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1. 发明授权

US07199178B2 Low-solvent, OH-functional dispersions 有权
标题翻译：低溶剂，OH官能的分散体
公开(公告)号：US07199178B2
公开(公告)日：2007-04-03
申请号：US11041774
申请日：2005-01-24
申请人： Martin Melchiors , Thomas Münzmay , Thomas Stingl , Hartmut Ottensmann , Heinz-Dietmar Gewiss
发明人： Martin Melchiors , Thomas Münzmay , Thomas Stingl , Hartmut Ottensmann , Heinz-Dietmar Gewiss
IPC分类号： C08L31/00 , C08L33/00 , C09D5/02 , C08F283/00 , C08F2/00 , C08F2/38 , C08J32/08
CPC分类号： C09J133/04 , C08K5/103 , C08L33/04 , C08L33/066 , C08L2666/04
摘要： A process for preparing copolymer dispersions that includes subjecting A) one or more vinyl monomer mixtures containing a) OH-free (meth)acrylic esters and/or vinylaromatics, b) hydroxy-functional vinyl monomers and/or hydroxy-functional (meth)acrylic esters, c) ionic and/or potentially ionic monomers capable of free-radical copolymerization, and d)optionally further monomers, other than the compounds of components a)–c), capable of free-radical copolymerization; to free-radical polymerization in the presence of e) compounds according to formula (I) where R1 is an aliphatic, araliphatic or aromatic radical having 1 to 18 carbon atoms, R2 is H or CH3, R3, R4 are identical or different aliphatc radicals having 1 to 7 carbon atoms and n is 1 to 4; and subsequently dispersing the resultant copolymer B) before or after addition of a neutralizing agent C) in water. The resulting dispersions can be used to coat substrates.
摘要翻译：一种制备共聚物分散体的方法，其包括使A）一种或多种乙烯基单体混合物含有a）不含OH的（甲基）丙烯酸酯和/或乙烯基芳烃，b）羟基官能的乙烯基单体和/或羟基官能（甲基）丙烯酸酯，c）能够进行自由基共聚的离子和/或潜在的离子单体，和d）任何其它单体，除了能够自由基共聚的组分a）-c）的化合物之外; 在e）根据式（I）的化合物存在下进行自由基聚合，

2. 发明申请

US20050165145A1 Low-solvent, OH-functional dispersions 有权
标题翻译：低溶剂，OH官能的分散体
公开(公告)号：US20050165145A1
公开(公告)日：2005-07-28
申请号：US11041774
申请日：2005-01-24
申请人： Martin Melchiors , Thomas Munzmay , Thomas Stingl , Hartmut Ottensmann , Heinz-Dietmar Gewiss
发明人： Martin Melchiors , Thomas Munzmay , Thomas Stingl , Hartmut Ottensmann , Heinz-Dietmar Gewiss
IPC分类号： C08F283/06 , C08K5/103 , C08L33/04 , C08L33/06 , C09D151/08 , C09J133/04 , C08K5/10
CPC分类号： C09J133/04 , C08K5/103 , C08L33/04 , C08L33/066 , C08L2666/04
摘要： A process for preparing copolymer dispersions that includes subjecting A) one or more vinyl monomer mixtures containing a) OH-free (meth)acrylic esters and/or vinylaromatics, b) hydroxy-functional vinyl monomers and/or hydroxy-functional (meth)acrylic esters, c) ionic and/or potentially ionic monomers capable of free-radical copolymerization, and d)optionally further monomers, other than the compounds of components a)-c), capable of free-radical copolymerization; to free-radical polymerization in the presence of e) compounds according to formula (I) where R1 is an aliphatic, araliphatic or aromatic radical having 1 to 18 carbon atoms, R2 is H or CH3, R3, R4 are identical or different aliphatc radicals having 1 to 7 carbon atoms and n is 1 to 4; and subsequently dispersing the resultant copolymer B) before or after addition of a neutralizing agent C) in water. The resulting dispersions can be used to coat substrates.
摘要翻译：一种制备共聚物分散体的方法，其包括使A）一种或多种乙烯基单体混合物含有a）不含OH的（甲基）丙烯酸酯和/或乙烯基芳烃，b）羟基官能的乙烯基单体和/或羟基官能（甲基）丙烯酸酯，c）能够进行自由基共聚的离子和/或潜在的离子单体，和d）任何其它单体，除了能够自由基共聚的组分a）-c）的化合物之外; 在e）根据式（I）的化合物存在下进行自由基聚合，其中R 1是具有1至18个碳原子的脂族，芳脂族或芳族基团，R 2， SUP>是H或CH 3，R 3，R 4是相同或不同的具有1至7个碳原子的烷基，n是1 到4; 随后将所得共聚物B）在加入中和剂C）之前或之后分散在水中。所得到的分散体可用于涂覆底物。

3. 发明申请

US20060100332A1 Polyester-polyacrylate dispersions with reactive diluents based on compounds containing lactone groups 审中-公开
标题翻译：聚酯 - 聚丙烯酸酯分散体与基于含内酯化合物的反应性稀释剂
公开(公告)号：US20060100332A1
公开(公告)日：2006-05-11
申请号：US11270218
申请日：2005-11-09
申请人： Rolf Gertzmann , Heinz-Dietmar Gewiss , Thomas Munzmay , Martin Melchiors
发明人： Rolf Gertzmann , Heinz-Dietmar Gewiss , Thomas Munzmay , Martin Melchiors
IPC分类号： C08K5/05
CPC分类号： C08J3/03 , C08J2367/00 , C08L33/08 , C08L33/10 , C08L67/00 , C08L67/04 , C09D167/00 , C08L2666/02 , C08L2666/18
摘要： The present invention related to a process for preparing aqueous polyester-polyacrylate dispersions having a cosolvent content of 0 to 5% by weight, based on the weight of the dispersion, by preparing a polymer P) in a first step by polymerizing A) a mixture of vinyl monomers that are capable of free-radical copolymerization, in the presence of B) one or more oligoesters prepared from compounds containing lactone groups and having a hydroxyl number of 145 to 710 mg KOH/g, an acid number of ≦0.5 mg KOH/g solids and an average OH functionality of 2.5 to 5 mg KOH/g solids, and then mixing polymer P) in a second step with C) one or more polyester polyols having a hydroxyl number of 10 to 500 mg KOH/g solids and an acid number of >0.5 to ≦30 mg KOH/g solids and dispersing the resulting polymer mixture in water in a further step, before or after addition of a neutralizing agent. The present invention also relates to the aqueous polyester-polyacrylate polymer dispersions obtained in accordance with the process of the invention and to aqueous coating compositions containing the aqueous polyester-polyacrylate polymer dispersions of the invention.
摘要翻译：本发明涉及通过聚合A）混合物在第一步中制备共聚物含量为0-5重量％，基于分散体重量的聚酯 - 聚丙烯酸酯分散体的方法，通过制备聚合物P）的乙烯基单体在B存在下存在下进行自由基共聚的乙烯基单体：一种或多种由含有内酯基团并且羟值为145至710mg KOH / g的化合物制备的低聚酯，酸值<= 0.5mg KOH / g固体，平均OH官能度为2.5至5mg KOH / g固体，然后在第二步中混合聚合物P）和C）一种或多种羟基数为10至500mg KOH / g固体的聚酯多元醇并且酸值> 0.5至<= 30mg KOH / g固体，并且在加入中和剂之前或之后将所得聚合物混合物进一步分散在水中。本发明还涉及根据本发明的方法获得的聚酯 - 聚丙烯酸酯聚合物水分散体和含有本发明的聚酯 - 聚丙烯酸酯聚合物水分散体的水性涂料组合物。

4. 发明申请

US20080214766A1 Binder combinations based on polyacrylate dispersions 审中-公开
标题翻译：基于聚丙烯酸酯分散体的粘合剂组合
公开(公告)号：US20080214766A1
公开(公告)日：2008-09-04
申请号：US12072815
申请日：2008-02-28
申请人： Thomas Munzmay , Sandra Hackbarth , Martin Melchiors , Heinz-Dietmar Gewiss
发明人： Thomas Munzmay , Sandra Hackbarth , Martin Melchiors , Heinz-Dietmar Gewiss
IPC分类号： C08F120/18
CPC分类号： C09D133/08
摘要： Aqueous polyacrylate dispersions comprising hydrophobic co-solvents are provided. The dispersions are prepared from copolymers P) which are comprised of I) a hydroxy-functional, hydrophobic polymer containing as structural monomers Ia) (meth)acrylic acid esters having from C1- to C18-hydrocarbon radicals in the alcohol part and/or vinyl aromatic compounds and/or vinyl esters and Ib) hydroxy-functional monomers; and II) a hydroxy-functional, hydrophilic polymer containing as structural components IIa) (meth)acrylic acid esters having from C1- to C18-hydrocarbon radicals in the alcohol part and/or vinyl aromatic compounds and/or vinyl esters, IIb) hydroxy-functional monomers and IIc) acid-functional monomers, and as solvents C) one or more solvents selected from the group consisting of hydrophobic, water-immiscible hydrocarbons having an initial boiling point of from 170° C. to 250° C. and a dry point of from 200° C. to 280° C., to a process for their preparation and to their use as binders for the production of blister-free coatings.
摘要翻译：提供了包含疏水性共溶剂的聚丙烯酸酯水分散体。分散体由共聚物P）制备，其由I）含有作为结构单体的羟基官能的疏水性聚合物Ia）（甲基）丙烯酸酯，其具有C 1至C 12 - 醇部分和/或乙烯基芳族化合物和/或乙烯基酯中的18-烃基和Ib）羟基官能单体; 和II）含有作为结构成分的结构组分的羟基官能的亲水性聚合物IIa）在醇中具有C 1至C 18 - 烃基的（甲基）丙烯酸酯部分和/或乙烯基芳族化合物和/或乙烯基酯，IIb）羟基官能单体和IIc）酸官能单体和溶剂C）一种或多种选自疏水性，水不混溶烃的溶剂，其具有初始沸点为170℃至250℃，干燥温度为200℃至280℃，其制备方法和用作生产无泡涂料的粘合剂。

5. 发明申请

US20090105409A1 AQUEOUS SECONDARY POLYMER DISPERSIONS FOR THE PRODUCTION OF COATINGS 失效
标题翻译：用于生产涂料的水性二次聚合物分散体
公开(公告)号：US20090105409A1
公开(公告)日：2009-04-23
申请号：US12177256
申请日：2008-07-22
申请人： Thomas Munzmay , Alice Munzmay , Martin Melchiors , Sandra Hackbarth , Heinz-Dietmar Gewiss
发明人： Thomas Munzmay , Alice Munzmay , Martin Melchiors , Sandra Hackbarth , Heinz-Dietmar Gewiss
IPC分类号： C09D133/12 , C08L33/12
CPC分类号： C08F263/02 , C08F257/02 , C08F263/00 , C08F265/00 , C08F265/04 , C08L51/003 , C09D4/00 , C09D151/003 , C08L2666/02
摘要： The invention concerns aqueous secondary polymer dispersions based on special acrylate building blocks, a process for their production and their use as binders for the production of blister-free coatings.
摘要翻译：本发明涉及基于特殊丙烯酸酯结构单元的水性次级聚合物分散体，其生产方法及其作为用于生产无泡罩涂料的粘合剂的用途。

6. 发明申请

US20060100348A1 Polyester-polyacrylate dispersions with reactive diluents based on hydroxy-functional esters 审中-公开
标题翻译：具有基于羟基官能酯的反应性稀释剂的聚酯 - 聚丙烯酸酯分散体
公开(公告)号：US20060100348A1
公开(公告)日：2006-05-11
申请号：US11270234
申请日：2005-11-09
申请人： Rolf Gertzmann , Heinz-Dietmar Gewiss , Thomas Munzmay , Martin Melchiors
发明人： Rolf Gertzmann , Heinz-Dietmar Gewiss , Thomas Munzmay , Martin Melchiors
IPC分类号： C09B67/00
CPC分类号： C08J3/03 , C08J2367/00 , C08K5/11 , C08L33/08 , C08L33/10 , C08L67/00 , C08L2201/50 , C09D167/00 , C08L2666/04
摘要： The present invention relates to a process for preparing aqueous, hydroxy-functional polyester-polyacrylate dispersions having a cosolvent content of 0 to 5% by weight, based on the weight of the dispersion, by preparing a polymer P) in a first step by polymerizing A) a mixture of vinyl monomers that are capable of free-radical copolymerization, in the presence of B) one or more compound(s) of formula (I) wherein R1 is an aliphatic, araliphatic or aromatic radical having 1 to 18 carbon atoms, R2 is H or CH3, R3 and R4 are identical or different aliphatic radicals having 1 to 7 carbon atoms, and n is 1 to 4, and then mixing polymer P) in a second step with C) one or more polyester polyols having a hydroxyl number of 10 to 500 mg KOH/g solids and an acid number of >0.5 to ≦30 mg KOH/g solids, and dispersing the resulting polymer mixture in water in a further step, before or after addition of a neutralizing agent. The present invention also relates to the aqueous polyester-polyacrylate polymer dispersions obtained in accordance with the process of the invention and to aqueous coating compositions containing the aqueous polyester-polyacrylate polymer dispersions of the invention.
摘要翻译：本发明涉及一种通过在第一步骤中通过聚合制备聚合物P而制备基于分散体重量的共溶剂含量为0-5重量％的水性羟基官能聚酯 - 聚丙烯酸酯分散体的方法 A）在B）一种或多种式（I）化合物的存在下能够进行自由基共聚的乙烯基单体的混合物，其中R 1是脂族，芳脂族或具有1至18个碳原子的芳族基团，R 2是H或CH 3，R 3和R 4，是具有1至7个碳原子的相同或不同的脂族基团，n为1至4，然后在第二步中将聚合物P）与C）羟基数为10至500mg KOH / g的一种或多种聚酯多元醇固体，酸值> 0.5至<= 30mg KOH / g固体，并且在加入中和剂之前或之后将所得聚合物混合物进一步分散在水中。本发明还涉及根据本发明的方法获得的聚酯 - 聚丙烯酸酯聚合物水分散体和含有本发明的聚酯 - 聚丙烯酸酯聚合物水分散体的水性涂料组合物。

7. 发明申请

US20140142244A1 AQUEOUS RESIN COMPOSITION COMPRISING A POLYESTER-POLYURETHANE RESIN INCLUDING A DENDRITIC POLYOL 审中-公开
标题翻译：包含聚酯多元醇的聚酯 - 聚氨酯树脂的水性树脂组合物
公开(公告)号：US20140142244A1
公开(公告)日：2014-05-22
申请号：US14232411
申请日：2012-07-10
申请人： Marc Claudius Schrinner , Heinz-Dietmar Gewiss
发明人： Marc Claudius Schrinner , Heinz-Dietmar Gewiss
IPC分类号： C09D175/06
CPC分类号： C09D175/06 , C08G18/0823 , C08G18/3221 , C08G18/6644 , C08G18/6659 , C08G18/755 , C09D175/04
摘要： An aqueous resin composition comprises a polyester-polyurethane resin which is obtained by reacting, in a one-stage process or multi-stage process, a reaction mixture comprising a polyester polyol with a number-average molecular weight Mn of >400 g/mole to
摘要翻译：含水树脂组合物包含聚酯 - 聚氨酯树脂，该聚酯聚氨酯树脂通过在一步法或多步法中使包含数均分子量Mn> 400g / mol的聚酯多元醇的反应混合物与至少一种含有至少两个异氰酸酯反应性基团和至少一个能够形成阴离子的基团的化合物，多异氰酸酯和树枝状多元醇。树枝状多元醇可以从具有至少一个反应性羟基（X）的中心引发剂分子或引发剂聚合物获得，其中初始树结构形成时的羟基（X）与单体的羧基（Y）键合具有两个反应性基团（X）和（Y）的扩链剂，并且其中扩链剂具有至少一个羧基（Y）和至少两个羟基（X）或羟烷基取代的羟基（X）。

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