会员体验
专利管家(专利管理)
工作空间(专利管理)
风险监控(情报监控)
数据分析(专利分析)
侵权分析(诉讼无效)
联系我们
交流群
官方交流:
QQ群: 891211   
微信请扫码    >>>
现在联系顾问~
热词
    • 10. 发明授权
    • Electroluminescent phosphor powder with D50 value of less than 12 μm and method of making
    • D50值小于12μm的电致发光荧光粉及其制造方法
    • US07291291B2
    • 2007-11-06
    • US10907360
    • 2005-03-30
    • Judy A. Belinski-WolfeThomas A. WolfeBrian J. Payne
    • Judy A. Belinski-WolfeThomas A. WolfeBrian J. Payne
    • C09K11/56C09K11/54
    • C09K11/584
    • There is presented an electroluminescent phosphor powder of copper-activated zinc sulfide particles that has a size distribution with a D50 value of less than 12 μm, and more preferably less than 10 μm. The powder is preferably made by a method that includes the steps of combining copper-doped zinc sulfide with sulfur, zinc oxide and a chloride-containing flux to form a first mixture; preliminarily firing the first mixture and milling the preliminarily fired first mixture to form a milled material having a D50 value of less than or equal to about 5 μm; blending the milled material with sulfur, zinc oxide and a chloride-containing flux to form a second mixture; firing the mixture in a first firing step at a temperature in a range of about 1020° C. to about 1080° C. to form a hexagonal zinc sulfide material; inducing defects into the hexagonal zinc sulfide material; firing the hexagonal zinc sulfide material in a second firing step at a temperature in a range of about 650° C. to about 850° C. to form an electroluminescent phosphor; and sifting the electroluminescent phosphor to provide an electroluminescent phosphor powder comprising phosphor particles that have a size distribution with a D50 value of less than 12 μm. The step of inducing defects may be accomplished by milling, mulling or sonification of the mixture.
    • 提出了具有D50值小于12μm,更优选小于10μm的尺寸分布的铜活化硫化锌颗粒的电致发光荧光体粉末。 该粉末优选通过包括以下步骤的方法制备:掺杂铜的硫化锌与硫,氧化锌和含氯化物的助熔剂以形成第一混合物; 预先烧制第一混合物并研磨预先烧制的第一混合物以形成D50值小于或等于约5μm的研磨材料; 将研磨的材料与硫,氧化锌和含氯化物的助熔剂混合以形成第二混合物; 在约1020℃至约1080℃的温度下,在第一烧制步骤中焙烧该混合物以形成六方硫化锌材料; 引起六方硫化锌材料的缺陷; 在第二烧成工序中,在约650℃〜约850℃的温度范围内烧成六方晶硫化锌材料,形成电致发光荧光体; 以及筛选所述电致发光荧光体以提供包含荧光体颗粒的电致发光荧光体粉末,所述荧光体颗粒具有D50值小于12μm的尺寸分布。 诱导缺陷的步骤可以通过研磨,研磨或超声波处理来实现。