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1. 发明申请

US20060252969A1 Method for producing 2,2'-dihydroxy-biphenyls 审中-公开
标题翻译：制备2,2'-二羟基 - 联苯的方法
公开(公告)号：US20060252969A1
公开(公告)日：2006-11-09
申请号：US10558400
申请日：2004-06-02
申请人： Miguel Flores , Michael Bartsch , Robert Baumann , Gerd Haderlein , Tim Jungkamp , Jens Scheidel , Hermann Luyken , Wolfgang Siegel , Christa Meyer , Ralf Widmaier
发明人： Miguel Flores , Michael Bartsch , Robert Baumann , Gerd Haderlein , Tim Jungkamp , Jens Scheidel , Hermann Luyken , Wolfgang Siegel , Christa Meyer , Ralf Widmaier
IPC分类号： C07C39/12
CPC分类号： C07C39/15 , C07C37/11
摘要： The invention is a process for preparing tetraalkyl-substituted biphenol which comprises reacting a 2,4- or 2,6-dialkyl substituted phenol in which the alkyl groups contain 1 to 6 carbon atoms with a peroxidase enzyme in the presence of a peroxide in an aqueous medium to yield a tetraalkyl-substituted biphenol by oxidative coupling of the 2,4- or 2,6-dialkyl substituted phenol, or yielding a tetra-alkyl substituted quinone, and reducing the quinone to obtain a tetraalkyl-substituted biphenol. The invention further includes a process for preparing a tetraaryl-substituted biphenol in which the aryl groups contain 6 to 10 carbon atoms which comprises racting a 2,4 or 2,6 diarylphenol with a peroxidase enzyme to yield a tetraaryl-substituted biphenol. A process for reducing a tetraalkyl-substituted quinone to corresponding tetraalkyl-substituted biphenol which comprises reducing the quinone with a phenol in an aqueous medium at a temperature of about 60° to 120° C. is also included.
摘要翻译：本发明是一种制备四烷基取代的联苯酚的方法，该方法包括在其中含有1至6个碳原子的烷基的2,4-或2,6-二烷基取代的苯酚与过氧化物酶在过氧化物存在下反应水性介质，通过2,4-或2,6-二烷基取代酚的氧化偶合得到四烷基取代的联苯酚，或得到四烷基取代的醌，还原醌以得到四烷基取代的联苯酚。本发明还包括一种制备四芳基取代的联苯酚的方法，其中芳基含有6至10个碳原子，其包括用过氧化物酶将2,4或2,6-二芳基苯酚反应以产生四芳基取代的联苯酚。还包括将四烷基取代的醌还原成相应的四烷基取代的联苯的方法，其包括在约60-120℃的温度下在含水介质中用苯酚还原醌。

2. 发明申请

US20090131549A1 PROCESS FOR PREPARING POLYVINYLPYRROLIDONES BY SPRAY POLYMERIZATION 审中-公开
标题翻译：通过喷雾聚合制备聚乙烯吡咯烷酮的方法
公开(公告)号：US20090131549A1
公开(公告)日：2009-05-21
申请号：US12271438
申请日：2008-11-14
申请人： Dennis Losch , Ralf Widmaier , Volker Seidl , Hans-Ulrich Moritz , Karim Asif , Silke Biedasek
发明人： Dennis Losch , Ralf Widmaier , Volker Seidl , Hans-Ulrich Moritz , Karim Asif , Silke Biedasek
IPC分类号： C08F26/10
CPC分类号： C08F2/00 , C08F26/10
摘要： A process for preparing polyvinylpyrrolidones by free-radically initiated polymerization in the presence of an initiator found, which comprises performing the polymerization as a spray or droplet polymerization.
摘要翻译：在发现的引发剂的存在下，通过自由基引发的聚合制备聚乙烯吡咯烷酮的方法，其包括进行聚合作为喷雾或液滴聚合。

3. 发明申请

US20080033091A1 Stabilisation of Aqueous Solutions of Homopolymers and Copolymers of N-Vinylpyrrolidones 有权
标题翻译： N-乙烯基吡咯烷酮的均聚物和共聚物水溶液的稳定化
公开(公告)号：US20080033091A1
公开(公告)日：2008-02-07
申请号：US11576612
申请日：2005-10-06
申请人： Erik Bohrer , Dieter Faul , Ivette Castro , Norbert Gebhardt , Peter Hossel , Peter Mendera , Olga Pinneker , Bernd de Potzolli , Stefan Stein , Karl-Hermann Strube , Ralf Widmaier , Josef Neutzner , Simone Lehnert
发明人： Erik Bohrer , Dieter Faul , Ivette Castro , Norbert Gebhardt , Peter Hossel , Peter Mendera , Olga Pinneker , Bernd de Potzolli , Stefan Stein , Karl-Hermann Strube , Ralf Widmaier , Josef Neutzner , Simone Lehnert
IPC分类号： C08K3/18 , C08K3/00
CPC分类号： C08K3/18 , C08K3/014 , C08L39/06
摘要： Aqueous solutions comprising: one or more polymeric components selected from the group consisting of homopolymers of N-vinylpyrrolidone, copolymers of N-vinylpyrrolidone, and mixtures thereof; and hydrogen peroxide; wherein the hydrogen peroxide is present in an amount of 100 to 5000 ppm; and methods of stabilizing aqueous solutions containing one or more polymeric components selected from the group consisting of homopolymers of N-vinylpyrrolidone, copolymers of N-vinylpyrrolidone, and mixtures thereof.
摘要翻译：水溶液，其包含：一种或多种选自N-乙烯基吡咯烷酮的均聚物，N-乙烯基吡咯烷酮的共聚物及其混合物的聚合物组分; 和过氧化氢; 其中所述过氧化氢的存在量为100至5000ppm; 以及稳定含有一种或多种聚合物组分的水溶液的方法，所述聚合物组分选自N-乙烯基吡咯烷酮的均聚物，N-乙烯基吡咯烷酮的共聚物及其混合物。

4. 发明申请

US20070149738A1 Method of producing water-soluble nonturbid copolymers of at least one water-soluble N-vinyllactam and at least one hydrophobic comonomer 有权
标题翻译：制备至少一种水溶性N-乙烯基内酰胺和至少一种疏水性共聚单体的水溶性非混浊共聚物的方法
公开(公告)号：US20070149738A1
公开(公告)日：2007-06-28
申请号：US11643396
申请日：2006-12-21
申请人： Rainer Dobrawa , Ralf Widmaier , Eberhard Schupp , Klaus Schnell
发明人： Rainer Dobrawa , Ralf Widmaier , Eberhard Schupp , Klaus Schnell
IPC分类号： C08F26/10
CPC分类号： C08F226/10 , C08F216/10
摘要： Method of producing vinyllactam copolymers by free-radical polymerization of at least one water-soluble N-vinyllactam and at least one hydrophobic comonomer in an organic solvent in the presence of an initiator under reflux conditions, where the initiator is introduced into the polymerization mixture from below.
摘要翻译：通过至少一种水溶性N-乙烯基内酰胺和至少一种疏水性共聚单体在引发剂存在下，在回流条件下，在引发剂存在下，在有机溶剂中自由基聚合制备乙烯基内酰胺共聚物的方法，其中将引发剂从下面。

5. 发明申请

US20070129578A1 Method for the production of 2,2'-dihydroxybiphenyls 审中-公开
标题翻译： 2,2'-二羟基联苯的制备方法
公开(公告)号：US20070129578A1
公开(公告)日：2007-06-07
申请号：US10576694
申请日：2004-10-21
申请人： Ralf Widmaier , Bettina Muller , Marianna Pierobon
发明人： Ralf Widmaier , Bettina Muller , Marianna Pierobon
IPC分类号： C07C39/12
CPC分类号： C07C37/11 , C07C39/15
摘要： A process for the preparation of a 2,2′-dihydroxybiphenyl by oxidative coupling of two phenyl molecules which have a hydrogen atom in an o-position by means of a peroxide in the presence of water at from 0 to 100° C., wherein the preparation is carried out in the presence of a water-insoluble polymer comprising a) from 0 to less than 100% by weight of a vinyl heterocycle b) from 0 to 10% by weight of a difunctional crosslinking component c) from 0 to less than 100% by weight of styrene or of a monounsaturated styrene derivative or a mixture thereof d) from 0 to 100% by weight of a N-vinylamide of an aliphatic carboxylic acid, or the monomers obtained by hydrolysis of said amido group e) from 0 to 100% by weight of a vinylcarboxylic acid or the esters, amides or salts thereof, or the monomers obtained by hydrolysis of said amido group or ester group, with the proviso that the content of compound d) or e), or d) and e), is more than 0% by weight.
摘要翻译：通过在0〜100℃的水存在下，借助于过氧化物，在两个位置上具有氢原子的两个苯基分子的氧化偶合来制备2,2'-二羟基联苯的方法，其中该制备在水不溶性聚合物的存在下进行，该水不溶性聚合物包含a）0至小于100重量％的乙烯基杂环b）0至10重量％的双官能交联组分c）0至少 100重量％的苯乙烯或单不饱和的苯乙烯衍生物或其混合物; d）0-100重量％的脂族羧酸的N-乙烯基酰胺，或通过所述酰氨基的水解获得的单体e） 0至100重量％的乙烯基羧酸或其酯，酰胺或盐，或通过水解所述酰胺基或酯基获得的单体，条件是化合物d）或e）的含量，或d）和e）大于0重量％。

6. 发明申请

US20100029854A1 THERMOPLASTIC POLYMER-BASED SOLID DISPERSIONS SUITABLE AS FILTER AIDS 审中-公开
标题翻译：基于热塑性聚合物的固体分散体适合作为过滤器的艾滋病
公开(公告)号：US20100029854A1
公开(公告)日：2010-02-04
申请号：US12515109
申请日：2007-12-03
申请人： Klemens Mathauer , Marianna Pierobon , Simone Schillo , Ralf Widmaier
发明人： Klemens Mathauer , Marianna Pierobon , Simone Schillo , Ralf Widmaier
IPC分类号： C08L39/06
CPC分类号： C12H1/0424 , B01J20/26 , B01J20/261 , B01J20/262 , B01J2220/445
摘要： Solid dispersions of thermoplastic polymers and a crosslinked water-insoluble polymer, which solid dispersions are suitable as filter aids, wherein the solid dispersions comprise 20 to 95% by weight of at least one thermoplastic polymer (component A) and 5 to 80% by weight of at least one crosslinked water-insoluble polymer selected from the group consisting of homopolymers of N-vinylformamide, N-vinylcaprolactam, N-vinylpiperidone, N-vinylpyridines, N-vinylimidazoles, styrene monomers, acrylates and methacrylates and also copolymers of basic N-vinyl compounds, styrene monomers, acrylates and methacrylates (component B).
摘要翻译：热塑性聚合物和交联的水不溶性聚合物的固体分散体，该固体分散体适合作为助滤剂，其中固体分散体包含20至95重量％的至少一种热塑性聚合物（组分A）和5至80重量％的至少一种交联的水不溶性聚合物，其选自N-乙烯基甲酰胺，N-乙烯基己内酰胺，N-乙烯基哌啶酮，N-乙烯基吡啶，N-乙烯基咪唑，苯乙烯单体，丙烯酸酯和甲基丙烯酸酯的均聚物，以及碱式N- 乙烯基化合物，苯乙烯单体，丙烯酸酯和甲基丙烯酸酯（组分B）。

7. 发明授权

US07572871B2 Method of producing water-soluble nonturbid copolymers of at least one water-soluble N-vinyllactam and at least one hydrophobic comonomer 有权
标题翻译：制备至少一种水溶性N-乙烯基内酰胺和至少一种疏水性共聚单体的水溶性非混浊共聚物的方法
公开(公告)号：US07572871B2
公开(公告)日：2009-08-11
申请号：US11643396
申请日：2006-12-21
申请人： Rainer Dobrawa , Ralf Widmaier , Eberhard Schupp , Klaus Schnell
发明人： Rainer Dobrawa , Ralf Widmaier , Eberhard Schupp , Klaus Schnell
IPC分类号： C08F26/10 , C08F2/06
CPC分类号： C08F226/10 , C08F216/10
摘要： Method of producing vinyllactam copolymers by free-radical polymerization of at least one water-soluble N-vinyllactam and at least one hydrophobic comonomer in an organic solvent in the presence of an initiator under reflux conditions, where the initiator is introduced into the polymerization mixture from below.
摘要翻译：通过至少一种水溶性N-乙烯基内酰胺和至少一种疏水性共聚单体在引发剂存在下，在回流条件下，在引发剂存在下，在有机溶剂中自由基聚合制备乙烯基内酰胺共聚物的方法，其中将引发剂从下面。

8. 发明授权

US07449531B2 Method of producing water-soluble nonturbid copolymers of at least one water-soluble N-vinyllactam and at least one hydrophobic comonomer 有权
标题翻译：制备至少一种水溶性N-乙烯基内酰胺和至少一种疏水性共聚单体的水溶性非混浊共聚物的方法
公开(公告)号：US07449531B2
公开(公告)日：2008-11-11
申请号：US11644480
申请日：2006-12-22
申请人： Rainer Dobrawa , Ralf Widmaier , Eberhard Schupp , Klaus Schnell , Martin Meister
发明人： Rainer Dobrawa , Ralf Widmaier , Eberhard Schupp , Klaus Schnell , Martin Meister
IPC分类号： C08F26/10 , C08F218/08
CPC分类号： C08F226/10 , C08F216/10
摘要： Method of producing vinyllactam copolymers by free-radical polymerization of at least one water-soluble N-vinyllactam and at least one hydrophobic comonomer in an organic solvent in the presence of an initiator under reflux conditions, where the condensate formed in the reflux is returned to the polymerization mixture from below.
摘要翻译：通过至少一种水溶性N-乙烯基内酰胺和至少一种疏水性共聚单体在有机溶剂中，在引发剂存在下，在回流条件下，在回流条件下形成的缩合物返回至聚合混合物从下面。

9. 发明申请

US20080139724A1 Method For the Stabilization of Polyvinylpyrrolidones 有权
标题翻译：聚乙烯吡咯烷酮的稳定化方法
公开(公告)号：US20080139724A1
公开(公告)日：2008-06-12
申请号：US11815478
申请日：2006-02-08
申请人： Karl Kolter , Ivette Garcia Castro , Olga Pinneker , Ralf Widmaier , Karl-Hermann Strube , Bernhard Fussnegger , Manfred Kroll , Frank Hofer , Hermann Ascherl , Peter Schmidt
发明人： Karl Kolter , Ivette Garcia Castro , Olga Pinneker , Ralf Widmaier , Karl-Hermann Strube , Bernhard Fussnegger , Manfred Kroll , Frank Hofer , Hermann Ascherl , Peter Schmidt
IPC分类号： C08L39/06 , C08K3/30
CPC分类号： C08K5/005 , C08F6/06 , C08K3/30 , C08K5/1535 , C08K2003/309 , C08K2201/014 , C08L39/06
摘要： Method for stabilizing polyvinylpyrrolidones, which comprises treating the polyvinylpyrrolidones with sulfur dioxide, sulfurous acid or alkali metal sulfites and then with free-radical scavenger, and converting the solutions treated in this way into the powdered polyvinylpyrrolidones by drying.
摘要翻译：用于稳定聚乙烯吡咯烷酮的方法，其包括用二氧化硫，亚硫酸或碱金属亚硫酸盐处理聚乙烯吡咯烷酮，然后用自由基清除剂处理聚乙烯吡咯烷酮，然后通过干燥将以这种方式处理的溶液转化成粉末状聚乙烯吡咯烷酮。

10. 发明申请

US20070154438A1 Method for producing a water-in-water polyvinyl lactam dispersion with a k value of = 120 审中-公开
标题翻译：水溶液聚乙烯内酰胺分散体的制造方法，k值= 120
公开(公告)号：US20070154438A1
公开(公告)日：2007-07-05
申请号：US10591654
申请日：2005-04-14
申请人： Lysander Chrisstoffels , Ralf Widmaier , Ivette Castro , Ludger Wegmann
发明人： Lysander Chrisstoffels , Ralf Widmaier , Ivette Castro , Ludger Wegmann
IPC分类号： A61K8/81 , C08F26/10 , C08F26/08
CPC分类号： C08F26/10
摘要： Method for producing water-in-water polyvinyl lactam dispersions with a K value of =120 by radical polymerisation.
摘要翻译：通过自由基聚合制备K值= 120的水包水聚乙烯内酰胺分散体的方法。

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