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    • 4. 发明申请
    • Method for Producing Linear Pentenenitrile
    • 生产线性戊烯腈的方法
    • US20080281120A1
    • 2008-11-13
    • US10586470
    • 2005-01-27
    • Tim JungkampRobert BaumannMichael BartschGerd HaderleinHermann LuykenJens ScheidelTobias AechtnerPeter PfabPetra DeckertWolfgang SiegelPeter Bassler
    • Tim JungkampRobert BaumannMichael BartschGerd HaderleinHermann LuykenJens ScheidelTobias AechtnerPeter PfabPetra DeckertWolfgang SiegelPeter Bassler
    • C07C255/00
    • C07C253/30C07C253/10Y02P20/582C07C255/07
    • A process is described for preparing 3-pentenenitrile, characterized by the following process steps: (a) isomerizing a reactant stream which comprises 2-methyl-3-butenenitrile over at least one dissolved or dispersed isomerization catalyst to give a stream 1 which comprises the at least one isomerization catalyst, 2-methyl-3-butenenitrile, 3-pentenenitrile and (Z)-2-methyl-2-butenenitrile, (b) distilling stream 1 to obtain a stream 2 as the top product which comprises 2-methyl-3-butenenitrile, 3-pentenenitrile and (Z)-2-methyl-2-butenenitrile, and a stream 3 as the bottom product which comprises the at least one isomerization catalyst, (c) distilling stream 2 to obtain a stream 4 as the top product which, compared to stream 2, is enriched in (Z)-2-methyl-2-butenenitrile, based on the sum of all pentenenitriles in stream 2, and a stream 5 as the bottom product which, compared to stream 2, is enriched in 3-pentenenitrile and 2-methyl-3-butenenitrile, based on the sum of all pentenenitriles in stream 2, (d) distilling stream 5 to obtain a stream 6 as the bottom product which comprises 3-pentenenitrile and a stream 7 as the top product which comprises 2-methyl-3-butenenitrile.
    • 描述了制备3-戊烯腈的方法,其特征在于以下方法步骤:(a)在至少一种溶解或分散的异构化催化剂上异构化包含2-甲基-3-丁烯腈的反应物流,得到流1,其包含 至少一种异构化催化剂,2-甲基-3-丁烯腈,3-戊烯腈和(Z)-2-甲基-2-丁烯腈,(b)蒸馏物流1,得到作为顶部产物的物流2,其包含2-甲基 -3-丁烯腈,3-戊烯腈和(Z)-2-甲基-2-丁烯腈,以及作为底部产物的料流3,其包含至少一种异构化催化剂,(c)蒸馏物流2以获得物流4, 与流2相比,基于流2中的所有五烯丙烯的总和和作为底部产物的流5,与流2相比富含(Z)-2-甲基-2-丁烯腈的顶部产物与流2相比较 ,富含3-戊烯腈和2-甲基-3-丁烯腈,基于所有pentenenit (d)蒸馏流5以获得作为底部产物的料流6,其包含3-戊烯腈和作为顶部产物的料流7,其包含2-甲基-3-丁烯腈。