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1. 发明授权

US4145305A Phosphorus activators for percompounds 失效
标题翻译：磷酸盐激活剂
公开(公告)号：US4145305A
公开(公告)日：1979-03-20
申请号：US802515
申请日：1977-06-01
申请人： Michel Demarcq , Michel Bakes , Marie-Christine Daude-Lagrave
发明人： Michel Demarcq , Michel Bakes , Marie-Christine Daude-Lagrave
IPC分类号： C09K3/00 , C07F9/50 , C07F9/54 , C11D3/36 , C11D3/39 , D06L3/02 , C11D3/395 , C11D7/54
CPC分类号： D06L3/021 , C07F9/5004 , C07F9/5407 , C11D3/36 , C11D3/393
摘要： Phosphorus-containing activators for percompounds, the activators being tris(acetoxymethyl) phosphine oxide and its precursors including tris(acetoxymethyl) phosphine and tetrakis(acetoxymethyl) phosphonium compounds, together with the use of such activators with percompounds for oxidizing or bleaching such as in bleaching fibers, oils, fats, and waxes, cosmetological treatment of hair and skin, metallic surface passivation, and purification, disinfection and sterilization techniques, the use of such activators providing more rapid action at a given temperature or equal activity at a lower temperature.

2. 发明授权

US4169118A Phosphorus derivatives of pentaerythritol monobromohydrin 失效
标题翻译：季戊四醇单溴醇的磷衍生物
公开(公告)号：US4169118A
公开(公告)日：1979-09-25
申请号：US803769
申请日：1977-06-06
申请人： Michel Demarcq
发明人： Michel Demarcq
IPC分类号： C07F9/6574 , C08K5/52 , C07F9/40
CPC分类号： C08K5/52 , C07F9/65748
摘要： Novel bicyclic phosphorus derivatives of 2,2-di(hydroxymethyl)-3-bromopropanol having the formula ##STR1## WHERE X IS ZERO OR ONE, NOVEL POLYPHOSPHONATE DERIVATIVES OF THE PHOSPHITE DERIVATIVES OBTAINED BY Michaelis-Arbuzov condensation and other processes; and processes for preparing such novel compounds, the bicyclic derivatives being useful as plastic stabilizers, fireproofing agents and intermediates and the polyphosphonates being useful as fireproofing agents for polymers and textiles.
摘要翻译：具有下式的图像的2-二（羟甲基）-3-溴丙醇的新型双环磷衍生物：其中X是ZERO或ONE，由Michaelis-Arbuzov缩合和其它方法获得的磷酸衍生物的新型多磷酸衍生物; 以及制备这种新化合物的方法，双环衍生物可用作塑料稳定剂，防火剂和中间体，并且聚膦酸盐可用作聚合物和纺织品的防火剂。

3. 发明授权

US4104309A Phosphine oxides having polyfluorinated-chain and their preparation 失效
标题翻译：具有多氟化链的氧化膦及其制备方法
公开(公告)号：US4104309A
公开(公告)日：1978-08-01
申请号：US537446
申请日：1975-01-03
申请人： Joseph Sleziona , Michel Demarcq
发明人： Joseph Sleziona , Michel Demarcq
IPC分类号： B01F17/14 , A62D1/00 , B01J31/00 , B29B13/00 , B29C33/00 , B29C33/62 , C07F9/53 , C09D5/00 , C09D5/02 , C09D7/00 , C09D7/12 , C09G1/00 , C09K3/00 , C09K21/12
CPC分类号： C07F9/5304
摘要： This invention relates to new products comprising at least one isomer of polyfluorinated-chain phosphine oxide with the general formula (I):c.sub.n F.sub.2n+1 (C.sub.2 H.sub.4) PO (CH.sub.3).sub.2 (I)and complying with one of the developed formulae II or III : ##STR1## in which C.sub.n F.sub.2n+1 represents a perfluorinated aliphatic chain, n lying between 2 and 18.The invention further relates to methods of obtaining the phosphine oxides of formula I.
摘要翻译：本发明涉及包含至少一种具有通式（I）的多氟化膦氧化物异构体的新产品：

4. 发明授权

US4034022A Phosphoric esters of polyfluorinated alcohols, and their preparation 失效
标题翻译：多氟醇的磷酸酯及其制备方法
公开(公告)号：US4034022A
公开(公告)日：1977-07-05
申请号：US206512
申请日：1971-12-09
申请人： Michel Demarcq , Joseph Sleziona
发明人： Michel Demarcq , Joseph Sleziona
IPC分类号： C07F9/09 , C07F9/14 , C07F9/24 , C08F2/22 , C11D1/00 , C07F9/12
CPC分类号： C11D1/006 , C07F9/091 , C07F9/14 , C07F9/2408
摘要： Phosphoric esters of polyfluorinated alcohols are disclosed comprising at least one isomer of phosphorous esters of polyfluorinated alcohols, or one of the derivatives thereof, said esters and derivatives thereof corresponding to the general formula: ##STR1## said two isomers corresponding to formulae (II) and (III): ##STR2## wherein C.sub.n F.sub.2n.sub.+1 is a perfluorinated aliphatic chain, n is an integer from 2 to 18, X and Y are the same or different and are each a halogen atom, a hydroxy radical, the group OM in which M is a metallic equivalent, or an alkoxy, chloroalkoxy, hydroxypolyalkylenoxy, aryloxy, or --NZZ' group in which Z and Z' are the same or different and are each a hydrogen atom or an alkyl, cycloalkyl or aryl group.The preparation of phosphoric esters having the general formula (I) and mixtures of the isomers (II) and (III) thereof are also disclosed.
摘要翻译：公开了多氟化醇的磷酸酯，其包含多氟醇的磷酯的至少一种异构体或其衍生物之一，所述酯及其衍生物对应于以下通式：（I）所述两种对应于式 II）和（III）：其中CnF2n + 1是全氟化脂族链，n是2至18的整数，X和Y各自相同或不同，卤素原子，羟基，其中M为金属当量的基团OM，或其中Z和Z'相同或不同且分别为氢的烷氧基，氯代烷氧基，羟基聚亚烷基氧基，芳氧基或-NZZ'基团原子或烷基，环烷基或芳基。

5. 发明授权

US4083899A Accelerated process of alcoholysis or phenolysis of phosporus pentasulfide 失效
标题翻译：咖啡醇或五硫化磷溶液的加速过程
公开(公告)号：US4083899A
公开(公告)日：1978-04-11
申请号：US659096
申请日：1976-02-18
申请人： Michel Demarcq
发明人： Michel Demarcq
IPC分类号： C07F9/165
CPC分类号： C07F9/165
摘要： New process of alcoholysis or phenolysis of P.sub.2 S.sub.5 in the presence of a catalyst having one of the following structures:(A) X(Y).sub.n NQQ' having 1 to 20 C-atoms and 1 to 10 heteroatoms O, S, N or P; X, Q and Q' are hydrogen or univalent hydrocarbon radicals or form rings together; Y is O, S or a bivalent nitrogen or phosphorus radical; n = 0 or 1.(B) (X').sub.m (Y).sub.n N.dbd.Z having 1 to 20 C-atoms and 1 to 10 heteroatoms O, S, N or P; m = 0 or 1; X' has the same meaning as X or is equivalent to --N.dbd.Z or --NQQ'; Z is O, S or a bivalent carbon or hydrocarbon radical, which may form a ring with X'.(c) x(y).sub.n --C.dbd.N with 0 to 20 C-atoms and 1 to 6 heteroatoms O, S, N or P.Application to the preparation of dialkyl- or diaryldithiophosphoric acids used to manufacture phosphorus insecticides, dopes for lubricants, ore flotation agents etc.
摘要翻译：在具有以下结构之一的催化剂存在下，新的P2S5醇解或酚解的方法：

6. 发明授权

US4059656A Processes for neutralizing 2,3-dibromopropanol phosphoric acid esters contained in tris(2,3-dibromo-1-propyl) phosphate 失效
标题翻译：用于中和三（2,3-二溴-1-丙基）磷酸酯中所含的2,3-二溴丙醇磷酸酯的方法
公开(公告)号：US4059656A
公开(公告)日：1977-11-22
申请号：US672988
申请日：1976-04-02
申请人： Michel Demarcq
发明人： Michel Demarcq
IPC分类号： C07F9/09
CPC分类号： C07F9/091
摘要： Processes for the neutralization of tris(2,3-dibromo-1-propyl) phosphate containing certain quantities of phosphoric acidity, and possibly halohydric acidity, which processes comprise heating the phosphate with at least one carbon-containing orthoester, the tris(2,3-dibromo-1-propyl) phosphate so produced being adapted for use as a flame- or fireproofing agent in plastics, synthetic fibers, and paints.
摘要翻译：含有一定量磷酸的三（2,3-二溴-1-丙基）磷酸酯中和可能的卤代酸的方法，该方法包括用至少一种含碳原酸酯加热磷酸盐，该三（2， 3-二溴-1-丙基）磷酸酯，适用于塑料，合成纤维和油漆中的阻燃剂或防火剂。

7. 发明授权

US4029722A Polyfluoroalkyl glycol monoesters of orthophosphoric acid, and their salts and method of preparation 失效
标题翻译：正磷酸的多氟烷基二醇单酯及其盐和制备方法
公开(公告)号：US4029722A
公开(公告)日：1977-06-14
申请号：US462549
申请日：1974-04-19
申请人： Michel Demarcq , Joseph Sleziona
发明人： Michel Demarcq , Joseph Sleziona
IPC分类号： B01F17/14 , B01F17/38 , C07F9/09
CPC分类号： C07F9/091
摘要： New monoesters of phosphoric acid with polyfluorinated glycols having the formulasC.sub.n F.sub.2n.sub.+1 CHYCH.sub.2 --OP(O)(OH).sub.2 ##STR1## wherein Y is hydroxyl, can be prepared by alkaline saponification of the corresponding compounds wherein Y is chlorine. The new diacid monoesters and their salts are effective surfactants, unexpectedly stable in alkaline media.
摘要翻译：具有式CnF2n + 1CHYCH2-OP（O）（OH）2，其中Y是羟基的磷酸的新单酯可以通过碱性皂化其中Y是氯的相应化合物来制备。新的二酸单酯及其盐是有效的表面活性剂，在碱性介质中出人意料地稳定。

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