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1. 发明授权

US5292848A Fluorosilicone composition and its gellike cured product 失效
标题翻译：氟硅酮组合物及其胶凝固化产物
公开(公告)号：US5292848A
公开(公告)日：1994-03-08
申请号：US964946
申请日：1992-10-22
申请人： Masayuki Ikeno , Miyuki Tanaka , Hiroyasu Hara , Hironao Fujiki , Shinichi Sato , Hiroshi Inomata
发明人： Masayuki Ikeno , Miyuki Tanaka , Hiroyasu Hara , Hironao Fujiki , Shinichi Sato , Hiroshi Inomata
IPC分类号： C08L83/05 , C08L83/07 , C08L83/08 , C08L83/12 , C08G77/06
CPC分类号： C08L83/08 , C08L83/12
摘要： The present fluorosilicone composition is an addition reaction curable composition that uses, as an alkenyl group-containing organopolysiloxane, a fluorine-containing organopolysiloxane represented by the following general formula (1): ##STR1## wherein R represents a vinyl group, R.sup.1 represents an alkyl group or a phenyl group, R.sup.2 represents a group represented by the following formula (2): ##STR2## in which p is an integer of 2 to 8 and q is an integer of 1 to 10, and n and m are each a positive integer. This composition can form a gellike cured product particularly excellent in acid resistance.
摘要翻译：本发明的氟硅酮组合物是使用由以下通式（1）表示的含氟有机聚硅氧烷作为含烯基的有机聚硅氧烷的加成反应固化性组合物：（*化学结构*）（1）其中R表示乙烯基基团，R 1表示烷基或苯基，R 2表示由下式（2）表示的基团：（*化学结构*）（2）其中p为2〜8的整数，q为 1〜10，n和m各自为正整数。该组合物可以形成特别优异的耐酸性的胶凝固化产物。

2. 发明授权

US5516838A Flame retardant silicone compositions 失效
标题翻译：阻燃硅酮组合物
公开(公告)号：US5516838A
公开(公告)日：1996-05-14
申请号：US516515
申请日：1995-08-17
申请人： Hironao Fujiki , Masayuki Ikeno , Hiroyasu Hara , Kazuyasu Satoh
发明人： Hironao Fujiki , Masayuki Ikeno , Hiroyasu Hara , Kazuyasu Satoh
IPC分类号： C08K5/18 , C08G77/34 , C08K5/00 , C08L83/04 , C08L83/05 , C08L83/07 , H01L23/29 , H01L23/31 , C08K5/49
CPC分类号： C08K5/0066 , C08G77/34 , C08L83/04 , C08G77/12 , C08G77/20
摘要： To a silicone composition comprising (A) an organopolysiloxane having at least two alkenyl groups in a molecule, (B) an organohydrogenpolysiloxane having at least two hydrogen atoms each directly attached to a silicon atom in a molecule, and (C) a platinum catalyst, (D) a compound having a phenyl group and a secondary or tertiary amino group directly attached thereto is added to render the composition flame retardant. The composition cures into a transparent product having improved flame retardancy meeting the UL standard and is suitable for use in the protection of electronic parts like ICs and hybrid ICs.
摘要翻译：对于包含（A）在分子中具有至少两个烯基的有机聚硅氧烷的聚硅氧烷组合物，（B）具有至少两个氢原子的有机氢聚硅氧烷，各自直接连接到分子中的硅原子上，和（C）铂催化剂，（D）加入具有苯基和与其直接连接的仲或叔氨基的化合物，使组合物阻燃。该组合物固化成具有符合UL标准的具有改进的阻燃性的透明产品，并且适用于保护电子部件如IC和混合IC。

3. 发明授权

US5438094A Adhesive silicone compositions 失效
标题翻译：粘合硅胶组合物
公开(公告)号：US5438094A
公开(公告)日：1995-08-01
申请号：US266336
申请日：1994-07-01
申请人： Hironao Fujiki , Hiroyasu Hara , Mikio Shiono , Masayuki Ikeno
发明人： Hironao Fujiki , Hiroyasu Hara , Mikio Shiono , Masayuki Ikeno
IPC分类号： C08L83/04 , C09J183/04 , C09J183/07 , C08K5/54
CPC分类号： C08L83/04 , C09J183/04 , C08G77/12 , C08G77/20 , C08G77/24 , C08G77/70
摘要： An adhesive silicone composition comprising (A) an alkenyl group-containing organopolysiloxane, (B) an organohydrogen-polysiloxane having at least three hydrogen atoms each directly bonded to a silicon atom in a molecule, (C) a compound having at least one aliphatic unsaturated group and at least two phenyl skeletons in a molecule, and (D) a platinum catalyst is well adhesive to both metals and reins, and even to difficult-to-adhere resins such as nylon, polycarbonate and acryl resins.
摘要翻译：一种粘合性硅氧烷组合物，其包含（A）含链烯基的有机聚硅氧烷，（B）具有至少三个氢原子的有机氢 - 聚硅氧烷，每个氢原子分别直接键合到硅原子上，（C）具有至少一个脂族不饱和基团的化合物基团和至少两个苯基骨架，以及（D）铂催化剂对金属和筘具有良好的粘合性，并且甚至难以粘附的树脂如尼龙，聚碳酸酯和丙烯酸树脂。

4. 发明授权

US5536803A Adhesive silicone compositions 失效
标题翻译：粘合硅胶组合物
公开(公告)号：US5536803A
公开(公告)日：1996-07-16
申请号：US461012
申请日：1995-06-05
申请人： Hironao Fujiki , Shigeki Shudo , Toshiaki Takahashi , Hiroyasu Hara , Takeshi Miyao
发明人： Hironao Fujiki , Shigeki Shudo , Toshiaki Takahashi , Hiroyasu Hara , Takeshi Miyao
IPC分类号： C08L83/07 , C09J183/04 , C09J183/07 , C08G77/08
CPC分类号： C09J183/04
摘要： An adhesive silicone composition comprising a diorganopolysiloxane, an organohydrogenpolysiloxane, and a platinum catalyst is blended with an organohydrogenpolysiloxane having at least two hydrogen atoms each bonded to a silicon atom in a molecule and containing an aromatic ring-bearing hydrocarbon radical in an amount of at least 12 mol % of the entire monovalent organic radicals bonded to silicon atoms, or a compound containing at least one hydrogen atom bonded to a silicon atom in a molecule and having a radical of two benzene rings separated by --R.sup.13 R.sup.14 Si--, --R.sup.13 R.sup.14 SiO--, --OR.sup.13 R.sup.14 SiO-- or --R.sup.13 R.sup.14 SiOR.sup.13 R.sup.14 Si-- wherein R.sup.13 and R.sup.14 are a monovalent hydrocarbon radical. The composition firmly adheres to organic resins, but is readily releasable from metal molds.
摘要翻译：将包含二有机聚硅氧烷，有机氢聚硅氧烷和铂催化剂的粘合性有机硅组合物与具有至少两个氢原子的有机氢聚硅氧烷共混，每个氢原子分子键合至硅原子并且含有至少含有芳环的烃基与硅原子键合的全部一价有机基团的12摩尔％，或分子中含有与硅原子键合的至少一个氢原子的化合物，其具有由-R 13 R 14 -Si，-R 13 R 14 SiO， - OR13R14SiO-或-R13R14SiOR13R14Si-，其中R13和R14是一价烃基。组合物牢固地粘附到有机树脂上，但是容易从金属模具中剥离。

5. 发明授权

US5332795A Silicone gel composition excellent in damping property 失效
标题翻译：硅胶组合物阻尼性能优异
公开(公告)号：US5332795A
公开(公告)日：1994-07-26
申请号：US944275
申请日：1992-09-14
申请人： Hironao Fujiki , Hiroyasu Hara
发明人： Hironao Fujiki , Hiroyasu Hara
IPC分类号： B01J13/00 , C08L83/04 , C08L83/05 , C08L83/07 , C08L83/08 , C08G77/08
CPC分类号： C08L83/04 , C08L83/08 , C08G77/12 , C08G77/20 , C08G77/24 , C08G77/70
摘要： A silicone gel composition, comprising as essential components(A) an organopolysiloxane comprising substantially 90 to 97 mol % of R(CH.sub.3)SiO units, 0.1 to 2.5 mol % of RSiO.sub.1.5 units, and 0.1 to 4.0 mol % of CH.sub.3 R(CH.sub.2 .dbd.CH)Si.sub.0.5 units, wherein R represents a group selected from the group consisting of a methyl group, a phenyl group, and a CF.sub.3 CH.sub.2 CH.sub.2 -- group, provided that the total of the phenyl groups and the CF.sub.3 CH.sub.2 CH.sub.2 -- groups out of the R groups amounts to 0.5 to 10 mol % in all the R groups,(B) a hydrogenpolysiloxane containing at least one silicon-bonded hydrogen atom per molecule in such an amount that the number of the silicon-bonded hydrogen atoms is 0.5 to 1.5 per vinyl group bonded to silicon atoms in the component (A), and(C) a platinum catalyst. From this composition, a silicone gel excellent damping properties, rapid curability, and low-temperature properties can be obtained.
摘要翻译：一种硅凝胶组合物，其包含基本组分（A）包含基本上90至97mol％的R（CH 3）SiO单元，0.1至2.5mol％的RSiO 1.5单元和0.1至4.0mol％的CH 3 R（CH 2） = CH）Si0.5单元，其中R表示选自甲基，苯基和CF 3 CH 2 CH 2 - 基团的基团，条件是R中的苯基和CF 3 CH 2 CH 2 - 基团的总数的基团在所有R基团中为0.5至10摩尔％，（B）每分子含有至少一个与硅键合的氢原子的氢聚硅氧烷，其量使得硅键合的氢原子的数量为每个乙烯基为0.5至1.5 组分（A）中与硅原子键合的基团，和（C）铂催化剂。通过该组合物，可以获得硅酮凝胶，阻尼性能优异，固化性快，温度低的特性。

6. 再颁专利

USRE40519E1 Conductive fluoro-resin compositions 失效
标题翻译：导电氟树脂组合物
公开(公告)号：USRE40519E1
公开(公告)日：2008-09-23
申请号：US10246412
申请日：2002-09-19
申请人： Hironao Fujiki , Hiroyasu Hara , Kenichi Fukuda
发明人： Hironao Fujiki , Hiroyasu Hara , Kenichi Fukuda
IPC分类号： C08J5/12 , C08K3/08 , C08L27/14
CPC分类号： H01B1/22 , C08K3/08 , C08K2003/0806 , C08L71/00
摘要： A conductive fluoro-resin composition of the addition reaction curing type is provided comprising (A) a reactive fluorinated polyether compound comprising fluorinated polyether units and having at least two aliphatic unsaturated hydrocarbon radicals in a molecule, (B) a compound having at least two hydrogen atoms each directly attached to a silicon atom, (C) a platinum group metal catalyst, and (D) silver particles. The composition cures into rubbery parts having improved heat resistance, weather resistance and solvent resistance and optionally forming firm bonds to various substrates.
摘要翻译：提供了一种加成反应固化型的导电性氟树脂组合物，其包含（A）包含氟化聚醚单元并且在分子中具有至少两个脂族不饱和烃基的反应性氟化聚醚化合物，（B）具有至少两个氢的化合物各自直接连接到硅原子的原子，（C）铂族金属催化剂和（D）银颗粒。该组合物固化成具有改善的耐热性，耐候性和耐溶剂性的橡胶状部分，并任选地形成与各种基材的牢固粘合。

7. 发明授权

US6121359A Conductive fluoro-resin compositions 有权
标题翻译：导电氟树脂组合物
公开(公告)号：US6121359A
公开(公告)日：2000-09-19
申请号：US210373
申请日：1998-12-14
申请人： Hironao Fujiki , Hiroyasu Hara , Kenichi Fukuda
发明人： Hironao Fujiki , Hiroyasu Hara , Kenichi Fukuda
IPC分类号： C08G77/46 , C08K3/08 , C08K5/544 , C08K9/06 , C08L71/00 , C08L83/05 , H01B1/22 , C08J5/12 , C08L27/14
CPC分类号： H01B1/22 , C08K3/08 , C08K2003/0806
摘要： A conductive fluoro-resin composition of the addition reaction curing type is provided comprising (A) a reactive fluorinated polyether compound comprising fluorinated polyether units and having at least two aliphatic unsaturated hydrocarbon radicals in a molecule, (B) a compound having at least two hydrogen atoms each directly attached to a silicon atom, (C) a platinum group metal catalyst, and (D) silver particles. The composition cures into rubbery parts having improved heat resistance, weather resistance and solvent resistance and optionally forming firm bonds to various substrates.
摘要翻译：提供了一种加成反应固化型的导电性氟树脂组合物，其包含（A）包含氟化聚醚单元并且在分子中具有至少两个脂族不饱和烃基的反应性氟化聚醚化合物，（B）具有至少两个氢的化合物各自直接连接到硅原子的原子，（C）铂族金属催化剂和（D）银颗粒。该组合物固化成具有改善的耐热性，耐候性和耐溶剂性的橡胶状部分，并任选地形成与各种基材的牢固粘合。

8. 发明申请

US20100004410A1 HYDROSILYLATION INHIBITOR, HYDROSILYLATION CATALYST COMPOSITION, AND CURABLE COMPOSITION 审中-公开
标题翻译：氢化抑制剂，氢化催化剂组合物和可固化组合物
公开(公告)号：US20100004410A1
公开(公告)日：2010-01-07
申请号：US12542193
申请日：2009-08-17
申请人： Shinji Kimura , Hiroyasu Hara , Masayuki Ikeno
发明人： Shinji Kimura , Hiroyasu Hara , Masayuki Ikeno
IPC分类号： C08F4/70 , B01J31/12 , C07F7/18
CPC分类号： C08L83/04 , C08G77/12 , C08G77/18 , C08G77/20 , C08G77/80 , C08K5/0091 , C08L83/00 , C08L2666/52
摘要： A hydrosilylation inhibitor comprising a reaction product of (1) a titanium compound having an alkoxy group in its ligand, and (2) an organosilicon compound having at least one hydrogen atom bonded to silicon atom per molecule is provided. This hydrosilylation inhibitor exhibits inhibitory activity for catalytic activity of a PGE (platinum group element)-bearing hydrosilylation catalyst in an oxygen atmosphere of up to 100 ppm and/or a moisture atmosphere of up to 100 ppm. By using the present invention, catalytic function of the hydrosilylation catalyst is reliably inhibited in the absence of oxygen and moisture while the same catalytic function is easily provided in the presence of the oxygen or the moisture.
摘要翻译：提供了一种氢化硅烷化抑制剂，其包含（1）在其配体中具有烷氧基的钛化合物和（2）每分子具有至少一个与硅原子键合的氢原子的有机硅化合物的反应产物。该氢化硅烷化抑制剂在高达100ppm的氧气氛和/或高达100ppm的湿气气氛中表现出对PGE（铂族元素）的氢化硅烷化催化剂的催化活性的抑制活性。通过使用本发明，在没有氧气和水分的情况下，可靠地抑制氢化硅烷化催化剂的催化功能，而在氧气或水分的存在下容易提供相同的催化功能。

9. 发明申请

US20080227938A1 HYDROSILYLATION INHIBITOR, HYDROSILYLATION CATALYST COMPOSITION, AND CURABLE COMPOSITION 审中-公开
标题翻译：氢化抑制剂，氢化催化剂组合物和可固化组合物
公开(公告)号：US20080227938A1
公开(公告)日：2008-09-18
申请号：US12045238
申请日：2008-03-10
申请人： Shinji KIMURA , Hiroyasu Hara , Masayuki Ikeno
发明人： Shinji KIMURA , Hiroyasu Hara , Masayuki Ikeno
IPC分类号： C08F4/606 , B01J31/12 , C07F7/28
CPC分类号： C08L83/04 , C08G77/12 , C08G77/18 , C08G77/20 , C08G77/80 , C08K5/0091 , C08L83/00 , C08L2666/52
摘要： A hydrosilylation inhibitor comprising a reaction product of (1) a titanium compound having an alkoxy group in its ligand, and (2) an organosilicon compound having at least one hydrogen atom bonded to silicon atom per molecule is provided. This hydrosilylation inhibitor exhibits inhibitory activity for catalytic activity of a PGE (platinum group element)-bearing hydrosilylation catalyst in an oxygen atmosphere of up to 100 ppm and/or a moisture atmosphere of up to 100 ppm. By using the present invention, catalytic function of the hydrosilylation catalyst is reliably inhibited in the absence of oxygen and moisture while the same catalytic function is easily provided in the presence of the oxygen or the moisture.
摘要翻译：提供了一种氢化硅烷化抑制剂，其包含（1）在其配体中具有烷氧基的钛化合物和（2）每分子具有至少一个与硅原子键合的氢原子的有机硅化合物的反应产物。该氢化硅烷化抑制剂在高达100ppm的氧气氛和/或高达100ppm的湿气气氛中表现出对PGE（铂族元素）的氢化硅烷化催化剂的催化活性的抑制活性。通过使用本发明，在没有氧气和水分的情况下，可靠地抑制氢化硅烷化催化剂的催化功能，而在氧气或水分的存在下容易提供相同的催化功能。

10. 发明授权

US5391674A Process for producing branched organopolysiloxane 失效
标题翻译：生产支链有机聚硅氧烷的方法
公开(公告)号：US5391674A
公开(公告)日：1995-02-21
申请号：US197872
申请日：1994-02-17
申请人： Hiroyasu Hara , Masayuki Ikeno , Akihito Tsukuno
发明人： Hiroyasu Hara , Masayuki Ikeno , Akihito Tsukuno
IPC分类号： C08G77/06 , C08G77/10 , C08G77/38
CPC分类号： C08G77/10 , C08G77/06
摘要： A process for producing a branched organopolysiloxane, comprising the steps of subjecting mixture of (A) a trialkoxysilane having the general formula (1):R.sup.1 Si(OR.sup.2).sub.3 (1)wherein R.sup.1 is a hydrocarbon group, and R.sup.2 are each a hydrocarbon group, and (B) an organosiloxane oligomer obtained by hydrolysis-condensation of a silane compound having the general formula (2):R.sup.3.sub.a SiCl.sub.4-a (2)wherein R.sup.3 are each a hydrocarbon group and a is 2 or 3, to equilibration reaction in the presence of an alkali catalyst, and adding water, subsequently to or concurrently with the equilibration reaction, to the reaction mixture, thereby hydrolyzing the Si--OR.sup.2 groups contained in the organopolysiloxane resulting from the hydrolysis-condensation. A branched organopolysiloxane stable in molecular composition and properties such as viscosity, can be produced.
摘要翻译：一种制备支链有机聚硅氧烷的方法，包括以下步骤：（A）具有通式（1）的三烷氧基硅烷：其中R 1为烃基的R 1 Si（OR 2）3（1）和R 2各自为烃基，（B）通过具有通式（2）的硅烷化合物的水解缩合得到的有机硅氧烷低聚物：R3aSiCl4-a（2）其中R3各自为烃基，a为2或3，以平衡反应存在碱催化剂，然后在平衡反应中或同时向反应混合物中加入水，由此水解由水解缩合产生的有机聚硅氧烷中所含的Si-OR 2基团。可以制备分子组成稳定的分支有机聚硅氧烷和粘度等性质。

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