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1. 发明授权

US08337958B2 Manufacturing process of electrodes for electrolysis 有权
标题翻译：电解电极的制造工艺
公开(公告)号：US08337958B2
公开(公告)日：2012-12-25
申请号：US12381962
申请日：2009-03-18
申请人： Yi Cao , Masashi Hosonuma
发明人： Yi Cao , Masashi Hosonuma
IPC分类号： C23C14/30 , C23C14/58 , B05D3/02 , B05D5/12
CPC分类号： C25B11/0426 , C23C14/16 , C23C14/325 , C23C14/5806 , C23C14/5853 , C25C7/02
摘要： A process for manufacturing electrodes for electrolysis, including the steps of forming an arc ion plating undercoating layer comprising valve metal or valve metal alloy including a crystalline tantalum component and a crystalline titanium component on the surface of the electrode substrate comprising valve metal or valve metal alloy, by an arc ion plating method; heat sintering the electrode substrate to transform only the tantalum component of the arc ion plating undercoating layer into an amorphous substance; and forming an electrode catalyst layer on the surface of the arc ion plating undercoating layer including the valve metal or valve metal alloy including the tantalum component transformed to the amorphous substance and the crystalline titanium component.
摘要翻译：一种制造电解电极的方法，包括以下步骤：在电极基材的表面上形成包括结晶钽组分和结晶钛组分的阀金属或阀金属合金的电弧离子镀底涂层，其包括阀金属或阀金属合金，通过电弧离子镀法; 对电极基板进行加热烧结，仅将电弧离子电镀底涂层的钽成分变形为无定形物质; 以及在包括转换成非晶体的钽成分和结晶钛成分的阀金属或阀金属合金的电弧离子电镀底涂层的表面上形成电极催化剂层。

2. 发明授权

US07438790B2 Electrode for electrolysis and process for producing the same 有权
标题翻译：电解用电极及其制造方法
公开(公告)号：US07438790B2
公开(公告)日：2008-10-21
申请号：US11491917
申请日：2006-07-25
申请人： Masashi Hosonuma , Masaharu Uno , Tomoyasu Shibata , Yoshinori Nishiki , Tsuneto Furuta
发明人： Masashi Hosonuma , Masaharu Uno , Tomoyasu Shibata , Yoshinori Nishiki , Tsuneto Furuta
IPC分类号： C25B11/12
CPC分类号： C23C16/278 , B82Y30/00 , C02F1/46104 , C02F2001/46138 , C02F2001/46152 , C02F2101/30 , C02F2101/303 , C02F2101/34 , C02F2305/08 , C23C16/0254 , C23C16/271 , C25B11/0478
摘要： The present invention provides an electrode for electrolysis including: a conductive substrate; and a conductive diamond formed on a surface of the conductive substrate, the conductive substrate having at least one surface shape selected from the group consisting of: (a) a surface shape of a combination of an Ra of 100-1,000-μm and an RSm of 50-10,000 μm; (b) a surface shape of a combination of an Ra of 2.5-100 μm and an RSm of 1.5-800 μm, and (c) a surface shape of a combination of an Ra of 0.01-2 μm and an RSm of 0.005-250 μm, and a process for producing the electrode.
摘要翻译：本发明提供一种电解用电极，包括：导电性基板; 以及形成在所述导电基板的表面上的导电金刚石，所述导电基板具有选自以下的至少一种表面形状：（a）Ra为100-1,000μm的组合的表面形状和RSm 50-10,000 mum; （b）Ra为2.5〜100μm，RSm为1.5〜800μm的组合的表面形状，（c）Ra为0.01〜2μm，RSm为0.005〜 250μm，以及电极的制造方法。

3. 发明授权

US07232508B2 Electrolytic electrode and process of producing the same 有权
标题翻译：电解电极及其制造方法
公开(公告)号：US07232508B2
公开(公告)日：2007-06-19
申请号：US10839246
申请日：2004-05-06
申请人： Masashi Hosonuma
发明人： Masashi Hosonuma
IPC分类号： C25B11/10
CPC分类号： C25B11/041 , C23C18/1216 , C23C18/1241 , C23C18/1279 , C23C18/1295 , C25B11/0405 , C25B11/0442 , C25D17/10
摘要： An electrolytic electrode having an interlayer having more excellent peeling resistance and corrosion resistance and longer electrolytic life than conventional electrolytic electrodes and capable of flowing a large amount of current at the industrial level and a process of producing the same are provided. The electrolytic electrode includes a valve metal or valve metal alloy electrode substrate on the surface of which is formed a high-temperature oxidation film by oxidation, and which is coated with an electrode catalyst. The high-temperature oxidation film is integrated with the electrode substrate, whereby peeling resistance is enhanced. Further, by heating the high-temperature oxidation film together with the electrode catalyst, non-electron conductivity of the interlayer is modified, thereby making it possible to flow a large amount of current.
摘要翻译：提供一种具有中间层的电解电极，其具有比常规电解电极更好的耐剥离性，耐腐蚀性和更长的电解寿命，并且能够在工业级流动大量电流及其制造方法。电解电极包括阀金属或阀金属合金电极基板，其表面通过氧化形成高温氧化膜，并且涂覆有电极催化剂。高温氧化膜与电极基板一体化，从而提高耐剥离性。此外，通过与电极催化剂一起加热高温氧化膜，改变了中间层的非电子传导性，从而可以流过大量的电流。

4. 发明申请

US20070029190A1 Electrode for electrolysis and process for producing the same 有权
标题翻译：电解用电极及其制造方法
公开(公告)号：US20070029190A1
公开(公告)日：2007-02-08
申请号：US11491917
申请日：2006-07-25
申请人： Masashi Hosonuma , Masaharu Uno , Tomoyasu Shibata , Yoshinori Nishiki , Tsuneto Furuta
发明人： Masashi Hosonuma , Masaharu Uno , Tomoyasu Shibata , Yoshinori Nishiki , Tsuneto Furuta
IPC分类号： C25C7/02
CPC分类号： C23C16/278 , B82Y30/00 , C02F1/46104 , C02F2001/46138 , C02F2001/46152 , C02F2101/30 , C02F2101/303 , C02F2101/34 , C02F2305/08 , C23C16/0254 , C23C16/271 , C25B11/0478
摘要： The present invention provides an electrode for electrolysis including: a conductive substrate; and a conductive diamond formed on a surface of the conductive substrate, the conductive substrate having at least one surface shape selected from the group consisting of: (a) a surface shape of a combination of an Ra of 100-1,000-μm and an RSm of 50-10,000 μm; (b) a surface shape of a combination of an Ra of 2.5-100 μm and an RSm of 1.5-800 μm, and (c) a surface shape of a combination of an Ra of 0.01-2 μm and an RSm of 0.005-250 μm, and a process for producing the electrode.
摘要翻译：本发明提供一种电解用电极，包括：导电性基板; 以及形成在所述导电基板的表面上的导电金刚石，所述导电基板具有选自以下的至少一种表面形状：（a）Ra为100-1,000μm的组合的表面形状和RSm 50-10,000 mum; （b）Ra为2.5〜100μm，RSm为1.5〜800μm的组合的表面形状，（c）Ra为0.01〜2μm，RSm为0.005〜 250μm，以及电极的制造方法。

5. 发明授权

US5034186A Process for providing titanium composite having a porous surface 失效
标题翻译：提供具有多孔表面的钛复合材料的方法
公开(公告)号：US5034186A
公开(公告)日：1991-07-23
申请号：US932551
申请日：1986-11-20
申请人： Takayuki Shimamune , Hideo Sato , Masashi Hosonuma
发明人： Takayuki Shimamune , Hideo Sato , Masashi Hosonuma
IPC分类号： B22F7/04 , A61F2/00 , A61F2/30 , A61L27/30 , A61L27/56 , B22F3/11 , B22F5/00 , B22F7/00 , C22C1/04 , C22C1/08 , C25B11/04
CPC分类号： C22C1/0458 , A61F2/30767 , A61L27/306 , A61L27/56 , B22F7/004 , C25B11/041 , A61F2002/30011 , A61F2002/30968 , A61F2250/0023 , A61F2310/00023 , A61F2310/00407 , B22F2998/00 , Y10T428/12042 , Y10T428/12063
摘要： A titanium or titanium alloy composite having a porous surface layer, which comprises a titanium or titanium alloy substrate and a porous titanium or titanium alloy layer that adheres strongly to said substrate, said porous layer being formed by first providing said substrate with a firmly adhering sinter of a mixture of a titanium or titanium alloy powder and a magnesium powder, and then removing magnesium from the sinter. A process for producing a titanium or titanium alloy composite having a porous surface layer, comprising: providing a coating composition comprising a binder added to a mixture of a titanium or titanium alloy powder and a magnesium powder; applying said composition to the surface of a titanium or titanium alloy substrate; heating the substrate at a temperature of from 650.degree. to 800.degree. C. in vacuo or an inert atmosphere so as to form a sinter of the powders of titanium or titanium alloy and magnesium which firmly adheres to said substrate; and removing magnesium from said sinter.
摘要翻译：一种具有多孔表面层的钛或钛合金复合体，其包括钛或钛合金基底和与所述基底强烈粘附的多孔钛或钛合金层，所述多孔层通过首先为所述基底提供牢固粘附的烧结体的钛或钛合金粉末和镁粉末的混合物，然后从烧结体中除去镁。一种制备具有多孔表面层的钛或钛合金复合材料的方法，包括：提供包含添加到钛或钛合金粉末和镁粉末的混合物中的粘合剂的涂料组合物; 将所述组合物施加到钛或钛合金基材的表面; 在真空或惰性气氛中，在650〜800℃的温度下加热基材，形成钛或钛合金和镁的粉末的烧结体，其牢固地附着在所述基材上; 并从所述烧结矿中除去镁。

6. 发明授权

US4847163A Metal-metal oxide composites and a coating layer of calcium phosphate on the oxide layer 失效
标题翻译：金属 - 金属氧化物复合物和氧化物层上的磷酸钙涂层
公开(公告)号：US4847163A
公开(公告)日：1989-07-11
申请号：US109887
申请日：1987-10-19
申请人： Takayuki Shimamune , Masashi Hosonuma
发明人： Takayuki Shimamune , Masashi Hosonuma
IPC分类号： A61C13/00 , A61C13/083 , A61C13/087 , A61F2/00 , A61K6/04 , A61L27/00 , A61L27/32 , C23C28/00
CPC分类号： C23C28/04 , A61L27/32 , C23C28/044 , A61F2310/00796 , Y10T428/12583 , Y10T428/1259 , Y10T428/12736 , Y10T428/12771 , Y10T428/12806
摘要： A calcium phosphate-coated composite material is disclosed, comprising a metallic substrate, an oxide layer on the metallic substrate, said oxide layer consisting essentially of the oxide of one or more metals selected from the group consisting of titanium, zirconium, hafnium, niobium, tantalum, tin, cobalt, aluminum, chromium, molybdenum and tungsten, and a coating layer of calcium phosphate provided on the oxide layer. A process for production of the calcium phosphate-coated composite material is also disclosed.
摘要翻译：公开了一种磷酸钙涂覆的复合材料，其包括金属基底，金属基底上的氧化物层，所述氧化物层主要由选自钛，锆，铪，铌等的一种或多种金属的氧化物组成，钽，锡，钴，铝，铬，钼和钨，以及设置在氧化物层上的磷酸钙涂层。还公开了一种生产磷酸钙复合材料的方法。

7. 发明授权

US4500405A Cathode for electrolyzing acid solutions and process for producing the same 失效
公开(公告)号：US4500405A
公开(公告)日：1985-02-19
申请号：US568515
申请日：1984-01-09
申请人： Hisoshi Asano , Takayuki Shimamune , Toshiki Goto , Masashi Hosonuma
发明人： Hisoshi Asano , Takayuki Shimamune , Toshiki Goto , Masashi Hosonuma
IPC分类号： C25B11/02 , C25B11/04 , C25B11/06 , C25B11/10
CPC分类号： C25B11/0478 , C25B11/0489
摘要： A cathode for electrolyzing acid solutions which comprises an electrically conductive metal substrate, a spray coated layer of a cathode active material containing tungsten, tungsten carbide or a mixture thereof in an amount of 10% by weight or more on the substrate, and an impregnation coated layer of 1 g/m.sup.2 or more of an acid-resistant fluorine containing resin on the outside surface of the coated layer of cathode active material, and a process for producing such.

8. 发明授权

US4400408A Method for forming an anticorrosive coating on a metal substrate 失效
标题翻译：在金属基材上形成防腐涂层的方法
公开(公告)号：US4400408A
公开(公告)日：1983-08-23
申请号：US263542
申请日：1981-05-14
申请人： Hiroshi Asano , Takayuki Shimamune , Toshiki Goto , Hideo Nitta , Masashi Hosonuma
发明人： Hiroshi Asano , Takayuki Shimamune , Toshiki Goto , Hideo Nitta , Masashi Hosonuma
IPC分类号： C25B11/06 , B22F7/04 , C23C18/14 , C23C24/08 , C23C24/10 , C23C26/00 , C25B11/10 , B05D3/02 , B05D3/12
CPC分类号： C23C24/106 , B22F7/04 , C23C18/14 , C23C24/08
摘要： A method for forming an anticorrosive coating on the surface of a metal substrate, which comprises, in one embodiment, (1) coating the surface of the metal substrate with an anticorrosive metal capable of forming an alloy with the substrate metal and/or a hydride of the anticorrosive metal; (2) heating the coated surface, and then; (3) heating the coated surface in a vacuum or in an atmosphere substantially inert to the metal coating and the metal substrate by irradiating the coated surface with electron beams, laser beams or a plasma arc to sinter the coated metal and form an alloy layer in the interface between the metal substrate and the metal coating and, in another embodiment, subsequent to Step (2) and prior Step (3) above, coating the coated surface with a solution of a thermally decomposable platinum-group metal compound and then heating the resulting coated surface at about 40.degree. C. to about 600.degree. C.
摘要翻译：一种在金属基材的表面上形成防腐涂层的方法，在一个实施方案中包括（1）用能够与基底金属和/或氢化物形成合金的防腐金属涂覆金属基材的表面的防腐金属; （2）加热涂层表面，然后; （3）通过用电子束，激光束或等离子体电弧照射涂覆的表面，在真空中或在基本上对金属涂层和金属基板惰性的气氛中加热涂覆的表面，以烧结涂覆的金属并形成合金层金属基材和金属涂层之间的界面，在另一个实施方案中，在上述步骤（2）和先前步骤（3）之后，用可热分解的铂族金属化合物的溶液涂覆涂布表面，然后加热得到的涂覆表面在约40℃至约600℃

9. 发明申请

US20090246410A1 Manufacturing process of electrodes for electrolysis 有权
标题翻译：电解电极的制造工艺
公开(公告)号：US20090246410A1
公开(公告)日：2009-10-01
申请号：US12381962
申请日：2009-03-18
申请人： Yi Cao , Masashi Hosonuma
发明人： Yi Cao , Masashi Hosonuma
IPC分类号： C23C14/26
CPC分类号： C25B11/0426 , C23C14/16 , C23C14/325 , C23C14/5806 , C23C14/5853 , C25C7/02
摘要： A process for manufacturing electrodes for electrolysis, including the steps of forming an arc ion plating undercoating layer comprising valve metal or valve metal alloy including a crystalline tantalum component and a crystalline titanium component on the surface of the electrode substrate comprising valve metal or valve metal alloy, by an arc ion plating method; heat sintering the electrode substrate to transform only the tantalum component of the arc ion plating undercoating layer into an amorphous substance; and forming an electrode catalyst layer on the surface of the arc ion plating undercoating layer including the valve metal or valve metal alloy including the tantalum component transformed to the amorphous substance and the crystalline titanium component.
摘要翻译：一种制造电解电极的方法，包括以下步骤：在电极基材的表面上形成包括结晶钽组分和结晶钛组分的阀金属或阀金属合金的电弧离子镀底涂层，其包括阀金属或阀金属合金，通过电弧离子镀法; 对电极基板进行加热烧结，仅将电弧离子电镀底涂层的钽成分变形为无定形物质; 以及在包括转换成非晶体的钽成分和结晶钛成分的阀金属或阀金属合金的电弧离子电镀底涂层的表面上形成电极催化剂层。

10. 发明授权

US07468121B2 Conductive diamond electrode and process for producing the same 有权
标题翻译：导电金刚石电极及其制造方法
公开(公告)号：US07468121B2
公开(公告)日：2008-12-23
申请号：US11496394
申请日：2006-08-01
申请人： Masashi Hosonuma , Masaharu Uno , Tomoyasu Shibata , Yoshinori Nishiki , Tsuneto Furuta
发明人： Masashi Hosonuma , Masaharu Uno , Tomoyasu Shibata , Yoshinori Nishiki , Tsuneto Furuta
IPC分类号： C25B11/12
CPC分类号： C25B11/0442 , C02F1/46109 , C02F2001/46138 , C23C16/0281 , C23C16/271 , C23C16/278 , Y10T428/12535 , Y10T428/12625
摘要： The present invention provides a conductive diamond electrode having: a conductive substrate; a coating layer formed on a surface of the conductive substrate, the coating layer containing one of a metal and an alloy each including at least one of niobium and tantalum; and a conductive diamond layer formed on a surface of the coating layer, and a process for producing the conductive diamond electrode.
摘要翻译：本发明提供一种导电金刚石电极，其具有导电性基板; 形成在所述导电性基材的表面上的被覆层，所述被覆层含有金属和合金中的至少一种，包含铌和钽中的至少一种; 以及形成在所述涂层的表面上的导电金刚石层，以及所述导电金刚石电极的制造方法。

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