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1. 发明授权

US07214394B2 Policosanol compositions, extraction from novel sources, and uses thereof 失效
标题翻译：二十二烷醇组合物，从新来源提取，及其用途
公开(公告)号：US07214394B2
公开(公告)日：2007-05-08
申请号：US10447212
申请日：2003-05-29
申请人： Mark W. Empie , Ahmad Hilaly , Alexandra J. Sanborn
发明人： Mark W. Empie , Ahmad Hilaly , Alexandra J. Sanborn
IPC分类号： A61K36/00
CPC分类号： C07C29/76 , A23L33/105 , A23L33/11 , A23L33/185 , A61K31/045 , C07C31/125
摘要： Compositions, novel isolation sources and processes, and uses for unique policosanol containing compositions are disclosed. Seed and vegetable processing byproduct and/or “waste” streams are disclosed as containing policosanols with various relative amounts of the various long chain fatty/waxy alcohols. The policosanols are isolated and may be combined with other phytochemical/processing products, and are used in numerous food, beverage, health and/or nutraceutical applications.
摘要翻译：公开了组合物，新型隔离源和方法以及用于独特的含聚乳糖醇的组合物的用途。种子和蔬菜加工副产物和/或“废物”流被公开为含有各种相对量的各种长链脂肪/蜡醇的聚山梨糖醇。聚山梨糖醇是分离的，并且可以与其它植物化学/加工产品组合，并且用于许多食品，饮料，健康和/或营养保健应用中。

2. 发明申请

US20070088182A1 Regenerating molecular sieve absorbents used for alcohol dehydration 有权
标题翻译：再生用于酒精脱水的分子筛吸附剂
公开(公告)号：US20070088182A1
公开(公告)日：2007-04-19
申请号：US11581825
申请日：2006-10-17
申请人： Ahmad Hilaly , Joseph Beggin
发明人： Ahmad Hilaly , Joseph Beggin
IPC分类号： C07C29/88 , B01J38/04
CPC分类号： B01J20/3408 , B01D15/00 , B01J20/18 , B01J20/3458 , B01J20/3483 , B01J29/90 , B01J38/02 , B01J38/04 , C07C29/76 , Y02P20/584 , C07C31/08
摘要： A process for regenerating a molecular sieve absorbent bed used for dehydrating an organic solvent is disclosed. The process is illustrated by regenerating a molecular sieve bed used for dehydrating ethanol, which includes a dehydrating cycle where an ethanol/water vapor mixture is loaded onto the molecular sieve bed at a first temperature to absorb water and recover a substantially dehydrated ethanol vapor effluent. In a regeneration cycle, the bed is subjected to a temperature swing technique whereby a dried gas, such as dried CO2, heated to at a second temperature greater than the first temperature, is passed over the molecular sieve bed, optimally in a counter current directional flow with respect to the dehydrating cycle. The process obviates the need for applying a vacuum pressure swing to regenerate the molecular sieve bed. Water and residual ethanol are removed with the CO2 effluent and can optionally be condensed and combined with a feed input for a subsequent dehydrating cycle.
摘要翻译：公开了一种用于再生用于使有机溶剂脱水的分子筛吸收剂床的方法。该方法通过再生用于脱水乙醇的分子筛床来说明，其包括脱水循环，其中乙醇/水蒸气混合物在第一温度下加载到分子筛床上以吸收水并回收基本上脱水的乙醇蒸汽流出物。在再生循环中，对床进行温度摆动技术，由此将加热到大于第一温度的第二温度的干燥的CO 2等干燥气体通过分子筛床，相对于脱水循环以最佳的逆流定向流动。该过程消除了施加真空压力摆动以再生分子筛床的需要。用CO 2 CO 2流出物除去水和残余的乙醇，并且可任选地冷凝并与进料输入物组合以用于随后的脱水循环。

3. 发明申请

US20070181504A1 Method of Preparing a Composition Using Argentation Chromatography 有权
标题翻译：使用阿根廷色谱法制备组合物的方法
公开(公告)号：US20070181504A1
公开(公告)日：2007-08-09
申请号：US11612250
申请日：2006-12-18
申请人： Thomas Binder , Doug Geier , Ahmad Hilaly , Robert Sandage , John Soper
发明人： Thomas Binder , Doug Geier , Ahmad Hilaly , Robert Sandage , John Soper
IPC分类号： B01D15/08
CPC分类号： B01D15/1828 , B01D15/20 , B01D15/362 , B01J20/0233 , B01J20/284 , B01J20/3234 , B01J20/3236 , B01J47/016 , C07C67/56 , C11B3/10 , G01N30/462 , C07C69/587 , C07C69/58
摘要： The present invention is directed to a method of preparing compositions enriched in compounds containing carbon chains of varying degrees of unsaturation using argentation chromatography. The present method utilizes an argentized cationic resin or a conditioned argentized alumina to separate compounds containing saturated or mono-unsaturated carbon chains from compounds having polyunsaturated carbon chains present in a starting composition. The invention is particularly useful for preparing a composition enriched in polyunsaturated fatty acid alkyl esters from mixtures of fatty acid esters in a starting composition derived from vegetable oils. The present invention is also directed to a method of preparing a conditioned argentized alumina adsorbent having increased selectivity for compounds containing one or more polyunsaturated carbon chains.
摘要翻译：本发明涉及使用梯度色谱法制备富集含有不同不饱和度的碳链的化合物的组合物的方法。本方法利用阳离子阳离子树脂或调节的氧化铝将起始组合物中存在的具有多不饱和碳链的化合物与饱和或单不饱和碳链分开。本发明特别可用于在源自植物油的起始组合物中由脂肪酸酯的混合物制备富含多不饱和脂肪酸烷基酯的组合物。本发明还涉及一种制备具有对含有一个或多个多不饱和碳链的化合物具有增加的选择性的调节的氧化铝吸附剂的方法。

4. 发明申请

US20050245405A1 Method of preparing fatty acid alkyl esters from waste or recycled fatty acid stock 有权
标题翻译：从废物或再循环脂肪酸原料制备脂肪酸烷基酯的方法
公开(公告)号：US20050245405A1
公开(公告)日：2005-11-03
申请号：US11102869
申请日：2005-04-11
申请人： Douglas Geier , Ahmad Hilaly , John Soper
发明人： Douglas Geier , Ahmad Hilaly , John Soper
IPC分类号： C07C69/00 , C10L1/02 , C11B13/02 , C11C1/02 , C11C1/08 , C11C1/10 , C11C3/00 , C10M15/34
CPC分类号： C11C3/003 , C10L1/026 , C11B13/02 , C11C1/02 , C11C1/08 , C11C1/10 , Y02E50/13 , Y02W30/74
摘要： The present invention is directed to a method or preparing fatty acid alkyl esters from fatty acids contained in co-product streams, or waste or recycled fatty acid stock. The present method utilizes an acidic resin to convert the fatty acid stock into esters. The present method encompasses the use of reactive simulated moving bed chromatography, wherein above about 95 percent of the fatty acid stock is converted to fatty acid alkyl esters. The present method has been optimized to separate the ester product from the raffinate stream formed during the chromatographic process, thereby improving the yield of the esterification and preventing acid hydrolysis of the ester.
摘要翻译：本发明涉及由共同产物流中所含脂肪酸或废物或再循环脂肪酸原料制备脂肪酸烷基酯的方法或方法。本方法利用酸性树脂将脂肪酸原料转化成酯。本方法包括使用反应性模拟移动床层析法，其中高于约95％的脂肪酸原料转化为脂肪酸烷基酯。本发明方法已被优化以将酯产物与色谱过程中形成的萃余液流分离，从而提高酯化产率并防止酯的酸水解。

5. 发明授权

US06867308B2 Process for separation of tocopherols 失效
标题翻译：生育酚分离方法
公开(公告)号：US06867308B2
公开(公告)日：2005-03-15
申请号：US10246760
申请日：2002-09-19
申请人： Laslow Bartok , Ahmad Hilaly , Christine M. Schuette , Rishi Shukla
发明人： Laslow Bartok , Ahmad Hilaly , Christine M. Schuette , Rishi Shukla
IPC分类号： C07D311/72
CPC分类号： C07D311/72
摘要： A process for separation of specific tocopherols from a mixture of tocopherols is disclosed. The process includes methods of separation of the tocopherols from residues of vegetable oil refining and other various food sources by dissolving in organic solvents and eluting over non-ionic adsorbent resins.
摘要翻译：公开了从生育酚混合物分离特定生育酚的方法。该方法包括通过溶解在有机溶剂中并通过非离子吸附树脂洗脱，将生育酚与植物油精炼和其它各种食物来源的残留物分离的方法。

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