
CPC分类号： C08K5/54 , C08L27/12 , C08L27/16 , C08L83/08 , C08L2205/22 , C08L83/04
摘要： Curable fluororubber compositions exhibit excellent processability on roll mills and can be molded without sticking to or staining the mold surfaces when the composition contains from 0.1 to 30 weight parts per 100 weight parts of fluororubber of a finely divided cured silicone material in the form of a rubber, gel or resin. An epoxy-substituted alkoxysilane or a partial hydrolysis product thereof is present as an ingredient of the curable composition when it is desired to cohesively bond the cured fluororubber to a metal or plastic substrate.

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