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1. 发明申请

US20110224469A1 Alkylated Aromatics Production 有权
标题翻译：烷基化芳烃生产
公开(公告)号：US20110224469A1
公开(公告)日：2011-09-15
申请号：US12721326
申请日：2010-03-10
申请人： Matthew J. Vincent , Vijay Nanda , Maruti Bhandarkar , Brian Maerz , Terry E. Helton
发明人： Matthew J. Vincent , Vijay Nanda , Maruti Bhandarkar , Brian Maerz , Terry E. Helton
IPC分类号： C07C2/66
CPC分类号： C07C2/66 , C07C6/126 , C07C7/13 , C07C2529/08 , C07C2529/18 , C07C2529/70 , C07C15/04 , C07C15/073 , C07C15/085 , C07C15/02
摘要： Disclosed is a process for the production of alkylated aromatics by contacting a feed stream comprising an alkylatable aromatic, an alkylating agent and trace amounts of water and impurities in the presence of first and second alkylation catalysts wherein the water and impurities are removed in order to improve the cycle length of such alkylation catalysts. Water and a portion of impurities are removed in a dehydration zone. A first alkylation zone having a first alkylation catalyst which, in some embodiments is a large pore molecular sieve, acts to remove a larger portion of impurities, such as nitrogenous and other species, and to alkylate a smaller portion of the alkylatable aromatic compound. A second alkylation zone, which in some embodiments is a medium pore molecular sieve, acts to remove a smaller portion of impurities, and to alkylate a larger portion of the alkylatable aromatic compound.
摘要翻译：公开了通过在第一和第二烷基化催化剂存在下使包含可烷基化芳族化合物，烷基化剂和痕量水和杂质的进料流接触来生产烷基化芳族化合物的方法，其中除去水和杂质以改善这种烷基化催化剂的循环长度。在脱水区中除去水和一部分杂质。具有第一烷基化催化剂的第一烷基化区，在一些实施方案中为大孔分子筛，起到除去较大部分杂质如氮和其它物质的作用，并将较小部分的可烷基化芳族化合物烷基化。在一些实施方案中，第二烷基化区是中孔分子筛，起到除去较少部分杂质的作用，并使大部分可烷基化芳族化合物烷基化。

2. 发明授权

US08629311B2 Alkylated aromatics production 有权
标题翻译：烷基化芳烃生产
公开(公告)号：US08629311B2
公开(公告)日：2014-01-14
申请号：US12721326
申请日：2010-03-10
申请人： Matthew J. Vincent , Vijay Nanda , Maruti Bhandarkar , Brian Maerz , Terry E. Helton
发明人： Matthew J. Vincent , Vijay Nanda , Maruti Bhandarkar , Brian Maerz , Terry E. Helton
IPC分类号： C07C2/66 , C07C6/12
CPC分类号： C07C2/66 , C07C6/126 , C07C7/13 , C07C2529/08 , C07C2529/18 , C07C2529/70 , C07C15/04 , C07C15/073 , C07C15/085 , C07C15/02
摘要： Disclosed is a process for the production of alkylated aromatics by contacting a feed stream comprising an alkylatable aromatic, an alkylating agent and trace amounts of water and impurities in the presence of first and second alkylation catalysts wherein the water and impurities are removed in order to improve the cycle length of such alkylation catalysts. Water and a portion of impurities are removed in a dehydration zone. A first alkylation zone having a first alkylation catalyst which, in some embodiments is a large pore molecular sieve, acts to remove a larger portion of impurities, such as nitrogenous and other species, and to alkylate a smaller portion of the alkylatable aromatic compound. A second alkylation zone, which in some embodiments is a medium pore molecular sieve, acts to remove a smaller portion of impurities, and to alkylate a larger portion of the alkylatable aromatic compound.
摘要翻译：公开了通过在第一和第二烷基化催化剂存在下使包含可烷基化芳族化合物，烷基化剂和痕量水和杂质的进料流接触来生产烷基化芳族化合物的方法，其中除去水和杂质以改善这种烷基化催化剂的循环长度。在脱水区中除去水和一部分杂质。具有第一烷基化催化剂的第一烷基化区，在一些实施方案中为大孔分子筛，起到除去较大部分杂质如氮和其它物质的作用，并将较小部分的可烷基化芳族化合物烷基化。在一些实施方案中，第二烷基化区是中孔分子筛，起到除去较少部分杂质的作用，并使大部分可烷基化芳族化合物烷基化。

3. 发明授权

US07777087B2 Liquid phase alkylation with multiple catalysts 有权
标题翻译：用多种催化剂进行液相烷基化
公开(公告)号：US07777087B2
公开(公告)日：2010-08-17
申请号：US12624118
申请日：2009-11-23
申请人： Michael C. Clark , Vijay Nanda , Chung-Ming Chi , Maruti Bhandarkar , Brian Maerz , Matthew J. Vincent
发明人： Michael C. Clark , Vijay Nanda , Chung-Ming Chi , Maruti Bhandarkar , Brian Maerz , Matthew J. Vincent
IPC分类号： C07C2/66
CPC分类号： C10G29/205 , C07C2/66 , C07C6/126 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/70 , C10G2300/1092 , C10G2300/1096 , C10G2400/30 , Y02P20/52 , C07C15/073 , C07C15/02 , C07C15/085
摘要： A process is disclosed for producing an alkylaromatic compound in a multistage reaction system comprising at least first and second series-connected alkylation reaction zones, each containing an alkylation catalyst. A first feed comprising an alkylatable aromatic compound and a second feed comprising an alkene are introduced into the first alkylation reaction zone. The first and second alkylation reaction zones are operated under conditions of temperature and pressure effective to cause alkylation of the aromatic compound with the alkene in the presence of the alkylation catalyst, the temperature and pressure being such that the aromatic compound is at least partly in the liquid phase. The alkylation catalyst in the first alkylation reaction zone, which may be a reactor guard bed, has more acid sites per unit volume of catalyst than the alkylation catalyst in the second reaction zone.
摘要翻译：公开了一种在多级反应体系中生产烷基芳族化合物的方法，其包含至少第一和第二串联连接的烷基化反应区，每个含有烷基化催化剂。将包含可烷基化芳族化合物和包含烯烃的第二进料的第一进料引入第一烷基化反应区。第一烷基化反应区和第二烷基化反应区在温度和压力有效的条件下运行，以在烷基化催化剂存在下使芳族化合物与烯烃进行烷基化，温度和压力使芳族化合物至少部分在液相。在第一烷基化反应区（其可以是反应器保护床）中的烷基化催化剂与第二反应区中的烷基化催化剂相比，每单位体积催化剂具有更多的酸性位点。

4. 发明授权

US07645913B2 Liquid phase alkylation with multiple catalysts 有权
公开(公告)号：US07645913B2
公开(公告)日：2010-01-12
申请号：US11655452
申请日：2007-01-19
申请人： Michael C. Clark , Vijay Nanda , Chung-Ming Chi , Maruti Bhandarkar , Brian Maerz , Matthew J. Vincent
发明人： Michael C. Clark , Vijay Nanda , Chung-Ming Chi , Maruti Bhandarkar , Brian Maerz , Matthew J. Vincent
IPC分类号： C07C2/66
CPC分类号： C10G29/205 , C07C2/66 , C07C6/126 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/70 , C10G2300/1092 , C10G2300/1096 , C10G2400/30 , Y02P20/52 , C07C15/073 , C07C15/02 , C07C15/085
摘要： A process is disclosed for producing an alkylaromatic compound in a multistage reaction system comprising at least first and second series-connected alkylation reaction zones, each containing an alkylation catalyst. A first feed comprising an alkylatable aromatic compound and a second feed comprising an alkene are introduced into the first alkylation reaction zone. The first and second alkylation reaction zones are operated under conditions of temperature and pressure effective to cause alkylation of the aromatic compound with the alkene in the presence of the alkylation catalyst, the temperature and pressure being such that the aromatic compound is at least partly in the liquid phase. The alkylation catalyst in the first alkylation reaction zone, which may be a reactor guard bed, has more acid sites per unit volume of catalyst than the alkylation catalyst in the second reaction zone.

5. 发明申请

US20080177120A1 Liquid phase alkylation with multiple catalysts 有权
标题翻译：用多种催化剂进行液相烷基化
公开(公告)号：US20080177120A1
公开(公告)日：2008-07-24
申请号：US11655452
申请日：2007-01-19
申请人： Michael C. Clark , Vijay Nanda , Chi Chung-Ming , Maruti Bhandarkar , Brian Maerz , Matthew J. Vincent
发明人： Michael C. Clark , Vijay Nanda , Chi Chung-Ming , Maruti Bhandarkar , Brian Maerz , Matthew J. Vincent
IPC分类号： C07C2/66
CPC分类号： C10G29/205 , C07C2/66 , C07C6/126 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/70 , C10G2300/1092 , C10G2300/1096 , C10G2400/30 , Y02P20/52 , C07C15/073 , C07C15/02 , C07C15/085
摘要： A process is disclosed for producing an alkylaromatic compound in a multistage reaction system comprising at least first and second series-connected alkylation reaction zones, each containing an alkylation catalyst. A first feed comprising an alkylatable aromatic compound and a second feed comprising an alkene are introduced into the first alkylation reaction zone. The first and second alkylation reaction zones are operated under conditions of temperature and pressure effective to cause alkylation of the aromatic compound with the alkene in the presence of the alkylation catalyst, the temperature and pressure being such that the aromatic compound is at least partly in the liquid phase. The alkylation catalyst in the first alkylation reaction zone, which may be a reactor guard bed, has more acid sites per unit volume of catalyst than the alkylation catalyst in the second reaction zone.
摘要翻译：公开了一种在多级反应体系中生产烷基芳族化合物的方法，其包含至少第一和第二串联连接的烷基化反应区，每个含有烷基化催化剂。将包含可烷基化芳族化合物和包含烯烃的第二进料的第一进料引入第一烷基化反应区。第一烷基化反应区和第二烷基化反应区在温度和压力有效的条件下运行，以在烷基化催化剂存在下使芳族化合物与烯烃进行烷基化，温度和压力使芳族化合物至少部分在液相。在第一烷基化反应区（其可以是反应器保护床）中的烷基化催化剂与第二反应区中的烷基化催化剂相比，每单位体积催化剂具有更多的酸性位点。

6. 发明申请

US20130137910A1 Alkylation Process 有权
标题翻译：烷基化方法
公开(公告)号：US20130137910A1
公开(公告)日：2013-05-30
申请号：US13746965
申请日：2013-01-22
申请人： Matthew J. Vincent , Vijay Nanda , Brian Maerz , Maruti Bhandarkar
发明人： Matthew J. Vincent , Vijay Nanda , Brian Maerz , Maruti Bhandarkar
IPC分类号： C07C2/66
CPC分类号： C07C2/66 , C07C2529/08 , C07C2529/70 , C10G29/205 , C10G2300/1044 , C10G2300/1092 , C10G2300/1096 , C10G2300/4006 , C10G2300/4012 , C10G2300/4018 , C10G2400/30 , Y02P20/52 , C07C15/073 , C07C15/085
摘要： The present invention provides an improved process for the catalytic conversion of a feedstock comprising an alkylatable aromatic compound and an alkylating agent to form a conversion product comprising the desired alkylaromatic compound by contacting said feedstock in at least partial liquid phase under catalytic conversion conditions with a catalyst composition comprising a porous crystalline material having a structure type of FAU, BEA* or MWW, or a mixture thereof, wherein the porous crystalline material has a Relative Activity measured at 220° C. as an RA220 of at least 7.5 or measured at 180° C. as RA180 of at least 2.5, allowing operation at lower reaction pressures, e.g., a reaction pressure of about 450 psig (3102 kPa) or less, and lower alkylating agent feed supply pressure of 450 psig (3102 kPa) or less.
摘要翻译：本发明提供了一种用于催化转化包含可烷基化芳族化合物和烷基化剂的原料的改进方法，以通过使催化转化条件下的至少部分液相与催化剂接触来形成包含所需烷基芳族化合物的转化产物组合物，其包含结构类型为FAU，BEA *或MWW的多孔结晶材料或其混合物，其中所述多孔结晶材料具有在220℃下测量的相对活性，RA220为至少7.5或在180° C.作为至少2.5的RA180，允许在较低反应压力下进行操作，例如约450psig（3102kPa）或更低的反应压力和450psig（3102kPa）或更低的烷基化剂进料供应压力。

7. 发明授权

US09249067B2 Alkylation process 有权
公开(公告)号：US09249067B2
公开(公告)日：2016-02-02
申请号：US13642676
申请日：2011-04-15
申请人： Matthew J. Vincent , Vijay Nanda , Terry E. Helton
发明人： Matthew J. Vincent , Vijay Nanda , Terry E. Helton
IPC分类号： C07C2/66 , C07C7/12
CPC分类号： C07C2/66 , C07C7/12 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/70 , Y02P20/52 , C07C15/02 , C07C15/073 , C07C15/085 , C07C15/04
摘要： The present invention provides an improved process for producing an alkylated aromatic compound from an at least partially untreated alkylatable aromatic compound having catalyst poisons and an alkylating agent, wherein said alkylatable aromatic compound stream is treated to reduce catalyst poisons with a treatment composition having a surface area/surface volume ratio of greater than or equal to 30 in−1 (12 cm−1) in a treatment zone separate from an alkylation reaction zone under treatment conditions including a temperature of from about 30° C. to about 300° C. to form an effluent comprising said treated alkylatable aromatic compound.

8. 发明申请

US20130211164A1 Alkylation Process 有权
标题翻译：烷基化方法
公开(公告)号：US20130211164A1
公开(公告)日：2013-08-15
申请号：US13642676
申请日：2011-04-15
申请人： Matthew J. Vincent , Vijay Nanda , Terry E. Helton
发明人： Matthew J. Vincent , Vijay Nanda , Terry E. Helton
IPC分类号： C07C2/66
CPC分类号： C07C2/66 , C07C7/12 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/70 , Y02P20/52 , C07C15/02 , C07C15/073 , C07C15/085 , C07C15/04
摘要： The present invention provides an improved process for producing an alkylated aromatic compound from an at least partially untreated alkylatable aromatic compound having catalyst poisons and an alkylating agent, wherein said alkylatable aromatic compound stream is treated to reduce catalyst poisons with a treatment composition having a surface area/surface volume ratio of greater than or equal to 30 in−1 (12 cm−1) in a treatment zone separate from an alkylation reaction zone under treatment conditions including a temperature of from about 30° C. to about 300° C. to form an effluent comprising said treated alkylatable aromatic compound.
摘要翻译：本发明提供了一种由至少部分未经处理的具有催化剂毒素和烷基化剂的可烷化芳族化合物制备烷基化芳族化合物的改进方法，其中用具有表面积的处理组合物处理所述可烷基化芳族化合物流以减少催化剂毒物 /表面体积比大于或等于30in-1（12cm-1）在处理区域与烷基化反应区分离，处理条件包括温度为约30℃至约300℃至形成包含所述经处理的可烷基化芳族化合物的流出物。

9. 发明申请

US20130197287A1 ALKYLATION PROCESS 有权
标题翻译：烷基化方法
公开(公告)号：US20130197287A1
公开(公告)日：2013-08-01
申请号：US13642690
申请日：2011-04-15
申请人： Matthew J. Vincent , Vijay Nanda , Terry E. Helton
发明人： Matthew J. Vincent , Vijay Nanda , Terry E. Helton
IPC分类号： C07C2/66 , C07C7/12
CPC分类号： C07C2/66 , C07C7/12 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/70 , Y02P20/52 , C07C15/02 , C07C15/073 , C07C15/085 , C07C15/04
摘要： The present invention provides an improved process for producing an alkylated aromatic compound from an at least partially untreated alkylatable aromatic compound having catalyst poisons, wherein said alkylatable aromatic compound stream is treated to reduce catalyst poisons with a treatment composition having a surface area/surface volume ratio of greater than or equal to 30 in−1 (12 cm−1) in a treatment zone separate from an alkylation reaction zone under treatment conditions including a temperature of from about 30° C. to about 300° C. to form an effluent comprising said treated alkylatable aromatic compound.
摘要翻译：本发明提供了一种由至少部分未处理的具有催化剂毒物的可烷化芳族化合物制备烷基化芳族化合物的改进方法，其中用具有表面积/表面体积比的处理组合物处理所述可烷基化芳族化合物流以还原催化剂毒物在包括温度为约30℃至约300℃的处理条件下与烷基化反应区分离的处理区中大于或等于30in -1（12cm -1），以形成流出物，其包含所述经处理的可烷基化芳族化合物。

10. 发明授权

US08993820B2 Alkylation process 有权
标题翻译：烷基化方法
公开(公告)号：US08993820B2
公开(公告)日：2015-03-31
申请号：US13642690
申请日：2011-04-15
申请人： Matthew J. Vincent , Vijay Nanda , Terry E. Helton
发明人： Matthew J. Vincent , Vijay Nanda , Terry E. Helton
IPC分类号： C07C2/66 , C07C7/12
CPC分类号： C07C2/66 , C07C7/12 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/70 , Y02P20/52 , C07C15/02 , C07C15/073 , C07C15/085 , C07C15/04
摘要： The present invention provides an improved process for producing an alkylated aromatic compound from an at least partially untreated alkylatable aromatic compound having catalyst poisons, wherein said alkylatable aromatic compound stream is treated to reduce catalyst poisons with a treatment composition having a surface area/surface volume ratio of greater than or equal to 30 in−1 (12 cm−1) in a treatment zone separate from an alkylation reaction zone under treatment conditions including a temperature of from about 30° C. to about 300° C. to form an effluent comprising said treated alkylatable aromatic compound.
摘要翻译：本发明提供了一种由至少部分未处理的具有催化剂毒物的可烷化芳族化合物制备烷基化芳族化合物的改进方法，其中用具有表面积/表面体积比的处理组合物处理所述可烷基化芳族化合物流以还原催化剂毒物在包括温度为约30℃至约300℃的处理条件下与烷基化反应区分离的处理区中大于或等于30in -1（12cm -1），以形成流出物，其包含所述经处理的可烷基化芳族化合物。

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