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1. 发明授权

US6045650A Hydrophilic materials and their method of preparation 失效
标题翻译：亲水材料及其制备方法
公开(公告)号：US6045650A
公开(公告)日：2000-04-04
申请号：US931623
申请日：1997-09-16
申请人： Mark A. Mitchnick , Garry Gwozdz , William A. Hendrickson
发明人： Mark A. Mitchnick , Garry Gwozdz , William A. Hendrickson
IPC分类号： B01J2/00 , C09C3/06 , C09C3/08 , C09C3/12 , B05B31/00
CPC分类号： C09C3/08 , B01J2/006 , C09C3/06 , C09C3/12 , C01P2002/84 , C01P2004/60 , C01P2004/80 , C01P2006/60 , C01P2006/90 , Y10T428/2993
摘要： A process is described for applying a solid coating onto a surface of an article. The surface of an article has a first physical property measurable as a degree of hydrophobicity and/or hydrophilicity. A liquid coating of an oxidizable material containing at least one element other than carbon, hydrogen, oxygen and nitrogen is applied onto the surface of the article. The oxidizable material is oxidized on the surface to attach an oxidized material having said at least one element other than carbon, oxygen, nitrogen and hydrogen onto said surface. This process thereby changes the first physical property with respect to its hydrophobicity and/or hydrophilicity. The process is relatively gentle to the underlying surface, at least in part because of the moderate temperatures which may be used for oxidation, and a wide range of properties may be provided onto the surface by appropriate selection and/or mixing of the liquid material and selection of the surface. The process is particularly useful with particulate materials.
摘要翻译：描述了将固体涂层施加到制品的表面上的方法。制品的表面具有可测量为疏水性和/或亲水性的第一物理性质。将包含至少一种除碳，氢，氧和氮之外的元素的可氧化材料的液体涂层施加到制品的表面上。可氧化材料在表面上被氧化，以将具有除了碳，氧，氮和氢以外的至少一种元素的氧化材料附着到所述表面上。因此，该方法相对于其疏水性和/或亲水性而改变第一物理性质。该方法至少部分地由于可用于氧化的中等温度而相对温和，并且可以通过适当选择和/或混合液体材料和选择表面。该方法对颗粒材料特别有用。

2. 发明授权

US6103267A Stabilized ascorbic acid, composition, and method of use 失效
标题翻译：稳定的抗坏血酸，组合物和使用方法
公开(公告)号：US6103267A
公开(公告)日：2000-08-15
申请号：US122828
申请日：1998-07-27
申请人： Mark A. Mitchnick , Garry Gwozdz
发明人： Mark A. Mitchnick , Garry Gwozdz
IPC分类号： A61K47/06 , A61K47/10 , A61K9/10 , A61K7/00 , A61K31/375
CPC分类号： A61K47/06 , A61K47/10 , A61K9/0014 , Y10S514/88 , Y10S514/937 , Y10S514/938
摘要： A dispersion for carrying at least one water-soluble material or water-dispersible material (especially ascorbic acid, Vitamin C) in a relatively stable form is described, the dispersion comprising an oil phase containing particles comprising water-soluble polymer, water-soluble material or water-dispersible material (ascorbic acid), and water. The dispersion preferably comprises particles which have number average diameter dimensions of less than 2 microns, more preferably less than 1 micron. The dispersion may comprise oil components such as, for example only, a mineral oil, silicone oil, or cosmetic oil. A method of forming a dispersion of solid particles which comprise water-soluble material or water-dispersible material (e.g., ascorbic acid) in a water-soluble polymer may comprise the steps of:a) forming a first solution of the water-soluble material or water-dispersible material (ascorbic acid), water and a water-soluble polymer,b) mixing the first solution with a second solution of a water in a surface active agent having an HLB of less than 12 or less than 10 and oil,c) dispersing the first solution and the second solution to form a mixture of the first solution and second solution, andd) cooling the mixture, solidifying the first solution to form particles dispersed in said oil. This method may have the emulsifying done at a temperature above 40.degree. C., preferably above 50.degree. C., more preferably above 55.degree. C.
摘要翻译：描述了用于以相对稳定的形式携带至少一种水溶性材料或水分散性材料（特别是抗坏血酸，维生素C）的分散体，该分散体包含含有水溶性聚合物，水溶性材料或水分散性材料（抗坏血酸）和水。分散体优选包含具有小于2微米，更优选小于1微米的数均粒径的颗粒。分散体可以包括油组分，例如仅矿物油，硅油或化妆油。在水溶性聚合物中形成包含水溶性材料或水分散性材料（例如抗坏血酸）的固体颗粒分散体的方法可以包括以下步骤：a）形成水溶性材料的第一溶液或水分散性材料（抗坏血酸），水和水溶性聚合物，b）将第一溶液与HLB小于12或小于10的表面活性剂和油的第二溶液混合， c）分散第一溶液和第二溶液以形成第一溶液和第二溶液的混合物，以及d）冷却混合物，固化第一溶液以形成分散在所述油中的颗粒。该方法可以在高于40℃，优选高于50℃，更优选高于55℃的温度下进行乳化。

3. 发明授权

US07419527B2 Increased density particle molding 有权
标题翻译：增加密度颗粒成型
公开(公告)号：US07419527B2
公开(公告)日：2008-09-02
申请号：US10434397
申请日：2003-05-08
申请人： Garry Gwozdz , Mark Mitchnick , David Fairhurst
发明人： Garry Gwozdz , Mark Mitchnick , David Fairhurst
IPC分类号： B22F1/02 , B22F3/00
CPC分类号： B22F1/007 , B22F1/0059 , B22F2998/00 , C04B35/62821 , C04B35/62823 , C04B35/62834
摘要： Novel powders or particles are formed by associating them with relatively small proportions of hydrolysable liquid material. The resulting particle/liquid mass is placed in a mold and sintered under conditions of heat and pressure that enables at least some of the hydrolysable liquid to react within the sintered mass. The sintered mass displays a controllable range of properties such as increased density, increased tensile strength, and improved natural polish finish. The hydrolysable liquid may partially hydrolyze and/or react with the powders and particles, but the liquid is not completely (not 100%) reduced to an inorganic oxide prior to introduction to the mold and performance of the sintering process.
摘要翻译：通过将它们与相对小比例的可水解液体材料缔合而形成新的粉末或颗粒。将所得的颗粒/液体物质置于模具中并在热和压力条件下烧结，使至少一些可水解液体在烧结体内发生反应。烧结体显示出可控范围的特性，例如增加的密度，增加的拉伸强度和改进的天然抛光光洁度。可水解液体可能部分水解和/或与粉末和颗粒反应，但是在引入模具和执行烧结过程之前，液体不会完全（不是100％）还原成无机氧化物。

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