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1. 发明申请

US20090227817A1 Process for producing 1,2-dialkoxy-3-fluorobenzene 失效
标题翻译： 1,2-二烷氧基-3-氟苯的制备方法
公开(公告)号：US20090227817A1
公开(公告)日：2009-09-10
申请号：US12379553
申请日：2009-02-24
申请人： Mingjian Qiu , Wei Zhang , Zhaohui Chen , Chunshan Zhang , Yali Zhang
发明人： Mingjian Qiu , Wei Zhang , Zhaohui Chen , Chunshan Zhang , Yali Zhang
IPC分类号： C07C43/225 , C07C39/26
CPC分类号： C07C39/27 , C07C41/16 , C07C41/26 , C07C43/225 , C07C43/23
摘要： The present invention relates to a process for producing a 2-fluoro-6-halophenol as an intermediate; a process for producing a 2-alkoxy-3-fluorophenol and further a 1,2-dialkoxy-3-fluorobenzene from the 2-fluoro-6-halophenol; a second process for producing a 1,2-dialkoxy-3-fluorobenzene from the 2-fluoro-6-halophenol; and a 2-alkoxy-3-fluorophenol. The 2-fluoro-6-halophenol can be obtained using a 2-fluorophenol as a starting material and through a sulfonation reaction, a halogenation reaction, and a deprotection reaction. The 2-fluoro-6-halophenol is alkyl-etherified, and subsequently the halogen atom is converted into a hydroxyl group to obtain the 2-alkoxy-3-fluorophenol, which is further alkyl-etherified to thereby obtain the 1,2-dialkoxy-3-fluorobenzene. Alternatively, a 1,2-dialkoxy-3-fluorobenzene is also obtained by converting the halogen atom of the 2-fluoro-6-halophenol into a hydroxyl group to thereby form 3-fluorocatechol and subsequently alkyl-etherifying two hydroxyl groups thereof. The processes of the invention realize low production costs and high process yields, and thus are suitable for industrial production of a 1,2-dialkoxy-3-fluorobenzene.
摘要翻译：本发明涉及作为中间体的2-氟-6-卤代苯酚的制造方法。从2-氟-6-卤苯酚制备2-烷氧基-3-氟苯酚和1,2-二烷氧基-3-氟苯的方法; 从2-氟-6-卤代苯酚制备1,2-二烷氧基-3-氟苯的第二种方法; 和2-烷氧基-3-氟苯酚。 2-氟-6-卤代苯酚可以使用2-氟苯酚作为原料，通过磺化反应，卤化反应和脱保护反应得到。 2-氟-6-卤代苯酚被烷基醚化，随后将卤素原子转化为羟基，得到2-烷氧基-3-氟苯酚，进一步进行烷基醚化，从而得到1,2-二烷氧基 -3-氟苯。或者，也可以通过将2-氟-6-卤代苯酚的卤素原子转化为羟基，从而形成3-氟邻苯二酚，然后将其两个羟基烷基醚化，得到1,2-二烷氧基-3-氟苯。本发明的方法实现了低生产成本和高工艺产率，因此适用于1,2-二烷氧基-3-氟苯的工业生产。

2. 发明授权

US07786330B2 Process for producing 1,2-dialkoxy-3-fluorobenzene 失效
公开(公告)号：US07786330B2
公开(公告)日：2010-08-31
申请号：US12379553
申请日：2009-02-24
申请人： Mingjian Qiu , Wei Zhang , Zhaohui Chen , Chunshan Zhang , Yali Zhang
发明人： Mingjian Qiu , Wei Zhang , Zhaohui Chen , Chunshan Zhang , Yali Zhang
IPC分类号： C07C37/04 , C07C41/26
CPC分类号： C07C39/27 , C07C41/16 , C07C41/26 , C07C43/225 , C07C43/23
摘要： The present invention relates to a process for producing a 2-fluoro-6-halophenol as an intermediate; a process for producing a 2-alkoxy-3-fluorophenol and further a 1,2-dialkoxy-3-fluorobenzene from the 2-fluoro-6-halophenol; a second process for producing a 1,2-dialkoxy-3-fluorobenzene from the 2-fluoro-6-halophenol; and a 2-alkoxy-3-fluorophenol. The 2-fluoro-6-halophenol can be obtained using a 2-fluorophenol as a starting material and through a sulfonation reaction, a halogenation reaction, and a deprotection reaction. The 2-fluoro-6-halophenol is alkyl-etherified, and subsequently the halogen atom is converted into a hydroxyl group to obtain the 2-alkoxy-3-fluorophenol, which is further alkyl-etherified to thereby obtain the 1,2-dialkoxy-3-fluorobenzene. Alternatively, a 1,2-dialkoxy-3-fluorobenzene is also obtained by converting the halogen atom of the 2-fluoro-6-halophenol into a hydroxyl group to thereby form 3-fluorocatechol and subsequently alkyl-etherifying two hydroxyl groups thereof. The processes of the invention realize low production costs and high process yields, and thus are suitable for industrial production of a 1,2-dialkoxy-3-fluorobenzene.

3. 发明授权

US07928268B2 Process for producing 1,2-dialkoxy-3-fluorobenzene 失效
标题翻译： 1,2-二烷氧基-3-氟苯的制备方法
公开(公告)号：US07928268B2
公开(公告)日：2011-04-19
申请号：US12805138
申请日：2010-07-14
申请人： Mingjian Qiu , Wei Zhang , Zhaohui Chen , Chunshan Zhang , Yali Zhang
发明人： Mingjian Qiu , Wei Zhang , Zhaohui Chen , Chunshan Zhang , Yali Zhang
IPC分类号： C07C41/01 , C07C43/205 , C07C39/24
CPC分类号： C07C41/16 , C07C37/00 , C07C37/02 , C07C41/01 , C07C41/26 , C07C43/23 , C07C39/27 , C07C43/225 , C07C39/245
摘要： The present invention relates to a process for producing a 2-fluoro-6-halophenol as an intermediate; a process for producing a 2-alkoxy-3-fluorophenol and further a 1,2-dialkoxy-3-fluorobenzene from the 2-fluoro-6-halophenol; a second process for producing a 1,2-dialkoxy-3-fluorobenzene from the 2-fluoro-6-halophenol; and a 2-alkoxy-3-fluorophenol. The 2-fluoro-6-halophenol can be obtained using a 2-fluorophenol as a starting material and through a sulfonation reaction, a halogenation reaction, and a deprotection reaction. The 2-fluoro-6-halophenol is alkyl-etherified, and subsequently the halogen atom is converted into a hydroxyl group to obtain the 2-alkoxy-3-fluorophenol, which is further alkyl-etherified to thereby obtain the 1,2-dialkoxy-3-fluorobenzene. Alternatively, a 1,2-dialkoxy-3-fluorobenzene is also obtained by converting the halogen atom of the 2-fluoro-6-halophenol into a hydroxyl group to thereby form 3-fluorocatechol and subsequently alkyl-etherifying two hydroxyl groups thereof. The processes of the invention realize low production costs and high process yields, and thus are suitable for industrial production of a 1,2-dialkoxy-3-fluorobenzene.
摘要翻译：本发明涉及作为中间体的2-氟-6-卤代苯酚的制造方法。从2-氟-6-卤苯酚制备2-烷氧基-3-氟苯酚和1,2-二烷氧基-3-氟苯的方法; 从2-氟-6-卤代苯酚制备1,2-二烷氧基-3-氟苯的第二种方法; 和2-烷氧基-3-氟苯酚。 2-氟-6-卤代苯酚可以使用2-氟苯酚作为原料，通过磺化反应，卤化反应和脱保护反应得到。 2-氟-6-卤代苯酚被烷基醚化，随后将卤素原子转化为羟基，得到2-烷氧基-3-氟苯酚，进一步进行烷基醚化，从而得到1,2-二烷氧基 -3-氟苯。或者，也可以通过将2-氟-6-卤代苯酚的卤素原子转化为羟基，从而形成3-氟邻苯二酚，然后将其两个羟基烷基醚化，得到1,2-二烷氧基-3-氟苯。本发明的方法实现了低生产成本和高工艺产率，因此适用于1,2-二烷氧基-3-氟苯的工业化生产。

4. 发明申请

US20100286451A1 Process for producing 1,2-dialkoxy-3-fluorobenzene 失效
标题翻译： 1,2-二烷氧基-3-氟苯的制备方法
公开(公告)号：US20100286451A1
公开(公告)日：2010-11-11
申请号：US12805138
申请日：2010-07-14
申请人： Mingjian Qiu , Wei Zhang , Zhaohui Chen , Chunshan Zhang , Yali Zhang
发明人： Mingjian Qiu , Wei Zhang , Zhaohui Chen , Chunshan Zhang , Yali Zhang
IPC分类号： C07C41/01 , C07C43/23
CPC分类号： C07C41/16 , C07C37/00 , C07C37/02 , C07C41/01 , C07C41/26 , C07C43/23 , C07C39/27 , C07C43/225 , C07C39/245
摘要： The present invention relates to a process for producing a 2-fluoro-6-halophenol as an intermediate; a process for producing a 2-alkoxy-3-fluorophenol and further a 1,2-dialkoxy-3-fluorobenzene from the 2-fluoro-6-halophenol; a second process for producing a 1,2-dialkoxy-3-fluorobenzene from the 2-fluoro-6-halophenol; and a 2-alkoxy-3-fluorophenol. The 2-fluoro-6-halophenol can be obtained using a 2-fluorophenol as a starting material and through a sulfonation reaction, a halogenation reaction, and a deprotection reaction. The 2-fluoro-6-halophenol is alkyl-etherified, and subsequently the halogen atom is converted into a hydroxyl group to obtain the 2-alkoxy-3-fluorophenol, which is further alkyl-etherified to thereby obtain the 1,2-dialkoxy-3-fluorobenzene. Alternatively, a 1,2-dialkoxy-3-fluorobenzene is also obtained by converting the halogen atom of the 2-fluoro-6-halophenol into a hydroxyl group to thereby form 3-fluorocatechol and subsequently alkyl-etherifying two hydroxyl groups thereof. The processes of the invention realize low production costs and high process yields, and thus are suitable for industrial production of a 1,2-dialkoxy-3-fluorobenzene.
摘要翻译：本发明涉及作为中间体的2-氟-6-卤代苯酚的制造方法。从2-氟-6-卤苯酚制备2-烷氧基-3-氟苯酚和1,2-二烷氧基-3-氟苯的方法; 从2-氟-6-卤代苯酚制备1,2-二烷氧基-3-氟苯的第二种方法; 和2-烷氧基-3-氟苯酚。 2-氟-6-卤代苯酚可以使用2-氟苯酚作为原料，通过磺化反应，卤化反应和脱保护反应得到。 2-氟-6-卤代苯酚被烷基醚化，随后将卤素原子转化为羟基，得到2-烷氧基-3-氟苯酚，进一步进行烷基醚化，从而得到1,2-二烷氧基 -3-氟苯。或者，也可以通过将2-氟-6-卤代苯酚的卤素原子转化为羟基，从而形成3-氟邻苯二酚，然后将其两个羟基烷基醚化，得到1,2-二烷氧基-3-氟苯。本发明的方法实现了低生产成本和高工艺产率，因此适用于1,2-二烷氧基-3-氟苯的工业生产。

5. 发明授权

US10170244B2 Fabrication of porous silicon electrochemical capacitors 有权
公开(公告)号：US10170244B2
公开(公告)日：2019-01-01
申请号：US13997881
申请日：2011-12-27
申请人： Donald S. Gardner , Cary L. Pint , Charles W. Holzwarth , Wei Jin , Zhaohui Chen , Yang Liu , Eric C. Hannah , John L. Gustafson
发明人： Donald S. Gardner , Cary L. Pint , Charles W. Holzwarth , Wei Jin , Zhaohui Chen , Yang Liu , Eric C. Hannah , John L. Gustafson
IPC分类号： H01G11/86 , H01G4/008 , H01G11/30 , H01G11/00 , H01G11/26
摘要： Methods of forming microelectronic structures are described. Embodiments of those methods may include forming an electrochemical capacitor device by forming pores in low-purity silicon materials. Various embodiments described herein enable the fabrication of high capacitive devices using low cost techniques.

6. 发明申请

US20150004471A1 ULTRAFAST RELIABLE SILICON ENABLED BATTERY AND ASSOCIATED METHODS 有权
标题翻译：超导可靠硅电池和相关方法
公开(公告)号：US20150004471A1
公开(公告)日：2015-01-01
申请号：US13931539
申请日：2013-06-28
申请人： Zhaohui Chen , Yang Liu , Charles W. Holzwarth , Nicolas Cirigliano , Bum Ki Moon
发明人： Zhaohui Chen , Yang Liu , Charles W. Holzwarth , Nicolas Cirigliano , Bum Ki Moon
IPC分类号： H01M4/66 , H01M10/04 , H01M4/48 , H01M4/36 , H01M4/38
CPC分类号： H01M4/66 , H01M4/24 , H01M4/38 , H01M4/48 , H01M4/5815 , H01M4/661 , H01M4/667 , H01M4/78 , H01M6/40 , H01M10/0436 , H01M10/287 , H01M2300/0014 , Y10T29/49115
摘要： Ultrafast battery devices having enhanced reliability and power density are provided. Such batteries can include a cathode including a first silicon substrate having a cathode structured surface, an anode including a second silicon substrate having an anode structured surface positioned adjacent to the cathode such that the cathode structured surface faces the anode structured surface, and an electrolyte disposed between the cathode and the anode. The anode structured surface can be coated with an anodic active material and the cathode structured surface can be coated with a cathodic active material.
摘要翻译：提供了具有增强的可靠性和功率密度的超快电池装置。这样的电池可以包括阴极，其包括具有阴极结构化表面的第一硅衬底，阳极，其包括具有邻近阴极定位的阳极结构化表面的第二硅衬底，使得阴极结构化表面面向阳极结构化表面，在阴极和阳极之间。阳极结构化表面可以涂覆有阳极活性材料，阴极结构化表面可以涂覆阴极活性材料。

7. 发明申请

US20150003033A1 THREE DIMENSIONAL ENERGY STORAGE DEVICE, METHOD OF MANUFACTURING SAME, AND MOBILE ELECTRONIC DEVICE CONTAINING SAME 有权
标题翻译：三维能量储存装置，其制造方法和含有其的移动电子装置
公开(公告)号：US20150003033A1
公开(公告)日：2015-01-01
申请号：US13929224
申请日：2013-06-27
申请人： Yang Liu , Priyanka Pande , Bum Ki Moon , Michael C. Graf , Donald S. Gardner , Nicolas Cirigliano , Shanthi Murali , Zhaohui Chen
发明人： Yang Liu , Priyanka Pande , Bum Ki Moon , Michael C. Graf , Donald S. Gardner , Nicolas Cirigliano , Shanthi Murali , Zhaohui Chen
IPC分类号： H01G9/048 , H01L23/50 , H01M4/52 , H01M4/04 , H01M4/485 , H01M4/505
CPC分类号： H01G11/84 , H01G11/26 , H01G11/46 , H01G11/50 , H01M2/145 , H01M2/1673 , H01M4/0421 , H01M4/0433 , H01M4/0473 , H01M4/13 , H01M4/131 , H01M4/136 , H01M4/139 , H01M4/5815 , H01M4/70 , H01M6/40 , H01M10/052 , H01M10/0565 , H01M10/058 , H01M2004/021 , H01M2004/025 , H01M2220/30 , Y02E60/13 , Y02T10/7011 , Y02T10/7022 , Y10T29/49108 , Y10T29/49115
摘要： An energy storage device includes an electrode made from an active material in which a plurality of channels have been etched. The channels are coated with an electrically functional substance selected from a conductor and an electrolyte.
摘要翻译：能量存储装置包括由多个通道被蚀刻的活性材料制成的电极。通道涂有选自导体和电解质的电功能物质。

8. 发明申请

US20140233152A1 FABRICATION OF POROUS SILICON ELECTROCHEMICAL CAPACITORS 审中-公开
标题翻译：多孔硅电化学电容器的制造
公开(公告)号：US20140233152A1
公开(公告)日：2014-08-21
申请号：US13997881
申请日：2011-12-27
申请人： Donald S. Gardner , Cary L. Pint , Charles W. Holzwarth , Wei Jin , Zhaohui Chen , Yang Liu , Eric C. Hannah , John L. Gustafson
发明人： Donald S. Gardner , Cary L. Pint , Charles W. Holzwarth , Wei Jin , Zhaohui Chen , Yang Liu , Eric C. Hannah , John L. Gustafson
IPC分类号： H01G11/86 , H01G11/30 , H01G4/008
CPC分类号： H01G4/008 , H01G11/00 , H01G11/26 , H01G11/30 , H01G11/86 , Y02E60/13 , Y10T29/41
摘要： Methods of forming microelectronic structures are described. Embodiments of those methods may include forming an electrochemical capacitor device by forming pores in low-purity silicon materials. Various embodiments described herein enable the fabrication of high capacitive devices using low cost techniques.
摘要翻译：描述形成微电子结构的方法。这些方法的实施例可以包括通过在低纯度硅材料中形成孔而形成电化学电容器装置。本文描述的各种实施例能够使用低成本技术来制造高电容性器件。

9. 发明申请

US20140185260A1 NANOSTRUCTURED ELECTROLYTIC ENERGY STORAGE DEVICES 有权
标题翻译：纳米结构电解能储存装置
公开(公告)号：US20140185260A1
公开(公告)日：2014-07-03
申请号：US13730324
申请日：2012-12-28
申请人： Zhaohui Chen , Donald S. Gardner , Bum Ki Moon , Charles W. Holzwarth , Cary L. Pint , Scott B. Clendenning
发明人： Zhaohui Chen , Donald S. Gardner , Bum Ki Moon , Charles W. Holzwarth , Cary L. Pint , Scott B. Clendenning
IPC分类号： H05K1/18
CPC分类号： H01G11/24 , G11C13/0002 , G11C13/0016 , H01L28/82 , Y02E60/13 , Y10T29/435
摘要： In one embodiment, a structure for an energy storage device may include a first nanostructured substrate having a conductive layer and a dielectric layer formed on the conductive layer. A second nanostructured substrate includes another conductive layer. A separator separates the first and second nanostructured substrates and allows ions of an electrolyte to pass through the separator. The structure may be a nanostructured electrolytic capacitor with the first nanostructured substrate forming a positive electrode and the second nanostructured substrate forming a negative electrode of the capacitor.
摘要翻译：在一个实施例中，用于能量存储装置的结构可以包括具有形成在导电层上的导电层和介电层的第一纳米结构化衬底。第二纳米结构衬底包括另一导电层。分离器分离第一和第二纳米结构的基底并允许电解质的离子通过分离器。该结构可以是纳米结构的电解电容器，其中第一纳米结构的衬底形成正电极，第二纳米结构衬底形成电容器的负极。

10. 发明授权

US10436803B2 Quantitation of insulin by tandem mass spectrometry of insulin B chain 有权
公开(公告)号：US10436803B2
公开(公告)日：2019-10-08
申请号：US13338123
申请日：2011-12-27
申请人： Zhaohui Chen , Nigel Clarke
发明人： Zhaohui Chen , Nigel Clarke
IPC分类号： G01N33/68 , G01N33/74 , G01N33/49 , H01J49/00
摘要： Methods are described for determining the amount of insulin in a sample. More specifically, mass spectrometric methods are described for detecting and quantifying insulin in a biological sample utilizing purification methods coupled with tandem mass spectrometric or high resolution/high accuracy mass spectrometric techniques.

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