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1. 发明授权

US08206463B2 Colored article of manufacture and a process for its preparation 有权
标题翻译：彩色制品及其制备工艺
公开(公告)号：US08206463B2
公开(公告)日：2012-06-26
申请号：US11417720
申请日：2006-05-04
申请人： Mark W. Witman , Robert A. Pyles , Rick L. Archey , Joseph D. Ventura
发明人： Mark W. Witman , Robert A. Pyles , Rick L. Archey , Joseph D. Ventura
IPC分类号： D06P3/60 , D06P5/00 , D06P3/52 , D06P3/70 , D06P3/79 , D06P3/24 , C09B67/00
CPC分类号： C08J7/065 , B05D5/06 , B05D5/067 , B27K5/02 , B33Y40/00 , B33Y70/00 , C03C17/32 , C03C17/38 , D06P1/65118 , D06P5/00
摘要： A process for making a colored article of manufacture is disclosed. Accordingly an article of manufacture is first prepared of a material selected from the group consisting of metal, wood, glass, ceramic, masonry and polymeric materials. A polymeric coating (superstrate) is then applied to at least a portion of the surface of the article. At least a portion of the superstrate is brought into contact with a material system that contains (i) water, (ii) a carrier, (iii) a dye and (iv) a diol, under conditions calculated to bring about diffusion of said dye into said superstrate.
摘要翻译：公开了制造彩色制品的方法。因此，首先由选自金属，木材，玻璃，陶瓷，砖石和聚合材料的材料制备制品。然后将聚合物涂层（覆盖层）施加到制品表面的至少一部分。所述覆层的至少一部分与材料体系接触，所述材料体系包含（i）水，（ii）载体，（iii）染料和（iv）二醇，所述条件被计算为使所述染料进入上层。

2. 发明申请

US20080286478A1 Apparatus and process for treating an article to impart color and/or enhance the properties of that article 有权
标题翻译：用于处理制品以赋予颜色和/或增强该制品的性质的装置和方法
公开(公告)号：US20080286478A1
公开(公告)日：2008-11-20
申请号：US11803917
申请日：2007-05-16
申请人： Edward F. Kaczkowski , Robert A. Pyles , Daniel E. Jaskiewicz , Rick L. Archey , George See , Ronald J. Rathi
发明人： Edward F. Kaczkowski , Robert A. Pyles , Daniel E. Jaskiewicz , Rick L. Archey , George See , Ronald J. Rathi
IPC分类号： B05D1/02 , B05B7/00
CPC分类号： B05D1/02 , B05D3/02 , B05D2201/00 , B05D2203/20 , C08J7/065 , D06M23/02 , D06M23/06 , D06P1/0016 , Y10T428/8305
摘要： A process and an apparatus for treating large articles to impart color or performance enhancing additives to the article in which a treatment system which includes: (i) a coloring solution and/or a solution containing at least one performance enhancing additive, (ii) water, and (iii) a solvent such as ethylene glycol monobutyl ether and diethylene glycol is applied to the article. The apparatus is made up of (a) a spray enclosure sized to contain the article(s) to be treated; (b) dispensing means, such as nozzles, which are configured to dispense sequentially, hot solution (i), hot solution (ii) and hot water (iii) directly onto the article surface(s); (c) means for securing and transporting the article to be treated into and out of the spray enclosure (such as a trolley system); and at least three closed vessels capable of delivering enough hot saturated coloring and/or performance enhancing solution, hot dye-free rinse solution and deionized water, respectively, with sufficient pressure to form small droplets from the spray nozzles, to thoroughly cover and rinse articles contained in the enclosure.
摘要翻译：一种用于处理大件物品以将颜色或性能增强添加剂赋予制品的方法和设备，其中处理系统包括：（i）着色溶液和/或含有至少一种性能增强添加剂的溶液，（ii）水，和（iii）将溶剂如乙二醇单丁醚和二甘醇应用于制品。该设备由（a）尺寸设计成容纳待处理物品的喷雾罩组成; （b）诸如喷嘴的分配装置，其被配置为将热溶液（i），热溶液（ii）和热水（iii）直接分配到物品表面上; （c）用于固定和运输要处理的物品进出喷雾外壳（例如手推车系统）的装置; 和至少三个密封容器，其能够分别以足够的压力输送足够的热饱和着色和/或性能增强溶液，不含热染料的漂洗溶液和去离子水，以从喷嘴形成小液滴，以彻底地覆盖和冲洗物品包含在外壳中。

3. 发明授权

US07175675B2 Method of dyeing a plastic article 有权
标题翻译：染色塑料制品的方法
公开(公告)号：US07175675B2
公开(公告)日：2007-02-13
申请号：US10733111
申请日：2003-12-11
申请人： Robert A. Pyles , Rick L. Archey , David M. Derikart
发明人： Robert A. Pyles , Rick L. Archey , David M. Derikart
IPC分类号： D06P5/00
CPC分类号： D06P1/613 , D06P1/60 , D06P1/65118 , D06P5/00
摘要： In the method of the present invention a plastic article (e.g., a molded article of thermoplastic polycarbonate) is immersed at least partially in a dye bath which includes one or more dyes, water, at least one carrier, and at least one diol. The dye bath contains: (i) at least one dye (e.g., a static and/or photochromic dye); (ii) water; (iii) at least one carrier represented by the following general formula I, R—O—(CH2)n—OHI wherein R is a radical selected from linear or branched C1–C18 alkyl, benzyl, benzoyl and phenyl, and n is 2 or 3; and (iv) a diol selected from at least one of linear or branched C2–C20 aliphatic diols, poly(C2–C4 alkylene glycol), cycloaliphatic diols having from 5 to 8 carbon atoms in the cyclic ring, monocyclic aromatic diols, bisphenols and hydrogenated bisphenols. In an embodiment of the present invention, the carrier is ethyleneglycol butyl ether, and the diol is diethylene glycol. The present invention also relates to a method of separating the dye from the water, carrier and diol components of the dye bath, by contacting the dye bath with particulate activated carbon.
摘要翻译：在本发明的方法中，将塑料制品（例如，热塑性聚碳酸酯的模塑制品）至少部分地浸入包括一种或多种染料，水，至少一种载体和至少一种二醇的染浴中。染浴包含：（i）至少一种染料（例如静电和/或光致变色染料）; （ii）水; （iii）由以下通式I表示的至少一种载体：<？in-line-formula description =“In-line Formulas”end =“lead”？> RO-（CH 2/2）其中R是选自直链或支链C 1〜C的基团，其中R是选自直链或支链C 1〜 C 18 -C 18烷基，苄基，苯甲酰基和苯基，n为2或3; 和（iv）选自直链或支链C 2 -C 20脂肪族二醇中的至少一种的二醇，聚（C 2 -C 20 - 亚烷基二醇），环中具有5-8个碳原子的脂环族二醇，单环芳族二醇，双酚和氢化双酚。在本发明的一个实施方案中，载体是乙二醇丁醚，二醇是二甘醇。本发明还涉及通过使染料浴与颗粒活性炭接触来分离染料与染浴的水，载体和二醇组分的方法。

4. 发明授权

US06733543B2 Process for making dyed articles 有权
标题翻译：染色制品的制造方法
公开(公告)号：US06733543B2
公开(公告)日：2004-05-11
申请号：US10106788
申请日：2002-03-26
申请人： Robert A. Pyles , Rick L. Archey
发明人： Robert A. Pyles , Rick L. Archey
IPC分类号： D06P500
CPC分类号： D06P3/54 , D06P1/613 , D06P1/928 , D06P3/00 , G02B1/041
摘要： A process of dyeing a molded article is disclosed. The process entails immersing at least a portion of the article in a dyeing bath, retaining the portion in the bath for a period of time sufficient to allow an amount of dye to diffuse into the article, and removing said article from the bath. The molded article comprises a polymeric resin such as (co)polyester, (co)polycarbonates, acrylonitrile-butadiene-styrene, polyamide, polyurethane, polyalkyl(meth)acrylate, allyldiglycol carbonate and styrene copolymers. The dyeing bath contains in addition to dye, water, a plasticizing agent and a leveling agent.
摘要翻译：公开了一种染色模制品的方法。该方法需要将至少一部分制品浸入染色浴中，将该部分保留在浴中一段足以使一定量的染料扩散到制品中的时间，以及从浴中除去所述制品。模制品包括聚合树脂，例如（共）聚酯，（共）聚碳酸酯，丙烯腈 - 丁二烯 - 苯乙烯，聚酰胺，聚氨酯，（甲基）丙烯酸烷基酯，烯丙基二醇碳酸酯和苯乙烯共聚物。染色浴除了染料，水，增塑剂和流平剂外还含有。

5. 发明授权

US07921680B2 Apparatus and process for treating an article to impart color and/or enhance the properties of that article 有权
标题翻译：用于处理制品以赋予颜色和/或增强该制品的性质的装置和方法
公开(公告)号：US07921680B2
公开(公告)日：2011-04-12
申请号：US11803917
申请日：2007-05-16
申请人： Edward F. Kaczkowski , Robert A. Pyles , Daniel E. Jaskiewicz , Rick L. Archey , George See , Ronald J. Rathi
发明人： Edward F. Kaczkowski , Robert A. Pyles , Daniel E. Jaskiewicz , Rick L. Archey , George See , Ronald J. Rathi
IPC分类号： D06F1/02
CPC分类号： B05D1/02 , B05D3/02 , B05D2201/00 , B05D2203/20 , C08J7/065 , D06M23/02 , D06M23/06 , D06P1/0016 , Y10T428/8305
摘要： A process and an apparatus for treating large articles to impart color or performance enhancing additives to the article in which a treatment system which includes: (i) a coloring solution and/or a solution containing at least one performance enhancing additive, (ii) water, and (iii) a solvent such as ethylene glycol monobutyl ether and diethylene glycol is applied to the article. The apparatus is made up of (a) a spray enclosure sized to contain the article(s) to be treated; (b) dispensing means, such as nozzles, which are configured to dispense sequentially, hot solution (i), hot solution (ii) and hot water (iii) directly onto the article surface(s); (c) means for securing and transporting the article to be treated into and out of the spray enclosure (such as a trolley system); and at least three closed vessels capable of delivering enough hot saturated coloring and/or performance enhancing solution, hot dye-free rinse solution and deionized water, respectively, with sufficient pressure to form small droplets from the spray nozzles, to thoroughly cover and rinse articles contained in the enclosure.
摘要翻译：一种用于处理大件物品以将颜色或性能增强添加剂赋予制品的方法和设备，其中处理系统包括：（i）着色溶液和/或含有至少一种性能增强添加剂的溶液，（ii）水，和（iii）将溶剂如乙二醇单丁醚和二甘醇应用于制品。该设备由（a）尺寸设计成容纳待处理物品的喷雾罩组成; （b）诸如喷嘴的分配装置，其被配置为将热溶液（i），热溶液（ii）和热水（iii）直接分配到物品表面上; （c）用于固定和运输要处理的物品进出喷雾外壳（例如手推车系统）的装置; 和至少三个密封容器，其能够分别以足够的压力输送足够的热饱和着色和/或性能增强溶液，不含热染料的漂洗溶液和去离子水，以从喷嘴形成小液滴，以彻底地覆盖和冲洗物品包含在外壳中。

6. 发明申请

US20090089942A1 Method of tinting a plastic article 审中-公开
标题翻译：塑料制品的着色方法
公开(公告)号：US20090089942A1
公开(公告)日：2009-04-09
申请号：US11973431
申请日：2007-10-09
申请人： Robert A. Pyles , Rick L. Archey
发明人： Robert A. Pyles , Rick L. Archey
IPC分类号： D06P3/24 , D06P3/79 , D06P3/52
CPC分类号： D06P1/00 , C08J7/065 , C08J2367/00 , C08J2371/00 , D06P1/0004 , D06P1/0008 , D06P1/0032
摘要： A method of tinting a plastic article is provided. The method comprises the steps of (a) providing a plastic article comprising a thermoset or thermoplastic polymer; (b) contacting at least a portion of the surface of said plastic article with a treatment composition comprising at least one dye and water; (c) maintaining said portion of said plastic article in contact with said treatment composition for a period of time at least sufficient to form a tinted plastic article; (d) removing said tinted plastic article from contact with said treatment composition; and (e) rinsing said tinted plastic article with water to remove excess dye. The method is carried out in the absence of an organic solvent, without the need for fixing or further processing steps.
摘要翻译：提供了一种着色塑料制品的方法。该方法包括以下步骤：（a）提供包含热固性或热塑性聚合物的塑料制品; （b）使所述塑料制品的表面的至少一部分与包含至少一种染料和水的处理组合物接触; （c）将所述塑料制品的所述部分保持与所述处理组合物接触至少足以形成有色塑料制品的时间; （d）除去所述有色塑料制品与所述处理组合物的接触; 和（e）用水漂洗所述有色塑料制品以除去多余的染料。该方法在不存在有机溶剂的情况下进行，而不需要固定或进一步的加工步骤。

7. 发明授权

US06929666B2 Composition comprising a dye 有权
标题翻译：包含染料的组合物
公开(公告)号：US06929666B2
公开(公告)日：2005-08-16
申请号：US10791114
申请日：2004-03-02
申请人： Robert A. Pyles , Rick L. Archey
发明人： Robert A. Pyles , Rick L. Archey
IPC分类号： D06P5/00 , D06P1/613 , D06P1/651 , D06P3/00 , D06P3/54 , D06P5/20 , C09B67/40
CPC分类号： D06P3/54 , D06P1/613 , D06P1/65131
摘要： A composition of matter (e.g., a molded article) is described. More particularly, the composition of matter includes: (a) a resinous component selected from at least one member of the group consisting of (co)polyester, (co)polycarbonates, acrylontrile-butadiene-styrene, polyamide, polyurethane, polyalkyl(meth)acrylate and styrene copolymers; (b) at least one dye; (c) a carrier represented by the following formula, R1[—O—(CH2)n]mOR2 wherein R2 is butyl, R1 is H, n is 2 or 3, and m is 2-35; and (d) optionally emulsifier. Also described is a dye bath that includes: (a) water; (b) at least one dye; (c) a carrier represented by the above formula; and (d) optionally an emulsifier.
摘要翻译：描述了一种物质的组成（例如模制品）。更具体地，物质组成包括：（a）选自（共）聚酯，（共）聚碳酸酯，丙烯腈 - 丁二烯 - 苯乙烯，聚酰胺，聚氨酯，聚（甲基）丙烯酸烷基酯，丙烯酸酯和苯乙烯共聚物; （b）至少一种染料; （c）由下式表示的载体：<？in-line-formula description =“In-line formula”end =“lead”？> R < - O-（CH

8. 发明授权

US06994735B2 Process for tinting plastic articles 有权
标题翻译：染色塑料制品的工艺
公开(公告)号：US06994735B2
公开(公告)日：2006-02-07
申请号：US10434242
申请日：2003-05-08
申请人： Robert A. Pyles , David M. Derikart , Rick L. Archey , Michael Nikolakopoulos
发明人： Robert A. Pyles , David M. Derikart , Rick L. Archey , Michael Nikolakopoulos
IPC分类号： D06P1/613
CPC分类号： D06P1/90 , C08J7/065 , C08J2369/00 , D06P1/65106 , D06P1/65118 , D06P1/65131
摘要： A process for tinting a molded article is disclosed. The process entails applying by spraying or by flow coating a hot, dye-solution onto at least a portion of the surface of a molded article to obtain a tinted article and washing the tinted article. In addition to the dissolved dye, the dye solution that is substantially free of particulate matter contains an aqueous solution of a carrier and an optional emulsifier. The article is one molded of a thermoplastic molding composition. In an embodiment of the invention, the dye solution is prepared by filtering a hot aqueous solution through a bag filter that contains a dye to obtain a hot, dye-solution. In a further embodiment, activated carbon is used to purify the dye solution to obtain a dye-free aqueous solution.
摘要翻译：公开了一种着色模制品的方法。该方法需要通过喷雾或通过将热的染料溶液流涂在模制品的表面的至少一部分上来获得有色制品并洗涤有色制品。除了溶解的染料之外，基本上不含颗粒物质的染料溶液含有载体和任选的乳化剂的水溶液。该制品是由热塑性模塑组合物成型的。在本发明的一个实施方案中，通过将热水溶液通过含有染料的袋式过滤器过滤以获得热的染料溶液来制备染料溶液。在另一个实施方案中，使用活性炭来纯化染料溶液以获得无染料的水溶液。

9. 发明授权

US06949127B2 Process for making dyed articles 有权
标题翻译：染色制品的制造方法
公开(公告)号：US06949127B2
公开(公告)日：2005-09-27
申请号：US10796523
申请日：2004-03-09
申请人： Robert A. Pyles , Rick L. Archey
发明人： Robert A. Pyles , Rick L. Archey
IPC分类号： G02C7/02 , D06P1/16 , D06P1/613 , D06P1/651 , D06P1/92 , D06P3/00 , D06P3/54 , D06P5/00 , D06P5/20 , G02B1/04 , D06P1/60 , D06P1/64
CPC分类号： D06P3/54 , D06P1/613 , D06P1/928 , D06P3/00 , G02B1/041
摘要： A process of dyeing a molded article is disclosed. The process entails immersing at least a portion of the article in a dyeing bath, retaining the portion in the bath for a period of time sufficient to allow an amount of dye to diffuse into the article, and removing said article from the bath. The molded article comprises a polymeric resin such as (co)polyester, (co)polycarbonates, acrylonitrile-butadiene-styrene, polyamide, polyurethane, polyalkyl(meth)-acrylate, allyldiglycol carbonate and styrene copolymers. The dyeing bath contains in addition to dye, water, a plasticizing agent and a leveling agent.
摘要翻译：公开了一种染色模制品的方法。该方法需要将至少一部分制品浸入染色浴中，将该部分保留在浴中一段足以使一定量的染料扩散到制品中的时间，以及从浴中除去所述制品。模制品包括聚合树脂，例如（共）聚酯，（共）聚碳酸酯，丙烯腈 - 丁二烯 - 苯乙烯，聚酰胺，聚氨酯，聚（甲基）丙烯酸烷基酯，烯丙基二醇碳酸酯和苯乙烯共聚物。染色浴除了染料，水，增塑剂和流平剂外还含有。

10. 发明授权

US07504054B2 Method of treating a plastic article 有权
标题翻译：处理塑料制品的方法
公开(公告)号：US07504054B2
公开(公告)日：2009-03-17
申请号：US10733657
申请日：2003-12-11
申请人： Robert A. Pyles , Rick L. Archey , David M. Derikart
发明人： Robert A. Pyles , Rick L. Archey , David M. Derikart
IPC分类号： B05D1/18 , B05D1/38 , G02C7/02
CPC分类号： C08J7/065
摘要： In the method of the present invention at least a portion of the surface of a plastic article (e.g., a molded article of thermoplastic polycarbonate) is contacted with (e.g., immersed in) a treatment composition which includes one or more performance additives. The treatment composition contains: (i) at least one performance additive (e.g., an ultraviolet light absorber); (ii) water; (iii) at least one carrier represented by the following general formula I, wherein R1 is a radical selected from the group consisting of linear or branched C1-C18 alkyl, benzyl, benzoyl and phenyl, R2 is a radical selected from the group consisting of linear or branched C1-C18 alkyl, benzyl, benzoyl, phenyl and H, n is 2, 3 or 4, and m is 1 to 35; and (iv) a diol selected from at least one of linear or branched C2-C20 aliphatic diols, poly(C2-C4 alkylene glycol), cycloaliphatic diols having from 5 to 8 carbon atoms in the cyclic ring, monocyclic aromatic diols, bisphenols and hydrogenated bisphenols. In an embodiment of the present invention, the carrier is ethyleneglycol monobutyl ether, and the diol is diethylene glycol.
摘要翻译：在本发明的方法中，将塑料制品的表面的至少一部分（例如，热塑性聚碳酸酯的模制品）与（例如，浸入）包含一种或多种性能添加剂的处理组合物接触。处理组合物包含：（i）至少一种性能添加剂（例如紫外光吸收剂）; （ii）水; （iii）由以下通式I表示的至少一种载体，其中R 1是选自直链或支链C 1 -C 18烷基，苄基，苯甲酰基和苯基的基团，R 2是选自直链或支链C 1 -C 18烷基，苄基，苯甲酰基，苯基和H，n为2,3或4，m为1至35; 和（iv）选自直链或支链C 2 -C 20脂族二醇，聚（C 2 -C 4亚烷基二醇），环中具有5至8个碳原子的脂环族二醇中的至少一种的二醇，单环芳族二醇，双酚和氢化双酚。在本发明的一个实施方案中，载体是乙二醇单丁醚，二醇是二甘醇。

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