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1. 发明申请

US20050118093A1 Method for reproducing lithium sulfide and method for producing polyarylene sulfide 审中-公开
标题翻译：再生硫化锂的方法及其制备方法
公开(公告)号：US20050118093A1
公开(公告)日：2005-06-02
申请号：US10498895
申请日：2002-12-17
申请人： Minoru Senga , Junji Matsui , Hideaki Kakimoto
发明人： Minoru Senga , Junji Matsui , Hideaki Kakimoto
IPC分类号： C01B17/22 , C08G75/02
CPC分类号： C08G75/0204 , C01B17/22 , C01P2006/80 , C08G75/0254
摘要： A method for reproducing lithium sulfide, including the steps of reacting lithium halide generated as a byproduct during the production of a polyarylene sulfide by a reaction between lithium sulfide and a halogenated aromatic compound with sodium carbonate to generate lithium sulfide, isolating the lithium carbonate and reacting the lithium carbonate with a sulfur compound to generate the lithium sulfide. According to the above method, lithium sulfide having a less Na content can be reproduced from lithium halide generated as a byproduct during the production of a polyarylene sulfide.
摘要翻译：一种再生硫化锂的方法，包括以下步骤：在硫化亚铜与卤代芳族化合物与碳酸钠反应生成聚芳硫醚期间作为副产物生成的卤化锂，生成硫化锂，分离碳酸锂并反应碳酸锂与硫化合物一起生成硫化锂。根据上述方法，可以在生产聚芳硫醚期间作为副产物产生的卤化锂再现具有较少Na含量的硫化锂。

2. 发明授权

US07026439B2 Process for continuous production of polyarylene sulfide 失效
标题翻译：连续生产聚芳硫醚的工艺
公开(公告)号：US07026439B2
公开(公告)日：2006-04-11
申请号：US10473366
申请日：2002-03-15
申请人： Minoru Senga , Masaya Okamoto , Mikiya Hayashi
发明人： Minoru Senga , Masaya Okamoto , Mikiya Hayashi
IPC分类号： C08G75/00 , C08G75/14 , C08G75/18
CPC分类号： C08G75/025
摘要： There is disclosed a process for continuously producing a polyarylene sulfide which comprises reacting a sulfur source with a dihalogenated aromatic compound in an aprotic organic solvent, characterized by maintaining the content of the dihalogenated aromatic compound in the polymerization liquid after the substantial completion of the polymerization reaction at 5 mg/g or higher. It is made possible by the process according to the present invention to efficiently produce the polyarylene sulfide which has a high molecular weight and is excellent in thermal stability.
摘要翻译：公开了一种连续生产聚芳硫醚的方法，其包括在非质子有机溶剂中使硫源与二卤代芳族化合物反应，其特征在于在聚合反应基本上完成后维持聚合液中的二卤代芳族化合物的含量在5mg / g以上。通过本发明的方法可以有效地制备分子量高且热稳定性优异的聚芳硫醚。

3. 发明授权

US09051201B2 Glass comprising solid electrolyte particles and lithium battery 有权
标题翻译：包含固体电解质颗粒和锂电池的玻璃
公开(公告)号：US09051201B2
公开(公告)日：2015-06-09
申请号：US13260054
申请日：2010-04-07
申请人： Ryo Aburatani , Minoru Senga , Tsuyoshi Ota , Masaru Nakagawa
发明人： Ryo Aburatani , Minoru Senga , Tsuyoshi Ota , Masaru Nakagawa
IPC分类号： H01M10/0562 , C03B19/12 , H01B1/12 , H01M4/13 , H01M4/62 , H01M10/052
CPC分类号： H01M10/0562 , C03B19/12 , C03B2201/86 , C03C1/02 , C03C3/321 , C03C4/18 , C03C10/00 , C03C12/00 , H01B1/122 , H01M4/13 , H01M4/62 , H01M10/052 , H01M2300/0068 , Y02E60/122 , Y02P70/54 , Y02T10/7011
摘要： Glass includes an aggregate of solid electrolyte particles including Li, P, and S, wherein when a Raman spectrum of the glass is repeatedly measured and a peak at 330 to 450 cm−1 in each Raman spectrum is separated to waveforms of individual components, a standard deviation of a waveform area ratio of each component is less than 4.0.
摘要翻译：玻璃包括包含Li，P和S的固体电解质颗粒的聚集体，其中当重复测量玻璃的拉曼光谱并且在每个拉曼光谱中在330至450cm -1处的峰分离成各个组分的波形时，各部件的波形面积比的标准偏差小于4.0。

4. 发明申请

US20130295464A1 COMPOSITE MATERIAL OF ALKALINE METAL SULFIDE AND CONDUCTING AGENT 审中-公开
标题翻译：碱金属硫化物和导电剂的复合材料
公开(公告)号：US20130295464A1
公开(公告)日：2013-11-07
申请号：US13981024
申请日：2012-01-25
申请人： Kazuaki Yanagi , Minoru Senga , Ryo Aburatani , Tsuyoshi Ota
发明人： Kazuaki Yanagi , Minoru Senga , Ryo Aburatani , Tsuyoshi Ota
IPC分类号： H01M4/136
CPC分类号： H01M4/136 , C01B17/22 , C01P2002/72 , C01P2002/85 , C01P2004/04 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/40 , H01M4/0497 , H01M4/1397 , H01M4/366 , H01M4/5815 , H01M4/624 , H01M4/625 , H01M4/626 , H01M10/0525
摘要： A composite material including a conducting material and an alkali metal sulfide formed integrally on the surface of the conducting material.
摘要翻译：一种复合材料，包括导电材料和一种碱金属硫化物，其一体地形成在导电材料的表面上。

5. 发明授权

US09196925B2 Glass particles 有权
标题翻译：玻璃颗粒
公开(公告)号：US09196925B2
公开(公告)日：2015-11-24
申请号：US14345809
申请日：2012-09-20
申请人： Ryo Aburatani , Minoru Senga , Tadanori Junke , Masao Aida
发明人： Ryo Aburatani , Minoru Senga , Tadanori Junke , Masao Aida
IPC分类号： C03C12/00 , H01M10/0562 , H01M10/0525 , C03C4/18 , C03C3/32 , H01B1/10 , C03C1/02 , C03C10/00 , C01B17/22 , C01B17/36
CPC分类号： H01M10/0562 , C01B17/22 , C01B17/36 , C01B25/14 , C01P2004/61 , C01P2006/12 , C01P2006/14 , C01P2006/80 , C03C1/02 , C03C3/321 , C03C4/18 , C03C10/00 , C03C12/00 , H01B1/10 , H01M10/0525 , H01M2300/0068
摘要： Glass particles including Li, P and S, wherein when a Raman spectrum of the glass particles is measured five times or more and a peak at 330 to 450 cm−1 in the Raman spectrum is separated into peaks of components by waveform separation, the standard deviation of the area ratio of each of the peaks of the components is 3.0 or less, the area of the peak of PS43− component obtained by the waveform separation is 10 to 95% of the total area, and the area of P2S74− component obtained by the waveform separation is 5 to 45% of the total area, and the area of the peak of PS43− component is larger than the area of the peak of P2S74− component.
摘要翻译：包括Li，P和S的玻璃颗粒，其中当拉曼光谱中的玻璃颗粒的拉曼光谱测量为五次以上且在330〜450cm -1处的峰值通过波形分离被分离成分量的峰值时，标准各部分的峰面积比的偏差为3.0以下，通过波形分离获得的PS43成分的峰面积为总面积的10〜95％，得到的P2S74-成分的面积通过波形分离占总面积的5〜45％，PS43-成分的峰面积大于P2S74-组分峰的面积。

6. 发明授权

US08012631B2 Lithium ion conductive sulfide-based solid electrolyte and all-solid lithium battery using same 有权
标题翻译：锂离子导电硫化物基固体电解质和全固态锂电池使用相同
公开(公告)号：US08012631B2
公开(公告)日：2011-09-06
申请号：US12096481
申请日：2006-11-28
申请人： Yoshikatsu Seino , Masaru Nakagawa , Minoru Senga , Masatoshi Shibata
发明人： Yoshikatsu Seino , Masaru Nakagawa , Minoru Senga , Masatoshi Shibata
IPC分类号： H01M6/18 , H01M4/13 , B05D5/12 , B05D3/00 , B05D3/04 , B05D3/10
CPC分类号： H01B1/122 , C03C3/321 , C03C4/18 , C03C10/00 , H01M10/052 , H01M10/0562 , H01M2300/0068 , Y02T10/7011
摘要： A solid electrolyte including a lithium (Li) element, a phosphorus (P) element and a sulfur (S) element, the 31P MAS NMR spectrum thereof having a peak ascribed to a crystal at 90.9±0.4 ppm and 86.5±0.4 ppm; and the ratio (xc) of the crystal in the solid electrolyte being from 60 mol % to 100 mol %.
摘要翻译：包含锂（Li）元素，磷（P）元素和硫（S））元素的固体电解质，具有归属于90.9±0.4ppm和86.5±0.4ppm的晶体的峰的31P MAS NMR光谱; 固体电解质中的结晶比例（xc）为60〜100摩尔％。

7. 发明申请

US20090159839A1 LITHIUM ION CONDUCTIVE SULFIDE-BASED SOLID ELECTROLYTE AND ALL-SOLID LITHIUM BATTERY USING SAME 有权
标题翻译：使用锂离子导电硫化物的固体电解质和全固体锂电池
公开(公告)号：US20090159839A1
公开(公告)日：2009-06-25
申请号：US12096481
申请日：2006-11-28
申请人： Yoshikatsu Seino , Masaru Nakagawa , Minoru Senga , Masatoshi Shibata
发明人： Yoshikatsu Seino , Masaru Nakagawa , Minoru Senga , Masatoshi Shibata
IPC分类号： H01M4/90
CPC分类号： H01B1/122 , C03C3/321 , C03C4/18 , C03C10/00 , H01M10/052 , H01M10/0562 , H01M2300/0068 , Y02T10/7011
摘要： A solid electrolyte including a lithium (Li) element, a phosphorus (P) element and a sulfur (S) element, the 31P MAS NMR spectrum thereof having a peak ascribed to a crystal at 90.9±0.4 ppm and 86.5±0.4 ppm; and the ratio (xc) of the crystal in the solid electrolyte being from 60 mol % to 100 mol %.
摘要翻译：包含锂（Li）元素，磷（P）元素和硫（S））元素的固体电解质，具有归属于90.9±0.4ppm和86.5±0.4ppm的晶体的峰的31P MAS NMR光谱; 固体电解质中的结晶比例（xc）为60〜100摩尔％。

8. 发明授权

US06982312B2 Process for producing polyarylene sulfide 失效
标题翻译：生产聚芳硫醚的方法
公开(公告)号：US06982312B2
公开(公告)日：2006-01-03
申请号：US10471663
申请日：2002-03-04
申请人： Minoru Senga , Masaya Okamoto , Mikiya Hayashi
发明人： Minoru Senga , Masaya Okamoto , Mikiya Hayashi
IPC分类号： C08G75/00
CPC分类号： C08G75/025 , C08G75/0254
摘要： There is disclosed a process for producing a polyarylene sulfide (PAS) which comprises reacting a sulfur source with a dihalogenated aromatic compound in the presence of an aprotic organic solvent, characterized in that the process comprises at least one polymerization reaction step wherein a polymer phase as a dispersed phase is in the form of spherical droplets. It is made possible by the continuous polymerization process to discharge the polymer phase and solvent phase from a polymerization vessel at a constant ratio and as a result, to maintain PAS composition (concentration) at a constant level at all times, and thus to provide a continuous PAS production process which is effective for enhancing its molecular weight and stabilizing the same.
摘要翻译：公开了一种生产聚芳硫醚（PAS）的方法，该方法包括在非质子有机溶剂存在下使硫源与二卤代芳族化合物反应，其特征在于该方法包括至少一个聚合反应步骤，其中聚合物相为分散相是球形液滴的形式。通过连续聚合方法可以以恒定比例从聚合容器中排出聚合物相和溶剂相，结果，始终保持PAS组成（浓度）在恒定水平，从而提供一种连续的PAS生产工艺，对于提高其分子量和稳定分子量是有效的。

9. 发明授权

US06316536B1 Polyarylene sulfide resin composition, and moldings and connectors made of it 失效
标题翻译：聚芳硫醚树脂组合物，以及由其制成的模制品和连接件
公开(公告)号：US06316536B1
公开(公告)日：2001-11-13
申请号：US09306050
申请日：1999-05-06
申请人： Masaya Okamoto , Minoru Senga , Koichi Suga , Kenji Seki
发明人： Masaya Okamoto , Minoru Senga , Koichi Suga , Kenji Seki
IPC分类号： C08J510
CPC分类号： C08L65/02 , C08G65/2612 , C08G2261/312 , C08K3/01 , C08K7/14 , C08L81/02
摘要： Provided is a polyarylene sulfide resin composition of which the moldings are burred little and which has good mechanical properties and good flow moldability. The composition comprises from 20 to 90% by weight of a polyarylene sulfide and from 10 to 80% by weight of an inorganic filler, and is characterized in that its burrs are on the level of at most 120 &mgr;m, that it has a weld strength of at least 50 MPa and that the length of its spiral flow having a thickness of 1 mm is at least 100 mm. Preferably, the polyarylene sulfide to be in the composition has a specific index to the degree of branching and a specific flexural strength.
摘要翻译：本发明提供一种聚酰亚胺硫化物树脂组合物，其模制品几乎没有被磨损，并且具有良好的机械性能和良好的流动成型性。该组合物包含20至90重量％的聚芳硫醚和10至80重量％的无机填料，其特征在于其毛刺的水平至多为120微米，其焊接强度至少50MPa，并且其具有1mm厚度的螺旋流的长度为至少100mm。优选地，组合物中的聚芳硫醚具有对支化度的特定指标和特定的弯曲强度。

10. 发明授权

US5856403A Process for preparing polyarylene sulfide copolymer, the copolymer prepared by the process, and resin composition comprising the copolymer 失效
标题翻译：制备聚芳硫醚共聚物的方法，通过该方法制备的共聚物和包含共聚物的树脂组合物
公开(公告)号：US5856403A
公开(公告)日：1999-01-05
申请号：US655675
申请日：1996-05-30
申请人： Minoru Senga , Koji Namiki
发明人： Minoru Senga , Koji Namiki
IPC分类号： C08G75/02 , C08G75/06 , C08G81/02 , C08L23/00 , C08L81/02 , C08L51/00
CPC分类号： C08G81/024 , C08G75/029 , C08L81/02 , C08L23/00
摘要： A process for efficiently manufacturing polyarylene sulfide copolymer in which polymers are well dispersed and which copolymer exhibiting superior mechanical properties. The process comprises reacting a polyarylene sulfide resin (A) and an amination agent (B) in a non-protonic organic solvent (C), and copolymerizing the resulting amino polyarylene sulfide resin (A') and a reactive elastomer (D) in a non-protonic organic solvent (C'), thereby obtaining a polyarylene sulfide resin (A") with the elastomer dispersed in the resin matrix.
摘要翻译：一种高分子制备聚芳硫醚共聚物的方法，其中聚合物分散良好，共聚物表现出优异的机械性能。该方法包括使聚芳硫醚树脂（A）和胺化剂（B）在非质子有机溶剂（C）中反应，并将得到的氨基聚芳硫醚树脂（A'）和反应性弹性体（D）共聚在非质子性有机溶剂（C'），由此得到分散在树脂基体中的弹性体的聚芳硫醚树脂（A“）。

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