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1. 发明授权

US5274057A Bead suspension polymerization process 失效
标题翻译：珠悬浮聚合工艺
公开(公告)号：US5274057A
公开(公告)日：1993-12-28
申请号：US812082
申请日：1991-12-23
申请人： Michael K. Georges , Robert D. Bayley , Lupu Alexandru
发明人： Michael K. Georges , Robert D. Bayley , Lupu Alexandru
IPC分类号： C08F2/20 , C08F236/10
CPC分类号： C08F2/20 , C08F236/10
摘要： An improved process for producing resin particles by a bead suspension polymerization reaction, and a polymer formed by the process wherein the process comprises: providing a liquid reaction medium suitable for conducting the polymerization; forming a suspension agent system in the reaction medium by an in situ interaction of at least two components in the reaction medium, for example, certain water soluble metal halides and polyvinylacetate derived polymers; adding at least one polymerizable monomer compound to the resulting reaction medium having the suspension agent system dispersed therein; and effecting polymerization of the monomer in the reaction medium to form low ash content beads of the polymer.A second embodiment comprises conducting a bead suspension polymerization process utilizing the suspension agent system formed in situ to limit the amount of fine particles of less than about 100 microns produced during the process comprising: providing a reaction medium suitable for conducting the polymerization in the reaction system; utilizing a suspension agent system which is appropriate for forming polymer beads having a desired size and for minimizing fine particle formation; adding at least one polymerizable monomer compound to the resulting reaction medium having the suspension agent system dispersed therein; effecting polymerization of the monomer in the reaction medium to form the beads of the polymer; and separating resin particles from the reaction followed by optional washing and drying.
摘要翻译：通过珠粒悬浮聚合反应制备树脂颗粒的改进方法和通过该方法形成的聚合物，其中所述方法包括：提供适于进行聚合的液体反应介质; 在反应介质中通过反应介质中至少两种组分的原位相互作用形成悬浮剂体系，例如某些水溶性金属卤化物和聚乙酸乙烯酯衍生的聚合物; 向其中分散有悬浮剂体系的所得反应介质中加入至少一种可聚合单体化合物; 并且在反应介质中进行单体的聚合以形成聚合物的低灰分珠粒。第二实施方案包括使用原位形成的悬浮剂体系进行珠粒悬浮聚合方法，以限制在该方法期间产生的小于约100微米的细颗粒的量，其包括：提供适于在反应体系中进行聚合的反应介质 ; 利用适于形成具有所需尺寸的聚合物珠粒并用于最小化细颗粒形成的悬浮剂体系; 向其中分散有悬浮剂体系的所得反应介质中加入至少一种可聚合单体化合物; 在反应介质中进行单体的聚合以形成聚合物的珠粒; 并从反应中分离树脂颗粒，然后任选地洗涤和干燥。

2. 发明申请

US20110053076A1 SUPERCRITICAL FLUID MICROENCAPSULATION OF DYE INTO LATEX FOR IMPROVED EMULSION AGGREGATION TONER 有权
标题翻译：超临界流体显微镜显影改良乳化聚集体
公开(公告)号：US20110053076A1
公开(公告)日：2011-03-03
申请号：US12546847
申请日：2009-08-25
申请人： Maura A. Sweeney , Grazyna Kmiecik-Lawrynowicz , Robert D. Bayley
发明人： Maura A. Sweeney , Grazyna Kmiecik-Lawrynowicz , Robert D. Bayley
IPC分类号： G03G9/087 , C08J3/215 , G03G9/00
CPC分类号： C08J3/03 , G03G9/0806 , G03G9/0812 , G03G9/08702 , G03G9/08706 , G03G9/08711 , G03G9/08728 , G03G9/08731 , G03G9/08733 , G03G9/08735 , G03G9/09 , G03G9/0926 , G03G9/09364 , G03G9/09378 , G03G9/09392 , Y02P20/544
摘要： The present disclosure provides methods for incorporating a dye into latex particles via a supercritical fluid microencapsulation technique, in order to achieve improved dispersion of a colorant in the latex and an increase in color gamut.
摘要翻译：本公开提供了通过超临界流体微胶囊化技术将染料掺入胶乳颗粒中的方法，以便实现改善着色剂在胶乳中的分散和色域的增加。

3. 发明申请

US20080299478A1 Toner compositions 有权
标题翻译：调色剂组合物
公开(公告)号：US20080299478A1
公开(公告)日：2008-12-04
申请号：US11809058
申请日：2007-05-31
申请人： Robert D. Bayley , Timothy L. Lincoln , Kevin F. Marcell , Grazyna E. Kmiecik-Lawrynowicz , Maura A. Sweeney , Daniel W. Asarese , Chieh-Min Cheng , Zhen Lai
发明人： Robert D. Bayley , Timothy L. Lincoln , Kevin F. Marcell , Grazyna E. Kmiecik-Lawrynowicz , Maura A. Sweeney , Daniel W. Asarese , Chieh-Min Cheng , Zhen Lai
IPC分类号： G03G9/087
CPC分类号： G03G9/0806 , C08F2/24 , G03G9/0819 , G03G9/08733
摘要： The present disclosure provides processes for reducing the particle size of latex resins and toners produced with such resins. In embodiments, a carboxylic acid may be added to materials utilized to produce a latex and reduce the particle size of the resulting latex particles and toner particles. In accordance with the present disclosure, one may be able to utilize materials for the production of latex resins and toners which may otherwise produce particles that are too large in the absence of the carboxylic acid.
摘要翻译：本公开提供了降低由这种树脂制备的胶乳树脂和调色剂的粒度的方法。在实施方案中，可以将羧酸加入用于生产胶乳的材料中，并降低所得胶乳颗粒和调色剂颗粒的粒度。根据本公开内容，可以使用材料来生产胶乳树脂和调色剂，否则可能在不存在羧酸的情况下产生过大的颗粒。

4. 发明授权

US06451495B1 Toner and developer compositions with charge enhancing additives 有权
标题翻译：具有电荷增强添加剂的调色剂和显影剂组合物
公开(公告)号：US06451495B1
公开(公告)日：2002-09-17
申请号：US09850075
申请日：2001-05-07
申请人： Robert D. Bayley , Angelo J. Barbetta
发明人： Robert D. Bayley , Angelo J. Barbetta
IPC分类号： G03G9097
CPC分类号： G03G9/09791
摘要： A toner comprised of resin, colorant, and a potassium stearate charge enhancing additive.
摘要翻译：由树脂，着色剂和硬脂酸钾充电添加剂组成的调色剂

5. 发明授权

US06426170B1 Toner and developer compositions with charge enhancing additives 有权
标题翻译：具有电荷增强添加剂的调色剂和显影剂组合物
公开(公告)号：US06426170B1
公开(公告)日：2002-07-30
申请号：US09850256
申请日：2001-05-07
申请人： Robert D. Bayley , Angelo J. Barbetta
发明人： Robert D. Bayley , Angelo J. Barbetta
IPC分类号： G03G900
CPC分类号： G03G9/09766 , G03G9/08711 , G03G9/09725 , G03G9/09741 , G03G9/0975 , G03G9/09783
摘要： A toner containing resin, colorant, and a potassium sorbate, or a potassium tartrate charge enhancing additive.
摘要翻译：含有树脂，着色剂和山梨酸钾的调色剂或酒石酸钾加料添加剂。

6. 发明授权

US6127080A Polyester process 有权
公开(公告)号：US6127080A
公开(公告)日：2000-10-03
申请号：US522734
申请日：2000-03-10
申请人： Guerino G. Sacripante , Daniel A. Foucher , J. Stephen Kittelberger , Dongming Li , Marko D. Saban , Alan E. J. Toth , Robert D. Bayley
发明人： Guerino G. Sacripante , Daniel A. Foucher , J. Stephen Kittelberger , Dongming Li , Marko D. Saban , Alan E. J. Toth , Robert D. Bayley
IPC分类号： C08G63/52 , C08G63/58 , C08G63/676 , C08G63/78 , C08G63/83 , G03G9/087 , G03G9/00 , C08G63/00
CPC分类号： C08G63/58 , C08G63/676 , G03G9/08755 , C08G63/83
摘要： A process for the preparation of an unsaturated polyester which comprises (i) reacting an organic diol with a cyclic akylene carbonate in the presence of a first catalyst to thereby form a polyalkoxy diol, and (ii) optionally adding thereto a further amount of cyclic alkylene carbonate in the presence of a second catalyst, and (iii) subsequently polycondensing the resulting mixture with a dicarboxylic acid.

7. 发明授权

US5548059A Unsaturated polyesters 失效
公开(公告)号：US5548059A
公开(公告)日：1996-08-20
申请号：US367609
申请日：1995-01-03
申请人： Robert D. Bayley , Carol A. Fox , Thomas R. Hoffend , Hadi K. Mahabadi , Enno E. Agur , Guerino Sacripante , Michael S. Hawkins
发明人： Robert D. Bayley , Carol A. Fox , Thomas R. Hoffend , Hadi K. Mahabadi , Enno E. Agur , Guerino Sacripante , Michael S. Hawkins
IPC分类号： C08G63/547 , G03G9/087 , C08G63/18
CPC分类号： C08G63/547 , G03G9/08755 , G03G9/08791 , G03G9/08793 , G03G9/08797
摘要： Unsaturated linear polymers have repeating units of a reaction product of a first monomer, a second monomer, a third monomer and optionally a fourth monomer. The linear polymers have a glass transition temperature ranging from about 52.degree. C. to about 61.degree. C. The first monomer should have a weight average molecular weight less than 200. The second monomer may be a dicarboxylic acid or diester which is different than the third monomer. A concentration of second residues of the polymer, derived from the second monomer, ranges from about 3 wt. % to about 15 wt. %, based on the total weight of the polymer. The third monomer is an aromatic dicarboxylic acid or an ester thereof. In the polymer, a concentration of third residues, derived from the third monomer, ranges from about 40 wt. % to about 55 wt. %, based on the total weight of the polymer. The fourth monomer is a diol having a higher molecular weight than the first monomer. In a process for preparing the inventive polymer, the first, second, third monomer (and optionally a fourth monomer) and/or a catalyst undergo transesterification to form the unsaturated, linear polymer.

8. 发明授权

US5407772A Unsaturated polyesters 失效
标题翻译：不饱和聚酯
公开(公告)号：US5407772A
公开(公告)日：1995-04-18
申请号：US159176
申请日：1993-11-30
申请人： Robert D. Bayley , Carol A. Fox , Thomas R. Hoffend , Hadi K. Mahabadi , Enno E. Agur , Guerino Sacripante , Michael S. Hawkins
发明人： Robert D. Bayley , Carol A. Fox , Thomas R. Hoffend , Hadi K. Mahabadi , Enno E. Agur , Guerino Sacripante , Michael S. Hawkins
IPC分类号： C08G63/547 , G03G9/087 , G03G9/00
CPC分类号： C08G63/547 , G03G9/08755 , G03G9/08791 , G03G9/08793 , G03G9/08797
摘要： Unsaturated linear polymers have repeating units of a reaction product of a first monomer, a second monomer, a third monomer and optionally a fourth monomer. The linear polymers have a glass transition temperature ranging from about 52.degree. C. to about 61.degree. C. The first monomer should have a weight average molecular weight less than 200. The second monomer may be a dicarboxylic acid or diester which is different than the third monomer. A concentration of second residues of the polymer, derived from the second monomer, ranges from about 3 wt. % to about 15 wt. %, based on the total weight of the polymer. The third monomer is an aromatic dicarboxylic acid or an ester thereof. In the polymer, a concentration of third residues, derived from the third monomer, ranges from about 40 wt. % to about 55 wt. %, based on the total weight of the polymer. The fourth monomer is a diol having a higher molecular weight than the first monomer. In a process for preparing the inventive polymer, the first, second, third monomer (and optionally a fourth monomer) and/or a catalyst undergo transesterification to form the unsaturated, linear polymer.
摘要翻译：不饱和线性聚合物具有第一单体，第二单体，第三单体和任选的第四单体的反应产物的重复单元。线性聚合物的玻璃化转变温度为约52℃至约61℃。第一单体应具有小于200的重均分子量。第二单体可以是二羧酸或二酯，其不同于第三单体。衍生自第二单体的聚合物的第二残余物的浓度范围为约3wt。％至约15wt。％，基于聚合物的总重量。第三单体是芳族二羧酸或其酯。在聚合物中，衍生自第三单体的第三残基的浓度范围为约40wt。％至约55wt。％，基于聚合物的总重量。第四单体是分子量高于第一单体的二醇。在制备本发明聚合物的方法中，第一，第二，第三单体（和任选的第四单体）和/或催化剂进行酯交换以形成不饱和的线性聚合物。

9. 发明授权

US5166029A Toner and developer compositions with charge enhancing additives 失效
标题翻译：具有电荷增强添加剂的调色剂和显影剂组合物
公开(公告)号：US5166029A
公开(公告)日：1992-11-24
申请号：US775869
申请日：1991-10-15
申请人： Robert D. Bayley , Thomas R. Hoffend
发明人： Robert D. Bayley , Thomas R. Hoffend
IPC分类号： G03G9/097
CPC分类号： G03G9/09741 , G03G9/0975
摘要： A toner composition comprised of resin particles, pigment particles, and a charge enhancing additive as represented by the following formula ##STR1## wherein R.sub.1 and R.sub.2 are independently selected from the group consisting of alkyl, and R.sub.3 is an aromatic group, and m represents the number of repeating segments.
摘要翻译：由以下结构式表示的树脂颗粒，颜料颗粒和电荷增强添加剂组成的调色剂组合物，其中R 1和R 2独立地选自烷基，R 3是芳基，m表示重复段的数量。

10. 发明授权

US08785102B2 Toner compositions 有权
标题翻译：调色剂组合物
公开(公告)号：US08785102B2
公开(公告)日：2014-07-22
申请号：US13453542
申请日：2012-04-23
申请人： Robert D. Bayley , Maura A. Sweeney , Grazyna E. Kmiecik-Lawrynowicz , Daniel W. Asarese
发明人： Robert D. Bayley , Maura A. Sweeney , Grazyna E. Kmiecik-Lawrynowicz , Daniel W. Asarese
IPC分类号： G03G9/08
CPC分类号： G03G9/09708 , G03G9/0804 , G03G9/0819 , G03G9/0823 , G03G9/0827 , G03G9/08797
摘要： A toner having charge control agents which impart excellent triboelectric charging characteristics. In embodiments, the toner particles are made by a process in which charge control agent is added and adhered to the particle surface through washing steps and is maintained through the drying steps. The process of the present embodiments impart desirable charging characteristics to the toner particles.
摘要翻译：具有赋予优异摩擦带电特性的电荷控制剂的调色剂。在实施方案中，调色剂颗粒通过其中加入电荷控制剂并通过洗涤步骤粘附到颗粒表面并通过干燥步骤维持的方法制备。本实施例的方法赋予调色剂颗粒所需的充电特性。

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