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1. 发明授权

US4591575A Novel crystalline metal oxide and process for production thereof 失效
标题翻译：新型结晶金属氧化物及其生产方法
公开(公告)号：US4591575A
公开(公告)日：1986-05-27
申请号：US606610
申请日：1984-05-03
申请人： Minahiro Okabayashi , Shigeki Yuasa , Koshi Kusumoto
发明人： Minahiro Okabayashi , Shigeki Yuasa , Koshi Kusumoto
IPC分类号： C01B33/113 , A61K6/08 , A61K6/083 , B01J20/10 , B01J39/14 , C01B33/12 , C01B33/20 , C04B35/622 , C08K3/22 , C08K3/34 , C30B7/00 , C04B35/16 , C09K3/10
CPC分类号： C30B29/22 , A61K6/083 , C01B33/20 , C04B35/6224 , C04B35/62259 , C08K3/22 , C08K3/34 , C30B7/00
摘要： A crystalline metal oxide in the form of a solid solution comprising an oxide of a metal of Group II of the periodic table, titanium oxide and silicon dioxide as main components and having main peaks at about 26.7.degree. and about 20.9.degree. in its Cu-K.alpha. X-ray diffraction pattern (2.theta.) and a specific refractive index. The crystalline metal oxide is produced, for example, by dissolving a compound of a metal of Group II of the periodic table, a hydrolyzable organic silicon compound and a hydrolyzable titanium compound in an organic solvent, hydrolyzing said starting compounds in said solution or after said solution is added to a separately prepared solvent incapable of dissolving the reaction product, thereby to form a sol- or gel-like product, and thereafter calcining the sol- or gel-like product at a temperature and for a period of time sufficient to crystallize said product.
摘要翻译：固体溶液形式的结晶金属氧化物，其包含周期表第II族金属的氧化物，氧化钛和二氧化硅作为主要组分，并且在其Cu-K中具有约26.7°和约20.9°的主峰 αX射线衍射图（2θ）和特定折射率。结晶金属氧化物例如通过将有机溶剂中的元素周期表第II族金属的化合物，可水解的有机硅化合物和可水解的钛化合物溶解在所述溶液中或在所述溶液中水解所述起始化合物将溶液加入到不能溶解反应产物的单独制备的溶剂中，从而形成溶胶 - 或凝胶状产物，然后在足以结晶的温度和时间内煅烧溶胶 - 或凝胶状产物说产品。

2. 发明授权

US4764497A Amorphous, spherical inorganic compound and process for preparation thereof 失效
标题翻译：无定形球形无机化合物及其制备方法
公开(公告)号：US4764497A
公开(公告)日：1988-08-16
申请号：US804181
申请日：1985-12-03
申请人： Shigeki Yuasa , Minahiro Okabayashi , Hideki Ohno , Katsumi Suzuki , Koshi Kusumoto
发明人： Shigeki Yuasa , Minahiro Okabayashi , Hideki Ohno , Katsumi Suzuki , Koshi Kusumoto
IPC分类号： C01G17/00 , A61K6/02 , A61K6/083 , B01J20/10 , B01J21/08 , B01J35/10 , C01B33/12 , C01B33/152 , C01B33/20 , C01B33/26 , C01B35/10 , C01G19/00 , C01G23/00 , C01G25/00 , C08K3/00 , C08K3/34 , C08K3/36 , C09C1/00
CPC分类号： B01J20/10 , A61K6/0008 , A61K6/0073 , C01B33/20 , C01B33/26 , C01B35/10 , C09C1/0081 , C01P2002/02 , C01P2004/32
摘要： Disclosed is an amorphous, spherical inorganic compound having a particle size of 0.1 to 1.0 .mu.m, which comprises as main constituents (1) an oxide of at least one metal selected from the group consisting of metals of the Groups I, II, III and IV of the Periodic Table, said metal oxide being capable of combining with silicon dioxide, and (2) silica.This amorphous, spherical inorganic compound is prepared by a process comprising adding a mixed solution containing a hydrolyzable organic silicon compound and a hydrolyzable organic compound of at least one metal (M) selected from the group consisting of metals of the Groups I, II, III and IV of the Periodic Table to an alkaline solvent capable of dissolving said organic silicon compound and said organic metal compound therein but substantially incapable of dissolving a reaction product of both the organic silicon compound and the organic metal compound therein, effecting the hydrolysis to precipitate the reaction product and, if necessary, calcining the reaction product.
摘要翻译：公开了一种粒径为0.1〜1.0μm的无定形球形无机化合物，其包含主要成分（1）选自由I，II，III族金属组成的组中的至少一种金属的氧化物，以及 IV，所述金属氧化物能够与二氧化硅结合，和（2）二氧化硅。该无定形球形无机化合物是通过以下方法制备的，该方法包括加入含有可水解有机硅化合物和至少一种金属（M）的可水解有机化合物的混合溶液，所述金属选自第I，II，III族金属和IV表示为能够溶解所述有机硅化合物和所述有机金属化合物的碱性溶剂，但基本上不能溶解有机硅化合物和有机金属化合物的反应产物，从而使水解沉淀反应产物，如果需要，煅烧反应产物。

3. 发明授权

US4567030A Amorphous, spherical inorganic compound and process for preparation thereof 失效
公开(公告)号：US4567030A
公开(公告)日：1986-01-28
申请号：US452735
申请日：1982-12-23
申请人： Shigeki Yuasa , Minahiro Okabayashi , Hideki Ohno , Katsumi Suzuki , Koshi Kusumoto
发明人： Shigeki Yuasa , Minahiro Okabayashi , Hideki Ohno , Katsumi Suzuki , Koshi Kusumoto
IPC分类号： C01G17/00 , A61K6/02 , A61K6/083 , B01J20/10 , B01J21/08 , B01J35/10 , C01B33/12 , C01B33/152 , C01B33/20 , C01B33/26 , C01B35/10 , C01G19/00 , C01G23/00 , C01G25/00 , C08K3/00 , C08K3/34 , C08K3/36 , C09C1/00
CPC分类号： B01J20/10 , A61K6/0008 , A61K6/0073 , C01B33/20 , C01B33/26 , C01B35/10 , C09C1/0081 , C01P2002/02 , C01P2004/32
摘要： Disclosed is an amorphous, spherical inorganic compound having a particle size of 0.1 to 1.0 .mu.m, which comprises as main constituents (1) an oxide of at least one metal selected from the group consisting of metals of the Groups I, II, III and IV of the Periodic Table, said metal oxide being capable of combining with silicon dioxide, and (2) silica.This amorphous, spherical inorganic compound is prepared by a process comprising adding a mixed solution containing a hydrolyzable organic silicon compound and a hydrolyzable organic compound of at least one metal (M) selected from the group consisting of metals of the Groups I, II, III and IV of the Periodic Table to an alkaline solvent capable of dissolving said organic silicon compound and said organic metal compound therein but substantially incapable of dissolving a reaction product of both the organic silicon compound and the organic metal compound therein, effecting the hydrolysis to precipitate the reaction product and, if necessary, calcining the reaction product.

4. 发明授权

US5051453A Cement composition 失效
标题翻译：水泥组成
公开(公告)号：US5051453A
公开(公告)日：1991-09-24
申请号：US304200
申请日：1989-01-31
申请人： Minahiro Okabayashi , Hideki Ohno , Koshi Kusumoto
发明人： Minahiro Okabayashi , Hideki Ohno , Koshi Kusumoto
IPC分类号： A61K6/083 , C08K3/40
CPC分类号： A61K6/0835 , A61K6/0023 , C08K3/40
摘要： Disclosed in a cement composition comprising an unsaturated carboxylic acid polymer and an alkaline earth metal aluminofluorosilicate glass, wherein the alkaline earth metal aluminofluorosilicate glass comprises (a) 50 to 95% by weight of coarse particles having a spherical shape and an F/Si ratio of at least 0.1 but lower than 0.6 and having a particle size larger than 3 .mu.m but not larger than 50 .mu.m and (b) 5 to 50% by weight of fine particles having an F/Si ratio of 0.6 to 5 and a particle size of up to 3 .mu.m.This cement composition gives a cured body having a good surface gloss and a high strength, and this cement composition has a good flowability and a good workability. Accordingly, the cement composition is valuable as a dental cement composition.
摘要翻译：本发明公开了一种包含不饱和羧酸聚合物和碱土金属铝氟硅酸盐玻璃的水泥组合物，其中碱土金属铝氟硅酸盐玻璃包含（a）50至95重量％的球形和F / Si比为至少0.1但小于0.6，并且具有大于3μm但不大于50μm的粒度，和（b）5至50重量％的F / Si比为0.6至5的细颗粒和颗粒面积达3亩。该水泥组合物得到具有良好的表面光泽度和高强度的固化体，该水泥组合物具有良好的流动性和良好的加工性。因此，水泥组合物作为牙科水泥组合物是有价值的。

5. 发明授权

US5468738A Fungicide and its use 失效
标题翻译：杀菌剂及其用途
公开(公告)号：US5468738A
公开(公告)日：1995-11-21
申请号：US121319
申请日：1993-09-15
申请人： Minahiro Okabayashi , Zhi-ping Bai
发明人： Minahiro Okabayashi , Zhi-ping Bai
IPC分类号： A01N55/00 , A01N55/10 , C07F7/18 , A01N25/08 , C09D5/14
CPC分类号： C07F7/182 , A01N55/00 , C07F7/1836
摘要： A fungicide containing, as an active ingredient, a metal complex of the formula (I),[M{W--Si(OA.sup.1).sub.k A.sub.3-k.sup.2 }.sub.g ]Z.sub.f (I)wherein M, W, A.sup.1, A.sup.2, k, f, g and Z are as defined in the bore formula (I) of claim 1; and use thereof for various fungicidal substances.
摘要翻译：含有式（I）的金属络合物，[M {W-Si（OA1）kA3-k2} g] Zf（I）作为活性成分的杀真菌剂，其中M，W，A1，A2，k，f ，g和Z如权利要求1的孔式（I）所定义; 并用于各种杀真菌物质。

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