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1. 发明申请

US20060257776A1 Charge control agent and toner for electrostatic image development 审中-公开
公开(公告)号：US20060257776A1
公开(公告)日：2006-11-16
申请号：US11407097
申请日：2006-04-20
申请人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
发明人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
IPC分类号： G03G9/08 , C07F15/02
CPC分类号： G03G9/091 , C09B45/22 , G03G9/09783
摘要： A charge control agent of the present invention comprises aggregate particles of an azo-type iron complex salt represented by the following chemical formula [I] in the chemical formula [I], R1—, R2—, R3—, R4—, R5— and R6— are same or different to each other, n is 0.7 to 0.99, the aggregate particles have an average particle size of 1 to 4 microns and an average particle size of a primary particulate crystalline, that is fined the aggregate particles with ultrasonic irradiation, is at most 3 microns. A toner for developing an electrostatic image comprises a resin for the toner and the charge control agent.

2. 发明授权

US08076465B2 Method for manufacturing charge control agent 有权
标题翻译：电荷控制剂制造方法
公开(公告)号：US08076465B2
公开(公告)日：2011-12-13
申请号：US10959069
申请日：2004-10-07
申请人： Kazuyoshi Kuroda , Masashi Yasumatsu , Osamu Yamate , Kaori Sato , Jun Hikata
发明人： Kazuyoshi Kuroda , Masashi Yasumatsu , Osamu Yamate , Kaori Sato , Jun Hikata
IPC分类号： C09B45/32
CPC分类号： G03G9/09783 , C09B45/14 , G03G9/091
摘要： A method for manufacturing a charge control agent comprising steps of: an initiative chelating step by reacting with a monoazo compound represented by the following chemical formula [1] (in the chemical formula [1], —Ar1— and —Ar2— are aromatic groups) and a metal chelating agent to prepare an azo-type metal complex salt intermediate; a subsequent ion-exchanging step by reacting with the azo-type metal complex salt intermediate and an ammonium counter ion forming agent including an inorganic ammonium salt and aqueous ammonia to prepare an azo-type metal complex salt having an ammonium ion of a counter ion represented by the following chemical formula [2] (in the chemical formula [2], —Ar1— and —Ar2— are the same as the chemical formula [1]; M is a trivalent metal; B+ is a cation except an ammonium ion; n is from 0.70 to 1.00).
摘要翻译：一种电荷控制剂的制造方法，包括以下步骤：通过与由下列化学式[1]表示的单偶氮化合物（在化学式[1]中，-Ar 1和-Ar 2）反应的主动螯合步骤是芳族基团）和金属螯合剂以制备偶氮型金属络合盐中间体; 随后的离子交换步骤通过与偶氮型金属络合物盐中间体和包含无机铵盐和氨水的铵抗衡离子形成剂反应以制备具有代表性的抗衡离子的铵离子的偶氮型金属络合盐通过以下化学式[2]（化学式[2]中，-Ar1-和-Ar2-与化学式[1]相同; M为三价金属; B +为除铵离子外的阳离子; n为0.70〜1.00）。

3. 发明授权

US07094513B2 Charge control agent and toner for electrostatic image development 有权
标题翻译：电荷控制剂和静电图像显影用调色剂
公开(公告)号：US07094513B2
公开(公告)日：2006-08-22
申请号：US10718637
申请日：2003-11-24
申请人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
发明人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
IPC分类号： G03G9/087
CPC分类号： G03G9/091 , C09B45/22 , G03G9/09783
摘要： A charge control agent of the present invention comprises aggregate particles of an azo-type iron complex salt represented by the following chemical formula [I] in the chemical formula [I], R1—, R2—, R3—, R4—, R5— and R6— are same or different to each other, n is 0.7 to 0.99, the aggregate particles have an average particle size of 1 to 4 microns and an average particle size of a primary particulate crystalline, that is fined the aggregate particles with ultrasonic irradiation, is at most 3 microns. A toner for developing an electrostatic image comprises a resin for the toner and the charge control agent.
摘要翻译：本发明的电荷控制剂包括化学式[I]中R 1，R 2，R 0，...的化学式[I]表示的偶氮型铁络合盐的聚集体颗粒 R 2，R 3，R 4，R 5，R 6， - 彼此相同或不同，n为0.7至0.99，聚集颗粒的平均粒度为1至4微米，并且通过超声波照射对聚集体颗粒进行精细化的初级颗粒状晶体的平均粒径为最多3微米。用于显影静电图像的调色剂包括用于调色剂的树脂和电荷控制剂。

4. 发明申请

US20050250034A1 Charge control agent and toner for electrostatic image development 有权
标题翻译：电荷控制剂和静电图像显影用调色剂
公开(公告)号：US20050250034A1
公开(公告)日：2005-11-10
申请号：US10718637
申请日：2003-11-24
申请人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
发明人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
IPC分类号： C09B45/22 , G03G9/09 , G03G9/097 , G03G9/087
CPC分类号： G03G9/091 , C09B45/22 , G03G9/09783
摘要： A charge control agent of the present invention comprises aggregate particles of an azo-type iron complex salt represented by the following chemical formula [1] in the chemical formula [I], R1—, R2—, R3—, R4—, R5— and R6— are same or different to each other, n is 0.7 to 0.99, the aggregate particles have an average particle size of 1 to 4 microns and an average particle size of a primary particulate crystalline, that is fined the aggregate particles with ultrasonic irradiation, is at most 3 microns. A toner for developing an electrostatic image comprises a resin for the toner and the charge control agent.
摘要翻译：本发明的电荷控制剂包括在化学式[I]中，R 1，R 2，R 2， R 2，R 3，R 4，R 5，R 6， - 彼此相同或不同，n为0.7至0.99，聚集颗粒的平均粒度为1至4微米，并且通过超声波照射对聚集体颗粒进行精细化的初级颗粒状晶体的平均粒径为最多3微米。用于显影静电图像的调色剂包括用于调色剂的树脂和电荷控制剂。

5. 发明授权

US07479360B2 Electric charge controlling agent, toner for developing electrostatic charge image containing the same, and method for forming image using the toner 有权
标题翻译：电荷控制剂，用于显影含有该静电荷图像的调色剂，以及使用该调色剂形成图像的方法
公开(公告)号：US07479360B2
公开(公告)日：2009-01-20
申请号：US10536404
申请日：2003-11-25
申请人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
发明人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
IPC分类号： G03G9/097 , C07F15/02
CPC分类号： G03G9/09783 , G03G9/091
摘要： The charge control agent comprises aggregate particles including an azo-type iron complex salt represented by the following chemical formula [VI] (in the chemical formula [VI], B+ is (H+)x(Na+) 1−x and x is mole ratio and 0.6 to 0.9, or B+ is (H+)y(Na+)1−y and y is mole ratio and 0 to 0.2) and the aggregate particles have 0.5 to 5.0 microns of an average particle size. A toner for developing an electrostatic image comprises a resin for the toner and the charge control agent. An image formation process of electrophotography comprises a step for developing an electrostatic latent image on an electrostatic latent image frame by a developer including the toner.
摘要翻译：电荷控制剂包括由以下化学式[VI]表示的偶氮型铁络合物盐（在化学式[VI]中，B +为（H +）x（Na +）1-x，x为摩尔比和0.6〜0.9，或B +为（H +）y（Na +）1-y，y为摩尔比，0〜0.2），骨料粒子的平均粒径为0.5〜5.0微米。用于显影静电图像的调色剂包括用于调色剂的树脂和电荷控制剂。电子照相术的图像形成方法包括通过包括调色剂的显影剂在静电潜像框上显影静电潜像的步骤。

6. 发明申请

US20060154165A1 Electric charge controlling agent, toner for developing electrostatic charge image containing the same, and method for forming image using the toner 有权
标题翻译：电荷控制剂，用于显影含有该静电荷图像的调色剂，以及使用该调色剂形成图像的方法
公开(公告)号：US20060154165A1
公开(公告)日：2006-07-13
申请号：US10536404
申请日：2003-11-25
申请人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
发明人： Masashi Yasumatsu , Kazuyoshi Kuroda , Osamu Yamate , Kaori Sato , Jun Hikata , Heihachi Yushina
IPC分类号： G03G9/097 , C07F15/02
CPC分类号： G03G9/09783 , G03G9/091
摘要： The charge control agent comprises aggregate particles including an azo-type iron complex salt represented by the following chemical formula [VI] (in the chemical formula [VI], B+ is (H+)x(Na+)1-x and x is mole ratio and 0.6 to 0.9, or B+ is (H+)y(Na+)1-y and y is mole ratio and 0 to 0.2) and the aggregate particles have 0.5 to 5.0 microns of an average particle size. A toner for developing an electrostatic image comprises a resin for the toner and the charge control agent. An image formation process of electrophotography comprises a step for developing an electrostatic latent image on an electrostatic latent image frame by a developer including the toner.
摘要翻译：电荷控制剂包括包含由以下化学式[VI]表示的偶氮型铁络合物的骨料颗粒（化学式[VI]中，B +）是（H + / SUP>）x 1（x + 1）x-x x，x是摩尔比，0.6-0.9，或B + 其中y是（H +），Y是摩尔比，Y是（H +） 0〜0.2），骨料粒子的平均粒径为0.5〜5.0微米。用于显影静电图像的调色剂包括用于调色剂的树脂和电荷控制剂。电子照相术的图像形成方法包括通过包括调色剂的显影剂在静电潜像框上显影静电潜像的步骤。

7. 发明申请

US20050084786A1 Method for manufacturing charge control agent 有权
标题翻译：电荷控制剂制造方法
公开(公告)号：US20050084786A1
公开(公告)日：2005-04-21
申请号：US10959069
申请日：2004-10-07
申请人： Kazuyoshi Kuroda , Masahi Yasumatsu , Osamu Yamate , Kaori Sato , Jun Hikata
发明人： Kazuyoshi Kuroda , Masahi Yasumatsu , Osamu Yamate , Kaori Sato , Jun Hikata
IPC分类号： G03G9/087 , C09B45/14 , G03G9/08 , G03G9/09 , G03G9/097
CPC分类号： G03G9/09783 , C09B45/14 , G03G9/091
摘要： A method for manufacturing a charge control agent comprising steps of: an initiative chelating step by reacting with a monoazo compound represented by the following chemical formula [1] (in the chemical formula [1], —Ar1— and —Ar2— are aromatic groups) and a metal chelating agent to prepare an azo-type metal complex salt intermediate; a subsequent ion-exchanging step by reacting with the azo-type metal complex salt intermediate and an ammonium counter ion forming agent including an inorganic ammonium salt and aqueous ammonia to prepare an azo-type metal complex salt having an ammonium ion of a counter ion represented by the following chemical formula [2] (in the chemical formula [2], —Ar1— and —Ar2 are the same as the chemical formula [1]; M is a trivalent metal; B+ is a cation except an ammonium ion; n is from 0.70 to 1.00).
摘要翻译：一种电荷控制剂的制备方法，包括以下步骤：主动螯合步骤，通过与由下列化学式[1]表示的单偶氮化合物（化学式[1]，-Ar 1 - 和-Ar 2 - 是芳族基团）和金属螯合剂以制备偶氮型金属络盐中间体; 随后的离子交换步骤通过与偶氮型金属络合物盐中间体和包含无机铵盐和氨水的铵抗衡离子形成剂反应以制备具有代表性的抗衡离子的铵离子的偶氮型金属络合盐通过以下化学式[2]（化学式[2]中，-Ar 1和 - 2）与化学式[1]相同。 M是三价金属; B +是除了铵离子以外的阳离子，n为0.70〜1.00）。

8. 发明申请

US20100279150A1 INTERLAYER FILM FOR LAMINATED GLASS AND LAMINATED GLASS 有权
标题翻译：层压玻璃和层压玻璃的层间膜
公开(公告)号：US20100279150A1
公开(公告)日：2010-11-04
申请号：US12445566
申请日：2009-01-22
申请人： Bungo Hatta , Hirofumi Kitano , Minoru Inada , Jun Hikata
发明人： Bungo Hatta , Hirofumi Kitano , Minoru Inada , Jun Hikata
IPC分类号： C08K5/3417 , B32B27/00
CPC分类号： C07D209/24 , B32B17/10678 , B32B17/10688 , B32B17/10761 , C08K5/3417 , Y10T428/31627 , Y10T428/3163 , Y10T428/31645 , Y10T428/31649 , Y10T428/31942 , Y10T428/31946 , C08L29/14
摘要： It is an object of the present invention to provide an interlayer film for a laminated glass which can reduce transmittance of ultraviolet rays having wavelength of 380 to 400 nm and has excellent durability to light exposure while maintaining high visible light transmittance.The interlayer film for a laminated glass of the present invention is an interlayer film for a laminated glass, which comprises a thermoplastic resin and an indole compound having a structure represented by the following general Chemical Formula (1): wherein R1 represents an alkyl group having 1 to 3 of carbon atoms, and R2 represents hydrogen, an alkyl group having 1 to 10 of carbon atoms, or an aralkyl group having 7 to 10 of carbon atoms.
摘要翻译：本发明的目的是提供一种能够降低波长为380〜400nm的紫外线的透射率并且在保持高的可见光透射率的同时具有优异的耐曝光性的夹层玻璃用中间膜。本发明的夹层玻璃用中间膜是夹层玻璃用中间膜，其包含热塑性树脂和具有以下通式（1）表示的结构的吲哚化合物：其中，R1表示具有 1〜3个碳原子，R2表示氢，碳原子数为1〜10的烷基或碳原子数为7〜10的芳烷基。

9. 发明授权

US08361625B2 Interlayer film for laminated glass and laminated glass 有权
标题翻译：用于夹层玻璃和夹层玻璃的夹层膜
公开(公告)号：US08361625B2
公开(公告)日：2013-01-29
申请号：US12445566
申请日：2009-01-22
申请人： Bungo Hatta , Hirofumi Kitano , Minoru Inada , Jun Hikata
发明人： Bungo Hatta , Hirofumi Kitano , Minoru Inada , Jun Hikata
IPC分类号： B32B17/10 , B32B27/42 , C08K5/3417
CPC分类号： C07D209/24 , B32B17/10678 , B32B17/10688 , B32B17/10761 , C08K5/3417 , Y10T428/31627 , Y10T428/3163 , Y10T428/31645 , Y10T428/31649 , Y10T428/31942 , Y10T428/31946 , C08L29/14
摘要： An interlayer film for a laminated glass which reduces transmittance of ultraviolet rays having wavelength of 380 to 400 nm and has an excellent durability to light exposure, while maintaining high visible light transmittance. The interlayer film for a laminated glass comprises a thermoplastic resin and an indole compound having a structure represented by the following chemical formula 1: Wherein R1 represents an alkyl group having 1-3 carbon atoms, and R2 represents hydrogen, an alkyl group having 1-10 carbon atoms, or an aralkyl group having 7-10 carbon atoms.
摘要翻译：一种用于夹层玻璃的中间膜，其降低具有380至400nm波长的紫外线的透射率，并且在保持高可见光透射率的同时具有优异的耐曝光性。夹层玻璃用中间膜包含热塑性树脂和具有以下化学式1表示的结构的吲哚化合物：其中，R1表示碳原子数1〜3的烷基，R2表示氢原子， 10个碳原子或具有7-10个碳原子的芳烷基。

10. 发明申请

US20130194659A1 INTERLAYER FOR LAMINATED GLASS, AND LAMINATED GLASS 有权
标题翻译：层压玻璃和层压玻璃的层间隔层
公开(公告)号：US20130194659A1
公开(公告)日：2013-08-01
申请号：US13817611
申请日：2011-08-19
申请人： Bungo Hatta , Kazuhiko Nakayama , Minoru Inada , Yuji Masaki , Jun Hikata
发明人： Bungo Hatta , Kazuhiko Nakayama , Minoru Inada , Yuji Masaki , Jun Hikata
IPC分类号： G02B1/04
CPC分类号： G02B1/04 , B32B17/10036 , B32B17/10678 , B32B17/10688 , B32B17/10761 , C08K5/3417 , C08K5/3475 , G02B5/223 , C08L29/14
摘要： The present invention aims to provide an interlayer film for laminated glass which can suppress the transmittance of ultraviolet rays with a wave length of 400 nm to 1% or less, and has high light resistance; and laminated glass including the interlayer film for laminated glass. The present invention provides an interlayer film for laminated glass including a thermoplastic resin, an ultraviolet absorber having a structure represented by the following formula (1), and an ultraviolet absorber having a structure represented by the following formula (2), wherein the amount of the ultraviolet absorber having a structure represented by the following formula (1) is 0.001 to 0.05% by weight, and the amount of the ultraviolet absorber having a structure represented by the following formula (2) is 0.4 to 1.5% by weight. In the formula (1), R1 represents a C1 to C3 alkyl group, and R2 represents hydrogen, a C1 to C10 alkyl group, or a C7 to C10 aralkyl group.In the formula (2), R3 represents hydrogen or a C1 to C8 alkyl group, and R4 represents hydrogen or a C1 to C8 alkyl group.
摘要翻译：本发明的目的在于提供一种能够抑制波长为400nm〜1％以下的紫外线的透射率并且耐光性高的夹层玻璃用中间膜。以及包含夹层玻璃用中间膜的夹层玻璃。本发明提供一种夹层玻璃用中间膜，其包含热塑性树脂，具有下述式（1）表示的结构的紫外线吸收剂和具有下述式（2）所示结构的紫外线吸收剂，其中，具有下式（1）表示的结构的紫外线吸收剂为0.001〜0.05重量％，由下式（2）表示的结构的紫外线吸收剂的量为0.4〜1.5重量％。式（1）中，R 1表示C1〜C3烷基，R2表示氢，C1〜C10烷基或C7〜C10芳烷基。在式（2）中，R 3表示氢或C 1至C 8烷基，R 4表示氢或C 1至C 8烷基。

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