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1. 发明授权

US4273907A Benzoin-bonded organopolysiloxanes and method for the preparation thereof 失效
标题翻译：苯偶姻键合的有机聚硅氧烷及其制备方法
公开(公告)号：US4273907A
公开(公告)日：1981-06-16
申请号：US58539
申请日：1979-07-18
申请人： Minoru Takamizawa , Fumio Okada , Yasuaki Hara , Hisashi Aoki
发明人： Minoru Takamizawa , Fumio Okada , Yasuaki Hara , Hisashi Aoki
IPC分类号： C08G77/20 , C08G77/04
CPC分类号： C08G77/20 , Y10S522/904
摘要： The invention provides a novel class of organopolysiloxane compounds having at least one benzoin group represented by the general formula ##STR1## in which Ph is a phenyl group and R is a hydrogen atom or an alkyl group, bonded to the silicon atom in a molecule. The benzoin-bonded organopolysiloxane compounds can readily be prepared by the dehydrohalogenation, dehydrogenation, dehydration or dealkoholation condensation reaction between a corresponding organopolysiloxane having silicon-bonded halogen atoms, hydrogen atoms, hydroxy groups or alkoxy groups and an .alpha.-substituted or unsubstituted benzoin compound in the presence of a suitable reaction promotor or a condensation catalyst.
摘要翻译：本发明提供了一类新颖的有机聚硅氧烷化合物，其具有至少一个由通式“IMAGE”表示的苯偶姻基团，其中Ph是苯基，R是与分子中的硅原子键合的氢原子或烷基。苯偶姻键合的有机聚硅氧烷化合物可以容易地通过相应的具有硅键合的卤素原子，氢原子，羟基或烷氧基的有机聚硅氧烷和α-取代或未取代的苯偶姻化合物之间的脱卤化氢，脱氢，脱水或脱烷基化缩合反应来制备存在合适的反应促进剂或缩合催化剂。

2. 发明授权

US4359369A Photocurable organopolysiloxane compositions 失效
标题翻译：光固化有机聚硅氧烷组合物
公开(公告)号：US4359369A
公开(公告)日：1982-11-16
申请号：US180934
申请日：1980-08-25
申请人： Minoru Takamizawa , Fumio Okada , Yasuaki Hara , Hsashi Aoki , Yoshio Inoue
发明人： Minoru Takamizawa , Fumio Okada , Yasuaki Hara , Hsashi Aoki , Yoshio Inoue
IPC分类号： C08G77/28 , C08G77/392 , C08L83/08 , G03F7/075 , G03C1/68 , C08G77/00
CPC分类号： C08L83/08 , C08G77/28 , C08G77/392 , G03F7/0757 , Y10S522/905
摘要： The invention provides a novel photocurable organopolysiloxane composition having an unusually high photosensitivity suitable, for example, for providing an anti-sticking layer on a release paper. The composition comprises an organopolysiloxane having, in a molecule, at least one thioacyloxy-containing organosiloxane unit as the photosensitive functional group and a photosensitizer. Further improved photocurable composition of the invention comprises an organopolysiloxane having, in addition to the above mentioned thioacyloxy-containing organosiloxane units, at least one mercaptohydrocarbyl-containing organosiloxane unit in a molecule. Alternatively, photosensitivity of the similar degree is obtained when the composition comprises a first organopolysiloxane having, in a molecule, at least one thioacyloxy-containing organosiloxane unit and a second organopolysiloxane having, in a molecule, at least one mercaptohydrocarbyl-containing organosiloxane unit as combined.
摘要翻译：本发明提供了一种新颖的光固化有机聚硅氧烷组合物，其具有非常高的光敏性，其适合于例如在剥离纸上提供防粘层。该组合物包含在分子中含有至少一个含硫代酰氧基的有机硅氧烷单元作为光敏官能团的有机聚硅氧烷和光敏剂。本发明的进一步改善的光固化性组合物还包含除上述含硫代酰氧基的有机硅氧烷单元外的分子中含有至少一个含巯基烃基的有机硅氧烷单元的有机聚硅氧烷。或者，当组合物包含在分子中含有至少一个含硫代酰氧基的有机硅氧烷单元和在分子中具有至少一个含巯基烃基的有机硅氧烷单元的第二有机聚硅氧烷时，得到相似程度的光敏性，。

3. 发明授权

US4303484A Photocurable organopolysiloxane compositions 失效
标题翻译：光固化有机聚硅氧烷组合物
公开(公告)号：US4303484A
公开(公告)日：1981-12-01
申请号：US68593
申请日：1979-08-22
申请人： Minoru Takamizawa , Fumio Okada , Yasuaki Hara , Aoki, Hisashi
发明人： Minoru Takamizawa , Fumio Okada , Yasuaki Hara , Aoki, Hisashi
IPC分类号： C08F2/46 , C08L83/08 , D21H19/32 , G03F7/075
CPC分类号： G03F7/0757 , C08F2/46 , C08L83/08 , D21H19/32 , Y10S522/904 , Y10T428/31663 , Y10T428/31667
摘要： A novel photocurable composition suitable for preparing, for example, release papers is proposed which is formulated with photocrosslinkable organopolysiloxanes necessitating no conventional photosensitizers. Thus, the composition comprises(a) an organopolysiloxane having at least two mercaptoalkyl, e.g. mercaptopropyl, groups bonded to the silicon atoms in a molecule,(b) an organopolysiloxane having at least two alkenyl, e.g. vinyl groups directly bonded to the silicon atoms in a molecule, and(c) an organopolysiloxane having at least one benzoin group ##STR1## where Ph is a phenyl group, bonded to the silicon atom in a molecule, which component (c) serves as a photosensitizing ingredient. Alternatively, the inventive composition comprises (a) a mercaptoalkyl-containing organopolysiloxane as above and (b') an organopolysiloxane having, simultaneously, at least two alkenyl groups and at least one benzoin group directly bonded to the silicon atoms in a molecule, which component (b') serves both as the crosslinking agent and as the photosensitizing ingredient simultaneously. Owing to the unquestionable affinity of the photosensitizing ingredient with the other components, the inventive compositions have very high sensitivity in photocuring along with several other advantageous characteristics.
摘要翻译：提出了适用于制备例如离型纸的新型光固化性组合物，其与光可交联的有机聚硅氧烷配制，不需要常规的光敏剂。因此，组合物包含（a）具有至少两个巯基烷基的有机聚硅氧烷。巯基丙基，分子中与硅原子键合的基团，（b）具有至少两个烯基的有机聚硅氧烷，例如分子中直接与硅原子键合的乙烯基，和（c）具有至少一个苯偶姻基团的成分的有机聚硅氧烷，其中Ph是分子中与硅原子键合的苯基，该组分（c）用作光敏成分。或者，本发明的组合物包含（a）如上所述的含巯基烷基的有机聚硅氧烷和（b'）有机聚硅氧烷，其同时具有至少两个烯基和至少一个与分子中的硅原子键合的苯偶姻基团，该组分（b'）同时用作交联剂和光敏成分。由于光敏成分与其它组分的无疑的亲和性，本发明的组合物在光固化中具有非常高的灵敏度以及若干其它有利特征。

4. 发明授权

US4337348A Benzoin group-containing cyclic organopolysiloxanes and a method for the preparation thereof 失效
标题翻译：含有苯偶姻基团的环状有机聚硅氧烷及其制备方法
公开(公告)号：US4337348A
公开(公告)日：1982-06-29
申请号：US274631
申请日：1981-06-17
申请人： Minoru Takamizawa , Fumio Okada , Hisashi Aoki
发明人： Minoru Takamizawa , Fumio Okada , Hisashi Aoki
IPC分类号： C08K5/00 , C07F7/08 , C07F7/10 , C07F7/21 , C08F2/50 , C08G77/04 , C08K5/549 , C07F7/18
CPC分类号： C08G77/045 , C07F7/0885 , C07F7/21 , C08F2/50
摘要： The invention provides a benzoin group-containing cyclic organopolysiloxane, which belongs to a novel class of organosilicon compounds hitherto not known or not described in any prior art literatures. The compound has at least one benzoin group of the formula ##STR1## in which Ph is a phenyl group and R.sup.1 is a hydrogen atom or an alkyl group having from 1 to 4 carbon atoms or, in particular, a methyl group, directly bonded to the silicon atom in the cyclic tri-, tetra-, penta- or hexasiloxane. The compound is useful as a sensitizer for the crosslinking reaction of a photo- or radiation-curable organopolysiloxane composition owing to the high miscibility of the inventive compounds with the organopolysiloxane composition.
摘要翻译：本发明提供了一种含苯偶姻基的环状有机聚硅氧烷，其属于迄今为止在任何现有技术文献中未知或未描述的新一类有机硅化合物。该化合物具有至少一个式“IMAGE”的苯偶姻基团，其中Ph是苯基，R 1是氢原子或具有1至4个碳原子的烷基或特别是甲基，直接键合到环状三，四，五或六硅氧烷中的硅原子。由于本发明化合物与有机聚硅氧烷组合物的高混溶性，该化合物可用作光或可辐射固化的有机聚硅氧烷组合物的交联反应的敏化剂。

5. 发明授权

US5104927A Release silicone emulsion composition and process for preparing it 失效
标题翻译：释放硅胶乳液组合物及其制备方法
公开(公告)号：US5104927A
公开(公告)日：1992-04-14
申请号：US732174
申请日：1991-07-18
申请人： Yasuaki Hara , Fumio Okada
发明人： Yasuaki Hara , Fumio Okada
IPC分类号： C08L83/07 , B01J13/00 , C08J3/24 , C09D183/04 , C09J7/02
CPC分类号： C09D183/04
摘要： A release silicone emulsion composition comprising:(A) 100 parts by weight of a specific organovinylpolysiloxane;(B) from 1 to 50 parts by weight of a specific organohydrogenpolysiloxane;(C) from 0.5 part to 5 parts by weight of a platinum catalyst having a viscosity of 10 cSt or less at 25.degree. C.;(D) from 1.5 to 15 parts by weight of a nonionic emulsifying agent having an average HLB of from 10 to 20, pH of 6.5 or less and an ionic conductivity of 30 .mu..OMEGA..sup.-1 cm.sup.-1 or less; and(E) water.This composition has good pot life and curability. The cured film had good release properties and residual adhesive properties of adhesives.

6. 发明授权

US5095067A Release silicone emulsion composition 失效
标题翻译：释放硅氧烷乳液组合物
公开(公告)号：US5095067A
公开(公告)日：1992-03-10
申请号：US184026
申请日：1988-04-20
申请人： Yasuaki Hara , Fumio Okada
发明人： Yasuaki Hara , Fumio Okada
IPC分类号： C08L83/07 , B01J13/00 , C08J3/24 , C09D183/04 , C09J7/02
CPC分类号： C09D183/04
摘要： A release silicone emulsion composition comprising:(A) 100 parts by weight of a specific organovinylpolysiloxane;(B) from 1 to 50 parts by weight of a specific organohydrogenpolysiloxane;(C) from 0.5 part to 5 parts by weight of a platinum catalyst having a viscosity of 10 cSt or less at 25.degree. C.;(D) from 1.5 to 15 parts by weight of a nonionic emulsifying agent having an average HLB of from 10 to 20, pH of 6.5 or less and an ionic conductivity of 30 .mu..OMEGA..sup.-1 cm.sup.-1 or less; and(E) water.This composition has good pot life and curability. The cured film has good release properties and residual adhesive properties of adhesives.
摘要翻译：一种脱模硅氧烷乳液组合物，其包含：（A）100重量份的特定有机乙烯基聚硅氧烷; （B）1〜50重量份的特定有机氢聚硅氧烷; （C）在25℃下粘度为10cSt以下的铂催化剂为0.5〜5重量份。（D）1.5〜15重量份的平均HLB为10〜20，pH值为6.5以下，离子电导率为30万欧姆〜1cm-1以下的非离子乳化剂。和（E）水。该组合物具有良好的适用期和固化性。固化膜具有良好的剥离性能和粘合剂的残留粘合性能。

7. 发明授权

US4770942A Silicone-coated release paper and a method for the preparation thereof 失效
标题翻译：有机硅涂层剥离纸及其制备方法
公开(公告)号：US4770942A
公开(公告)日：1988-09-13
申请号：US808866
申请日：1985-12-13
申请人： Kunio Itoh , Fumio Okada , Hisashi Aoki , Yasushi Yamamoto
发明人： Kunio Itoh , Fumio Okada , Hisashi Aoki , Yasushi Yamamoto
IPC分类号： C09J7/02 , C08L83/00 , C08L83/04 , C08L83/07 , C09D5/00 , C09D183/04 , A23B4/04
CPC分类号： C08L83/04 , C09D183/04 , C08G77/12 , C08G77/20 , C08G77/24 , Y10T428/31663
摘要： The invention provides a silicone-coated release paper having a coating surface film of an organopolysiloxane composition curable by irradiation with ultraviolet light or electron beams to give a fully cured film resistant to migration of the organopolysiloxane constituents therefrom on to other surfaces in contact therewith. The composition comprises (a) a diorganopolysiloxane terminatd at both molecular chain ends each with a divinylmethylsilyl group or trivinylsilyl group, (b) an organohydrogenpolysiloxane having at least 2 hydrogen atoms directly bonded to the silicon atoms in a molecule, (c) a catalytic amount of a platinum or rhodium catalyst and, optionally, (d) a compound of a rare earth element such as ceric oxide.
摘要翻译：本发明提供一种具有硅氧烷涂层的剥离纸，其具有通过用紫外线或电子束照射可固化的有机聚硅氧烷组合物的涂层表面膜，以产生耐受其中的有机聚硅氧烷组分从而与其接触的其它表面的完全固化膜。该组合物包含（a）在两个分子链端分别具有二乙烯基甲基甲硅烷基或三乙烯基甲硅烷基的二有机聚硅氧烷，（b）具有至少2个氢原子的有机氢聚硅氧烷，其直接与分子中的硅原子键合，（c）催化量的铂或铑催化剂，和任选地（d）稀土元素如氧化铈的化合物。

8. 发明授权

US4707503A Radiation-curable organopolysiloxane compositions 失效
标题翻译：可辐射固化的有机聚硅氧烷组合物
公开(公告)号：US4707503A
公开(公告)日：1987-11-17
申请号：US800087
申请日：1985-11-21
申请人： Kunio Itoh , Fumio Okada , Yasushi Yamamoto , Hisashi Aoki
发明人： Kunio Itoh , Fumio Okada , Yasushi Yamamoto , Hisashi Aoki
IPC分类号： C08L83/00 , C08K5/54 , C08K5/548 , C08L83/04 , C08L83/06 , C08L83/07 , C08L83/08 , C09J7/02 , C08G75/04 , C08G77/28
CPC分类号： C08K5/5406 , C08L83/08
摘要： The radiation-curable organopolysiloxane composition of the invention is quite free from the problem of the migration of silicone toward the surface of a body in contact with the surface of the cured film of the composition even by curing with an extremely small dose of radiation, e.g. ultraviolet light and electron beams, for curing. The mechanism for curing is in principle the radiation-induced addition reaction between the aliphatically unsaturated bonds in a first organopolysiloxane and the mercapto groups in a second organopolysiloxane but the aliphatically unsaturated bond in the first organopolysiloxane is bonded preferably remotely from the silicon atom with an electron-attractive atom or group intervening therebetween such as the divalent groups of the formula --O--CH.sub.2).sub.2 S-- and --CH.sub.2 --O--CH.sub.2 --S--.
摘要翻译：本发明的可辐射固化的有机基聚硅氧烷组合物，甚至通过用极小剂量的辐射固化，例如与组合物的固化膜的表面相接触的方式，完全没有硅离子迁移到身体表面的问题。紫外光和电子束，用于固化。固化机理原则上是第一有机聚硅氧烷中的脂族不饱和键与第二有机聚硅氧烷中的巯基之间的辐射诱导的加成反应，但第一有机聚硅氧烷中的脂族不饱和键优选与硅原子远离电子吸收原子或介于其间的基团，例如式-O-CH2）2S-和-CH2-O-CH2-S-的二价基团。

9. 发明申请

US20100040885A1 HIGHLY DISPERSIBLE FINE POWDER OF ALKALINE EARTH METAL CARBONATE 有权
标题翻译：碱性金属碳酸盐的高度分散的精细粉末
公开(公告)号：US20100040885A1
公开(公告)日：2010-02-18
申请号：US12530919
申请日：2008-03-12
申请人： Yojiro Ichimura , Takashi Watanabe , Fumio Okada
发明人： Yojiro Ichimura , Takashi Watanabe , Fumio Okada
IPC分类号： C01F11/18
CPC分类号： C01F11/18 , B82Y30/00 , C01F11/186 , C01P2004/54 , C01P2004/62 , C01P2004/64 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/22 , Y10T428/2982 , Y10T428/2998
摘要： A fine powder of an alkaline earth metal carbonate selected from the group consisting of barium carbonate, strontium carbonate and calcium carbonate, in which a primary particle of the powder has a mean diameter of 30 to 90 nm, in which the mean diameter is measured on a circle obtained from a projected area of the primary particle, and in which an accumulated volume of micropores having a pore size in the range of 10 to 20 nm is not less than 5×10−2 cm3/g can be easily dispersed in an aqueous medium in the form of essentially primary particles by an industrially employable dispersing method.
摘要翻译：选自碳酸钡，碳酸锶和碳酸钙的碱土金属碳酸盐的细粉末，其中粉末的初级颗粒的平均直径为30至90nm，其中平均直径在从一次粒子的投影面积获得的圆，其中孔径在10〜20nm范围内的微细孔的累积体积不小于5×10 -2 cm 3 / g可以容易地分散在水性介质，其基本上是初级粒子的形式，通过工业上可用的分散方法。

10. 发明授权

US06187939B1 Method for preparing fatty acid esters and fuel comprising fatty acid esters 有权
标题翻译：制备脂肪酸酯和包含脂肪酸酯的燃料的方法
公开(公告)号：US06187939B1
公开(公告)日：2001-02-13
申请号：US09392478
申请日：1999-09-09
申请人： Toshio Sasaki , Tomoyuki Suzuki , Fumio Okada
发明人： Toshio Sasaki , Tomoyuki Suzuki , Fumio Okada
IPC分类号： C11C100
CPC分类号： C11C3/003 , C07C67/03 , C10L1/026 , C10L1/19 , C10M101/04 , Y02E50/13 , Y02P20/544 , Y02P30/20 , C07C69/52
摘要： Fatty acid esters, which are prepared by reacting fats and oils with an alcohol in the absence of a catalyst under a condition under which at least one of the fats and oils and the alcohol is in a supercritical state, are useful as fuels such as diesel fuels, lubrication base oils or fuel additives.
摘要翻译：在脂肪和油和醇中的至少一种处于超临界状态的条件下，在不存在催化剂的情况下使脂肪和油与醇反应制备的脂肪酸酯可用作燃料如柴油燃料，润滑基础油或燃料添加剂。

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