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1. 发明申请

US20060257776A1 Charge control agent and toner for electrostatic image development 审中-公开
公开(公告)号：US20060257776A1
公开(公告)日：2006-11-16
申请号：US11407097
申请日：2006-04-20
申请人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
发明人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
IPC分类号： G03G9/08 , C07F15/02
CPC分类号： G03G9/091 , C09B45/22 , G03G9/09783
摘要： A charge control agent of the present invention comprises aggregate particles of an azo-type iron complex salt represented by the following chemical formula [I] in the chemical formula [I], R1—, R2—, R3—, R4—, R5— and R6— are same or different to each other, n is 0.7 to 0.99, the aggregate particles have an average particle size of 1 to 4 microns and an average particle size of a primary particulate crystalline, that is fined the aggregate particles with ultrasonic irradiation, is at most 3 microns. A toner for developing an electrostatic image comprises a resin for the toner and the charge control agent.

2. 发明授权

US07094513B2 Charge control agent and toner for electrostatic image development 有权
标题翻译：电荷控制剂和静电图像显影用调色剂
公开(公告)号：US07094513B2
公开(公告)日：2006-08-22
申请号：US10718637
申请日：2003-11-24
申请人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
发明人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
IPC分类号： G03G9/087
CPC分类号： G03G9/091 , C09B45/22 , G03G9/09783
摘要： A charge control agent of the present invention comprises aggregate particles of an azo-type iron complex salt represented by the following chemical formula [I] in the chemical formula [I], R1—, R2—, R3—, R4—, R5— and R6— are same or different to each other, n is 0.7 to 0.99, the aggregate particles have an average particle size of 1 to 4 microns and an average particle size of a primary particulate crystalline, that is fined the aggregate particles with ultrasonic irradiation, is at most 3 microns. A toner for developing an electrostatic image comprises a resin for the toner and the charge control agent.
摘要翻译：本发明的电荷控制剂包括化学式[I]中R 1，R 2，R 0，...的化学式[I]表示的偶氮型铁络合盐的聚集体颗粒 R 2，R 3，R 4，R 5，R 6， - 彼此相同或不同，n为0.7至0.99，聚集颗粒的平均粒度为1至4微米，并且通过超声波照射对聚集体颗粒进行精细化的初级颗粒状晶体的平均粒径为最多3微米。用于显影静电图像的调色剂包括用于调色剂的树脂和电荷控制剂。

3. 发明申请

US20050250034A1 Charge control agent and toner for electrostatic image development 有权
标题翻译：电荷控制剂和静电图像显影用调色剂
公开(公告)号：US20050250034A1
公开(公告)日：2005-11-10
申请号：US10718637
申请日：2003-11-24
申请人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
发明人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
IPC分类号： C09B45/22 , G03G9/09 , G03G9/097 , G03G9/087
CPC分类号： G03G9/091 , C09B45/22 , G03G9/09783
摘要： A charge control agent of the present invention comprises aggregate particles of an azo-type iron complex salt represented by the following chemical formula [1] in the chemical formula [I], R1—, R2—, R3—, R4—, R5— and R6— are same or different to each other, n is 0.7 to 0.99, the aggregate particles have an average particle size of 1 to 4 microns and an average particle size of a primary particulate crystalline, that is fined the aggregate particles with ultrasonic irradiation, is at most 3 microns. A toner for developing an electrostatic image comprises a resin for the toner and the charge control agent.
摘要翻译：本发明的电荷控制剂包括在化学式[I]中，R 1，R 2，R 2， R 2，R 3，R 4，R 5，R 6， - 彼此相同或不同，n为0.7至0.99，聚集颗粒的平均粒度为1至4微米，并且通过超声波照射对聚集体颗粒进行精细化的初级颗粒状晶体的平均粒径为最多3微米。用于显影静电图像的调色剂包括用于调色剂的树脂和电荷控制剂。

4. 发明授权

US07479360B2 Electric charge controlling agent, toner for developing electrostatic charge image containing the same, and method for forming image using the toner 有权
标题翻译：电荷控制剂，用于显影含有该静电荷图像的调色剂，以及使用该调色剂形成图像的方法
公开(公告)号：US07479360B2
公开(公告)日：2009-01-20
申请号：US10536404
申请日：2003-11-25
申请人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
发明人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
IPC分类号： G03G9/097 , C07F15/02
CPC分类号： G03G9/09783 , G03G9/091
摘要： The charge control agent comprises aggregate particles including an azo-type iron complex salt represented by the following chemical formula [VI] (in the chemical formula [VI], B+ is (H+)x(Na+) 1−x and x is mole ratio and 0.6 to 0.9, or B+ is (H+)y(Na+)1−y and y is mole ratio and 0 to 0.2) and the aggregate particles have 0.5 to 5.0 microns of an average particle size. A toner for developing an electrostatic image comprises a resin for the toner and the charge control agent. An image formation process of electrophotography comprises a step for developing an electrostatic latent image on an electrostatic latent image frame by a developer including the toner.
摘要翻译：电荷控制剂包括由以下化学式[VI]表示的偶氮型铁络合物盐（在化学式[VI]中，B +为（H +）x（Na +）1-x，x为摩尔比和0.6〜0.9，或B +为（H +）y（Na +）1-y，y为摩尔比，0〜0.2），骨料粒子的平均粒径为0.5〜5.0微米。用于显影静电图像的调色剂包括用于调色剂的树脂和电荷控制剂。电子照相术的图像形成方法包括通过包括调色剂的显影剂在静电潜像框上显影静电潜像的步骤。

5. 发明申请

US20060154165A1 Electric charge controlling agent, toner for developing electrostatic charge image containing the same, and method for forming image using the toner 有权
标题翻译：电荷控制剂，用于显影含有该静电荷图像的调色剂，以及使用该调色剂形成图像的方法
公开(公告)号：US20060154165A1
公开(公告)日：2006-07-13
申请号：US10536404
申请日：2003-11-25
申请人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
发明人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
IPC分类号： G03G9/097 , C07F15/02
CPC分类号： G03G9/09783 , G03G9/091
摘要： The charge control agent comprises aggregate particles including an azo-type iron complex salt represented by the following chemical formula [VI] (in the chemical formula [VI], B+ is (H+)x(Na+)1-x and x is mole ratio and 0.6 to 0.9, or B+ is (H+)y(Na+)1-y and y is mole ratio and 0 to 0.2) and the aggregate particles have 0.5 to 5.0 microns of an average particle size. A toner for developing an electrostatic image comprises a resin for the toner and the charge control agent. An image formation process of electrophotography comprises a step for developing an electrostatic latent image on an electrostatic latent image frame by a developer including the toner.
摘要翻译：电荷控制剂包括包含由以下化学式[VI]表示的偶氮型铁络合物的骨料颗粒（化学式[VI]中，B +）是（H + / SUP>）x 1（x + 1）x-x x，x是摩尔比，0.6-0.9，或B + 其中y是（H +），Y是摩尔比，Y是（H +） 0〜0.2），骨料粒子的平均粒径为0.5〜5.0微米。用于显影静电图像的调色剂包括用于调色剂的树脂和电荷控制剂。电子照相术的图像形成方法包括通过包括调色剂的显影剂在静电潜像框上显影静电潜像的步骤。

6. 发明授权

US08076465B2 Method for manufacturing charge control agent 有权
标题翻译：电荷控制剂制造方法
公开(公告)号：US08076465B2
公开(公告)日：2011-12-13
申请号：US10959069
申请日：2004-10-07
申请人： Kazuyoshi Kuroda , Masashi Yasumatsu , Osamu Yamate , Kaori Sato , Jun Hikata
发明人： Kazuyoshi Kuroda , Masashi Yasumatsu , Osamu Yamate , Kaori Sato , Jun Hikata
IPC分类号： C09B45/32
CPC分类号： G03G9/09783 , C09B45/14 , G03G9/091
摘要： A method for manufacturing a charge control agent comprising steps of: an initiative chelating step by reacting with a monoazo compound represented by the following chemical formula [1] (in the chemical formula [1], —Ar1— and —Ar2— are aromatic groups) and a metal chelating agent to prepare an azo-type metal complex salt intermediate; a subsequent ion-exchanging step by reacting with the azo-type metal complex salt intermediate and an ammonium counter ion forming agent including an inorganic ammonium salt and aqueous ammonia to prepare an azo-type metal complex salt having an ammonium ion of a counter ion represented by the following chemical formula [2] (in the chemical formula [2], —Ar1— and —Ar2— are the same as the chemical formula [1]; M is a trivalent metal; B+ is a cation except an ammonium ion; n is from 0.70 to 1.00).
摘要翻译：一种电荷控制剂的制造方法，包括以下步骤：通过与由下列化学式[1]表示的单偶氮化合物（在化学式[1]中，-Ar 1和-Ar 2）反应的主动螯合步骤是芳族基团）和金属螯合剂以制备偶氮型金属络合盐中间体; 随后的离子交换步骤通过与偶氮型金属络合物盐中间体和包含无机铵盐和氨水的铵抗衡离子形成剂反应以制备具有代表性的抗衡离子的铵离子的偶氮型金属络合盐通过以下化学式[2]（化学式[2]中，-Ar1-和-Ar2-与化学式[1]相同; M为三价金属; B +为除铵离子外的阳离子; n为0.70〜1.00）。

7. 发明申请

US20050084786A1 Method for manufacturing charge control agent 有权
标题翻译：电荷控制剂制造方法
公开(公告)号：US20050084786A1
公开(公告)日：2005-04-21
申请号：US10959069
申请日：2004-10-07
申请人： Kazuyoshi Kuroda , Masahi Yasumatsu , Osamu Yamate , Kaori Sato , Jun Hikata
发明人： Kazuyoshi Kuroda , Masahi Yasumatsu , Osamu Yamate , Kaori Sato , Jun Hikata
IPC分类号： G03G9/087 , C09B45/14 , G03G9/08 , G03G9/09 , G03G9/097
CPC分类号： G03G9/09783 , C09B45/14 , G03G9/091
摘要： A method for manufacturing a charge control agent comprising steps of: an initiative chelating step by reacting with a monoazo compound represented by the following chemical formula [1] (in the chemical formula [1], —Ar1— and —Ar2— are aromatic groups) and a metal chelating agent to prepare an azo-type metal complex salt intermediate; a subsequent ion-exchanging step by reacting with the azo-type metal complex salt intermediate and an ammonium counter ion forming agent including an inorganic ammonium salt and aqueous ammonia to prepare an azo-type metal complex salt having an ammonium ion of a counter ion represented by the following chemical formula [2] (in the chemical formula [2], —Ar1— and —Ar2 are the same as the chemical formula [1]; M is a trivalent metal; B+ is a cation except an ammonium ion; n is from 0.70 to 1.00).
摘要翻译：一种电荷控制剂的制备方法，包括以下步骤：主动螯合步骤，通过与由下列化学式[1]表示的单偶氮化合物（化学式[1]，-Ar 1 - 和-Ar 2 - 是芳族基团）和金属螯合剂以制备偶氮型金属络盐中间体; 随后的离子交换步骤通过与偶氮型金属络合物盐中间体和包含无机铵盐和氨水的铵抗衡离子形成剂反应以制备具有代表性的抗衡离子的铵离子的偶氮型金属络合盐通过以下化学式[2]（化学式[2]中，-Ar 1和 - 2）与化学式[1]相同。 M是三价金属; B +是除了铵离子以外的阳离子，n为0.70〜1.00）。

8. 发明授权

US07879520B2 Toner for developing electrostatic image and image formation process using it 有权
标题翻译：用于显影静电图像的调色剂和使用它的图像形成过程
公开(公告)号：US07879520B2
公开(公告)日：2011-02-01
申请号：US11806922
申请日：2007-06-05
申请人： Kaori Sato , Masashi Yasumatsu
发明人： Kaori Sato , Masashi Yasumatsu
IPC分类号： G03G9/087
CPC分类号： G03G9/09783 , G03G9/081 , G03G9/0821 , G03G9/0823 , G03G9/08708 , G03G9/091
摘要： A toner for developing an electrostatic image comprises a binding resin for a toner and a charge control agent including an azo-type iron complex salt represented by the following chemical formula (1) (in the chemical formula (1), R1 and R3 are the same or different to each other and are an alkyl group having a straight chain or a branch chain of 3 to 8 carbons; R2a, R2b, R4a and R4b are the same or different to each other and are selected from the group consisting of a hydrogen atom, an alkyl group, an alkoxyl group, a halogen atom, a nitro group and a carboxyl group; A+ indicates m(H+)+n(K+)+p(Na+), which m, n and p satisfy numerical equations of m+n+p=1, 0.7≦m≦1, 0≦n≦0.3 and 0≦p≦0.3), wherein an average particle size thereof is 1 to 4 microns, and a specific volume resistivity thereof is ranging from 0.2×1015 to 7×1015 Ω·cm.
摘要翻译：用于显影静电图像的调色剂包括用于调色剂的粘合树脂和包含由以下化学式（1）表示的偶氮型铁络合盐的电荷控制剂（在化学式（1）中，R 1和R 3为彼此相同或不同，是具有3至8个碳原子的直链或支链的烷基; R 2a，R 2b，R 4a和R 4b彼此相同或不同，并且选自氢原子，烷基，烷氧基，卤素原子，硝基和羧基; A +表示m（H +）+ n（K +）+ p（Na +），m，n和p满足m + n + p = 1，0.7＆nlE; m＆nlE; 1,0＆amp; nlE; n＆nlE; 0.3和0＆amp; nlE; p＆nlE; 0.3），其中平均粒径为1至4微米，其体积电阻率范围为0.2× 1015〜7×1015＆OHgr;·cm。

9. 发明申请

US20070292779A1 Toner for developing electrostatic image and image formation process using it 有权
标题翻译：用于显影静电图像的调色剂和使用它的图像形成过程
公开(公告)号：US20070292779A1
公开(公告)日：2007-12-20
申请号：US11806922
申请日：2007-06-05
申请人： Kaori Sato , Masashi Yasumatsu
发明人： Kaori Sato , Masashi Yasumatsu
IPC分类号： G03G9/097 , G03G13/04
CPC分类号： G03G9/09783 , G03G9/081 , G03G9/0821 , G03G9/0823 , G03G9/08708 , G03G9/091
摘要： A toner for developing an electrostatic image comprises a binding resin for a toner and a charge control agent including an azo-type iron complex salt represented by the following chemical formula (1) (in the chemical formula (1), R1 and R3 are the same or different to each other and are an alkyl group having a straight chain or a branch chain of 3 to 8 carbons; R2a, R2b, R4a and R4b are the same or different to each other and are selected from the group consisting of a hydrogen atom, an alkyl group, an alkoxyl group, a halogen atom, a nitro group and a carboxyl group; A+ indicates m(H+)+n(K+)+p(Na+), which m, n and p satisfy numerical equations of m+n+p=1, 0.7≦m≦1, 0≦n≦0.3 and 0≦p≦0.3), wherein an average particle size thereof is 1 to 4 microns, and a specific volume resistivity thereof is ranging from 0.2×1015 to 7×1015 Ω·cm.
摘要翻译：用于显影静电图像的调色剂包括用于调色剂的粘合树脂和包含由以下化学式（1）表示的偶氮型铁配盐的电荷控制剂（在化学式（1）中，R 1 R 3和R 3彼此相同或不同，是具有3至8个碳原子的直链或支链的烷基; R 2a，，R 2b，R 4a和R 4b彼此相同或不同，并且选自氢原子，烷基，烷氧基，卤素原子，硝基和羧基; A ^{+表示m（H + +）+ n（K + 其中m，n和p满足m + n + p = 1，0.7 <= m <= 1,0,0 <= n的数值方程式， = 0.3和0 <= p <= 0.3），其中其平均粒度为1至4微米，其体积电阻率为0.2×10 15至7×10 15， /SUP>Omega.cm。}

10. 发明申请

US20100294081A1 METHOD AND APPARATUS FOR REMOVING AND RECOVERING COPPER FROM COPPER-CONTAINING ACIDIC WASTE LIQUID AND METHOD FOR PRODUCING COPPER-CONTAINING SUBSTANCE 有权
标题翻译：从包含酸性废液中去除和回收铜的方法和装置以及生产含铜物质的方法
公开(公告)号：US20100294081A1
公开(公告)日：2010-11-25
申请号：US12812252
申请日：2008-08-28
申请人： Atsushi Kobayashi , Toshihiro Suzuki , Kaori Sato , Yoko Kubota
发明人： Atsushi Kobayashi , Toshihiro Suzuki , Kaori Sato , Yoko Kubota
IPC分类号： C22B15/00 , C22B3/02 , C01G3/02
CPC分类号： C22B3/44 , C01G3/02 , C02F1/66 , C02F1/722 , C02F2101/20 , C02F2103/16 , C02F2209/06 , C22B3/02 , C22B7/008 , C22B15/0089 , Y02P10/234 , Y02P10/236 , Y02W30/54
摘要： The present invention relates to a method and apparatus for removing and recovering copper by treating an acidic waste liquid containing copper ions such as an etching waste liquid resulting from etching a copper printed board in an etching solution of cupric chloride and a waste liquid after renewing a plating bath liquid in producing electrolytic copper foil.The present invention relates to a copper recovering method of recovering copper from a copper-containing acidic waste liquid by adding a liquid mixture of a copper-containing acidic waste liquid and an oxidizing agent to an alkaline agent solution while a pH of the alkaline agent solution to which the liquid mixture has been added is being controlled so as not to decrease to seven or lower even for a moment, and by obtaining a solid material whose main component is copper oxide.
摘要翻译：本发明涉及一种通过处理含有铜离子的酸性废液的方法和装置，该方法和装置是在铜氯化物和废液的蚀刻溶液中蚀刻铜印刷板而得到的蚀刻废液，电镀液中生产电解铜箔。本发明涉及通过将碱性试剂溶液的pH添加到碱性试剂溶液中而将含铜酸性废液和氧化剂的液体混合物加入到含铜酸性废液中回收铜的铜回收方法，已经加入液体混合物的方法被控制成即使暂时不降低到七度或更低，并且通过获得主要成分是氧化铜的固体材料。

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