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1. 发明授权

US5852140A Semisuspension polymerization processes 失效
标题翻译：半悬浮聚合工艺
公开(公告)号：US5852140A
公开(公告)日：1998-12-22
申请号：US37192
申请日：1993-03-25
申请人： Michael K. Georges , Raj D. Patel
发明人： Michael K. Georges , Raj D. Patel
IPC分类号： C08F2/00 , C08F2/02 , C08F2/16 , C08F4/00
CPC分类号： C08F2/001 , C08F4/00
摘要： Disclosed is a process for the preparation of a polymer which comprises effecting bulk polymerization of a mixture of at least one monomer, a free radical polymerization initiator, and a stable free radical agent until from about 10 to about 50 weight percent of the monomer has been polymerized; optionally adding additional free radical initiator; optionally adding a colorant; dispersing with a high shear mixer the aforementioned partially polymerized mixture in water containing a stabilizing component selected from the group consisting of non-ionic and ionic water soluble polymeric stabilizers to obtain a suspension of particles with an average diameter of from about 0.1 to about 10 microns; polymerizing the resulting suspension to form said polymer.
摘要翻译：公开了一种制备聚合物的方法，其包括进行至少一种单体，自由基聚合引发剂和稳定自由基试剂的混合物的本体聚合，直到约10至约50重量％的单体已经聚合的任选地加入另外的自由基引发剂; 任选地加入着色剂; 用高剪切混合器将上述部分聚合的混合物在含有选自非离子和离子水溶性聚合物稳定剂的稳定组分的水中分散，以获得平均直径为约0.1至约10微米的颗粒悬浮液 ; 聚合所得悬浮液以形成所述聚合物。

2. 发明授权

US07910275B2 Toner having crystalline wax 有权
标题翻译：具有结晶蜡的调色剂
公开(公告)号：US07910275B2
公开(公告)日：2011-03-22
申请号：US11274459
申请日：2005-11-14
申请人： Raj D. Patel , David J. Sanders , Christine Anderson , Allan K. Chen , Daryl W. Vanbesien , Patricia A. Burns
发明人： Raj D. Patel , David J. Sanders , Christine Anderson , Allan K. Chen , Daryl W. Vanbesien , Patricia A. Burns
IPC分类号： G03G9/087
CPC分类号： G03G9/08708 , G03G9/0806 , G03G9/0821 , G03G9/08711 , G03G9/08726 , G03G9/08782 , G03G9/08795 , G03G9/08797
摘要： Embodiments include a chemical toner composition having a first resin including a styrene vinyl copolymer and having a Tg of from about 46 to about 56° C., b) a second resin including a styrene vinyl copolymer having a Tg of from about 55 to about 65° C., c) a distilled wax having a heat of crystallization and a heat of enthalpy, both from about 1.0 to about 4.0 J/g for every weight percent of the wax used in the chemical toner composition, and wherein the wax has a peak melting point of from about 70 to about 99° C., and d) a colorant, wherein the chemical toner has a gloss of from about 30 to about 80 GGU.
摘要翻译：实施方案包括化学调色剂组合物，其具有包含苯乙烯乙烯基共聚物的第一树脂，Tg为约46至约56℃，b）包含Tg为约55至约65的苯乙烯乙烯基共聚物的第二树脂 ℃，c）具有结晶热和焓热的蒸馏蜡，对于化学调色剂组合物中使用的每重量百分比的蜡，其摩尔数为约1.0至约4.0J / g，并且其中蜡具有峰值熔点为约70至约99℃，和d）着色剂，其中化学调色剂的光泽度为约30至约80GGU。

3. 发明授权

US07781138B2 Low melt toners and processes thereof 有权
标题翻译：低熔点调色剂及其工艺
公开(公告)号：US07781138B2
公开(公告)日：2010-08-24
申请号：US12574019
申请日：2009-10-06
申请人： Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allen K. Chen , Edward G. Zwartz , T. Hwee Ng
发明人： Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allen K. Chen , Edward G. Zwartz , T. Hwee Ng
IPC分类号： G03G5/00
CPC分类号： G03G9/0819 , G03G9/0804 , G03G9/0821 , G03G9/08755 , G03G9/08791 , G03G9/08793 , G03G9/08795 , G03G9/08797
摘要： A process for preparing toner particles and compositions adapted for use in preparing toners that comprise a blend of a first polyester resin with a second sharp melting polyester resin. The process includes forming an emulsion resin comprising a branched polyester resin, a crystalline polyester resin, a colorant, and optionally a wax. The resin mixture is aggregated using an aggregating agent, such as a zinc acetate solution, to form an aggregate mixture. The aggregate mixture is then coalesced at a temperature of from about 5 to about 20° C. above the Tg of the emulsion resin to produce the resultant toner particles.
摘要翻译：一种用于制备调色剂颗粒和组合物的方法，所述调色剂颗粒和组合物适用于制备调色剂，所述调色剂包括第一聚酯树脂与第二尖锐熔融聚酯树脂的共混物。该方法包括形成包含支链聚酯树脂，结晶聚酯树脂，着色剂和任选的蜡的乳液树脂。树脂混合物使用聚集剂如乙酸锌溶液聚集以形成骨料混合物。然后将聚集体混合物在高于乳液树脂的Tg约5至约20℃的温度下聚结，以产生所得到的调色剂颗粒。

4. 发明申请

US20090061349A1 LOW MELT TONERS AND PROCESSES THEREOF 失效
标题翻译：低熔体粉末及其工艺
公开(公告)号：US20090061349A1
公开(公告)日：2009-03-05
申请号：US12140738
申请日：2008-06-17
申请人： Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allan K. Chen , Edward G. Zwartz , T. Hwee Ng
发明人： Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allan K. Chen , Edward G. Zwartz , T. Hwee Ng
IPC分类号： G03G9/08
CPC分类号： G03G9/0819 , G03G9/0804 , G03G9/0821 , G03G9/08755 , G03G9/08791 , G03G9/08793 , G03G9/08795 , G03G9/08797
摘要： A process for preparing toner particles and compositions adapted for use in preparing toners that comprise a blend of a first polyester resin with a second sharp melting polyester resin. The process includes forming an emulsion resin comprising a branched polyester resin, a crystalline polyester resin, a colorant, and optionally a wax. The resin mixture is aggregated using an aggregating agent, such as a zinc acetate solution, to form an aggregate mixture. The aggregate mixture is then coalesced at a temperature of from about 5 to about 20° C. above the Tg of the emulsion resin to produce the resultant toner particles.
摘要翻译：一种用于制备调色剂颗粒和组合物的方法，所述调色剂颗粒和组合物适用于制备调色剂，所述调色剂包括第一聚酯树脂与第二尖锐熔融聚酯树脂的共混物。该方法包括形成包含支链聚酯树脂，结晶聚酯树脂，着色剂和任选的蜡的乳液树脂。树脂混合物使用聚集剂如乙酸锌溶液聚集以形成骨料混合物。然后将聚集体混合物在高于乳液树脂的Tg约5至约20℃的温度下聚结，以产生所得到的调色剂颗粒。

5. 发明授权

US07429443B2 Method of making emulsion aggregation toner 有权
标题翻译：制备乳液聚集调色剂的方法
公开(公告)号：US07429443B2
公开(公告)日：2008-09-30
申请号：US12015475
申请日：2008-01-16
申请人： Raj D. Patel
发明人： Raj D. Patel
IPC分类号： G03G9/08 , C08J3/215
CPC分类号： G03G9/08755 , G03G9/0804 , G03G9/08782
摘要： A polyester toner includes particles of a resin, a colorant, an optional wax, and a polyion coagulant, where the toner is prepared by an emulsion aggregation process.
摘要翻译：聚酯调色剂包括树脂颗粒，着色剂，任选的蜡和聚离子凝结剂，其中调色剂通过乳液聚集方法制备。

6. 发明授权

US07358022B2 Control of particle growth with complexing agents 失效
标题翻译：用络合剂控制颗粒生长
公开(公告)号：US07358022B2
公开(公告)日：2008-04-15
申请号：US11094428
申请日：2005-03-31
申请人： Valerie M. Farrugia , Allan K. Chen , Kimberly Nosella , Raj D. Patel , Tie Hwee Ng
发明人： Valerie M. Farrugia , Allan K. Chen , Kimberly Nosella , Raj D. Patel , Tie Hwee Ng
IPC分类号： G03G5/00
CPC分类号： G03G9/0819 , G03G9/0804 , G03G9/08755 , G03G9/08791 , G03G9/08795 , G03G9/08797
摘要： A method of making particles suitable for use as toners includes forming a mixture of sulfonated polyester resin, a colorant dispersion and optionally a wax dispersion, homogenizing the mixture, adding a coagulant to the mixture to aggregate the mixture to form aggregated particles, and coalescing the aggregated particles to form coalesced particles. In the method, when a predetermined average particle size is achieved during the aggregation and/or coalescing step, a complexing agent that complexes with ions of the coagulant is added in an amount effective to substantially halt any further particle growth. The complexing agent is believed to halt further growth by complexing with free coagulant ions still in the solution.
摘要翻译：制备适合用作调色剂的颗粒的方法包括形成磺化聚酯树脂，着色剂分散体和任选的蜡分散体的混合物，使混合物均化，向混合物中加入凝结剂以将混合物聚集形成凝集颗粒，并将聚集的颗粒形成聚结的颗粒。在该方法中，当在聚集和/或聚结步骤期间达到预定平均粒径时，加入与絮凝剂的离子相配合的络合剂，其量可以有效地基本上停止任何其它颗粒生长。据信络合剂通过与仍在溶液中的游离凝结剂离子络合来停止进一步的生长。

7. 发明授权

US07358021B2 Hybrid toner processes 有权
公开(公告)号：US07358021B2
公开(公告)日：2008-04-15
申请号：US11044847
申请日：2005-01-27
申请人： Raj D. Patel , Guerino G. Sacripante , Edward G. Zwartz , Enno E. Agur , Allan K. Chen , T Hwee Ng , Kimberly D. Nosella , Cuong Vong , Karen A. Moffat
发明人： Raj D. Patel , Guerino G. Sacripante , Edward G. Zwartz , Enno E. Agur , Allan K. Chen , T Hwee Ng , Kimberly D. Nosella , Cuong Vong , Karen A. Moffat
IPC分类号： G03G5/00
CPC分类号： G03G9/0806 , G03G9/0804 , G03G9/08711 , G03G9/08726 , G03G9/08755 , G03G9/08782 , G03G9/08793 , G03G9/08795 , G03G9/08797
摘要： A toner process that includes a first heating of a colorant dispersion, a first polyester resin free latex emulsion, a second polyester latex emulsion, and a wax dispersion in the presence of a coagulant containing a metal ion; adding a third polyester free latex; adding an organic sequestering compound or a silicate salt sequestering compound, followed by a second heating.

8. 发明授权

US07282314B2 Toner processes 有权
标题翻译：墨粉处理
公开(公告)号：US07282314B2
公开(公告)日：2007-10-16
申请号：US11046109
申请日：2005-01-28
申请人： Raj D. Patel , Allan K. Chen , Cuong Vong
发明人： Raj D. Patel , Allan K. Chen , Cuong Vong
IPC分类号： G03G9/08
CPC分类号： G03G9/0804 , G03G9/0833 , G03G9/0835 , G03G9/0836 , G03G9/0837 , G03G9/08708 , G03G9/08711 , G03G9/08728 , G03G9/08731 , G03G9/08737 , G03G9/08782 , G03G9/08793 , G03G9/08795 , G03G9/08797 , G03G9/09783
摘要： A toner process involving the heating a mixture of an acicular magnetite dispersion, a colorant dispersion, a wax dispersion, a first latex containing a crosslinked resin, and a second latex containing a resin free of crosslinking in the presence of a coagulant to provide aggregates, stabilizing the aggregates with an organic complexing compound salt dissolved in a base, and further heating the aggregates to provide coalesced toner particles.
摘要翻译：一种调色剂方法，包括加热针状磁铁矿分散体，着色剂分散体，蜡分散体，含有交联树脂的第一胶乳和含有在凝结剂存在下无交联的树脂的第二胶乳的混合物，以提供聚集体，用溶解在基体中的有机络合化合物盐稳定聚集体，并进一步加热聚集体以提供聚结的调色剂颗粒。

9. 发明授权

US06673500B1 Document security processes 失效
标题翻译：文档安全流程
公开(公告)号：US06673500B1
公开(公告)日：2004-01-06
申请号：US10225214
申请日：2002-08-20
申请人： Raj D. Patel , Fatima M. Mayer , Michael A. Hopper , Kurt I. Halfyard
发明人： Raj D. Patel , Fatima M. Mayer , Michael A. Hopper , Kurt I. Halfyard
IPC分类号： G03G908
CPC分类号： G03G9/0926 , B41M3/14 , B41M3/144 , G03G9/0821 , G03G9/08795 , G03G9/08797 , G03G9/0902 , G03G9/0908 , G03G9/0916 , G03G9/0924 , G03G9/09708
摘要： A process comprising applying a toner security mark on a document generated by xerographic means, and which mark possesses white glossy characteristics, and wherein said toner is comprised of a waterborne polymer resin and a colorant, and optionally a second security mark generated by a toner comprised of a waterborne polymer resin and a UV fluorescent component.
摘要翻译：一种方法，包括在由静电印刷装置产生的文件上施加调色剂安全标记，以及哪个标记具有白色光泽特性，并且其中所述调色剂由水性聚合物树脂和着色剂组成，并且可选地由包含的调色剂产生的第二安全标记的水性聚合物树脂和UV荧光成分。

10. 发明授权

US06652959B2 Marking particles 有权
公开(公告)号：US06652959B2
公开(公告)日：2003-11-25
申请号：US10042341
申请日：2002-01-11
申请人： Daniel A. Foucher , Raj D. Patel , Naveen Chopra , Peter M. Kazmaier
发明人： Daniel A. Foucher , Raj D. Patel , Naveen Chopra , Peter M. Kazmaier
IPC分类号： B32B516
CPC分类号： G03G9/0914 , G03G9/0906 , G03G9/0916 , G03G9/0922 , Y10T428/25 , Y10T428/254 , Y10T428/2982 , Y10T428/2989
摘要： Disclosed are marking particles comprising a resin, a chelating agent, and a spiropyran material which is of the formula The marking particles are prepared by an emulsion aggregation process.

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