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1. 发明授权

US5176941A Process of producing a ceramic/fiber composite using a molten polysilazone 失效
标题翻译：使用熔融聚硅氧烷制造陶瓷/纤维复合材料的方法
公开(公告)号：US5176941A
公开(公告)日：1993-01-05
申请号：US444032
申请日：1989-11-30
申请人： Marcellus Peuckert , Martin Bruck , Thomas Gerdau , Tilo Vaahs , Hans-Jerg Kleiner , Fritz Aldinger
发明人： Marcellus Peuckert , Martin Bruck , Thomas Gerdau , Tilo Vaahs , Hans-Jerg Kleiner , Fritz Aldinger
IPC分类号： C04B35/589 , C04B35/80 , C04B41/45 , C04B41/50 , C04B41/81 , C04B41/87 , C08G77/62
CPC分类号： C04B41/81 , C04B35/589 , C04B35/806 , C04B41/4554 , C04B41/4584 , C04B41/5066 , C04B41/87 , C08G77/62
摘要： The invention relates to a process for the production of a ceramic/fiber composite.The process comprises impregnating fibers with a molten polysilazane in a first step, converting the polysilazane in the fibers into the infusible state in a second step and, in a third step, heating the impregnated fibers to 800.degree. to 2000.degree. C. in an atmosphere of nitrogen, noble gas, or ammonia.
摘要翻译：本发明涉及一种生产陶瓷/纤维复合材料的方法。该方法包括在第一步骤中用熔融的聚硅氮烷浸渍纤维，在第二步中将纤维中的聚硅氮烷转化为不熔状态，并且在第三步中，将浸渍的纤维在气氛中加热至800℃至2000℃ 的氮气，惰性气体或氨气。

2. 发明授权

US5081078A Sinterable ceramic powder, process for its preparation, silicon nitride ceramic manufactured therefrom, process for its manufacture and its use 失效
标题翻译：可烧结陶瓷粉末，其制备方法，其制造的硅酸盐陶瓷，其制造方法及其用途
公开(公告)号：US5081078A
公开(公告)日：1992-01-14
申请号：US443881
申请日：1989-11-30
申请人： Marcellus Peuckert , Martin Bruck , Thomas Gerdau , Hans-Jerg Kleiner , Tilo Vaahs , Fritz Aldinger
发明人： Marcellus Peuckert , Martin Bruck , Thomas Gerdau , Hans-Jerg Kleiner , Tilo Vaahs , Fritz Aldinger
IPC分类号： C01B21/068 , C04B35/589 , C04B35/593 , C08G77/48 , C08G77/62
CPC分类号： C04B35/589 , C04B35/5935
摘要： The invention relates to a novel sinterable ceramic powder, to its preparation, to its processing to form silicon nitride ceramic and to said material itself and its use. The sinterable ceramic powder is prepared by dissolving the polysilazane of formula (I)[CH.sub.3 SiHNH].sub.n [CH.sub.3 SiN].sub.nwhere n is about 10 to 12, in an organic solvent, suspending a pulverulent sinter aid in this solution and then evaporating the solvent and pyrolyzing the residue in an inert gas atmosphere at 500.degree. to 1600.degree. C.The resulting ceramic powder can be used to form a shaped article and then to manufacture silicon nitride ceramic by sintering. It is also possible, however, to form a shaped article from the as yet unpyrolyzed residue obtained after evaporation of the solvent, and then to pyrolyze and sinter said article.The ceramic obtained can be used to manufacture components subject to high mechanical, thermal and corrosive stress.
摘要翻译：本发明涉及一种新型的可烧结陶瓷粉末，用于其制备，以形成氮化硅陶瓷的加工以及所述材料本身及其用途。可烧结陶瓷粉末是通过在有机溶剂中溶解式（I）[CH3SiHNH] n [CH3SiN] n的聚硅氮烷[N，N-二甲基甲酰胺] n [CH3SiN] n，其中n为约10〜12，将粉状烧结助剂悬浮在该溶液中，然后蒸发溶剂，在惰性气体气氛中在500〜1600℃下热解残渣。得到的陶瓷粉末可用于形成成形制品，然后通过烧结制造氮化硅陶瓷。然而，也可以从蒸发溶剂后获得的仍然未裂解的残余物形成成型制品，然后热解并烧结所述制品。获得的陶瓷可用于制造受到高机械，热和腐蚀应力的部件。

3. 发明授权

US5189132A Polymeric hydridochlorosilazanes, process for their preparation, ceramic materials containing silicon nitride which can be manufactured therefrom, and their manufacture 失效
标题翻译：聚合氢氯硅氮烷，其制备方法，可由其制造的含氮化硅的陶瓷材料及其制造方法
公开(公告)号：US5189132A
公开(公告)日：1993-02-23
申请号：US759035
申请日：1991-09-05
申请人： Tilo Vaahs , Thomas Gerdau , Hans-Jerg Kleiner , Marcellus Peuckert , Martin Bruck
发明人： Tilo Vaahs , Thomas Gerdau , Hans-Jerg Kleiner , Marcellus Peuckert , Martin Bruck
IPC分类号： C04B35/589 , C08G77/62
CPC分类号： C04B35/589 , C08G77/62
摘要： The invention relates to novel polymeric hydridochlorosilazanes, to their preparation, to their processing to form ceramic materials containing silicon nitride, and to said materials themselves. The polymeric hydridochlorosilazanes are prepared by reacting oligohydridoorganosilazanes of the general formula (R.sup.1 SiHNH).sub.n, in which n is about 3 to about 12, with at least one of the chlorosilanes R.sup.2 SiHCl.sub.2, R.sup.3 SiCl.sub.3, Cl.sub.2 R.sup.4 Si--CH.sub.2 CH.sub.2 --SiR.sup.4 Cl.sub.2 or Cl.sub.3 Si--CH.sub.2 CH.sub.2 --SiR.sup.5 Cl.sub.2 at 30.degree. C. to 300.degree. C., where the radicals independently of one another have the following meanings:R.sup.1 =a C.sub.1 -C.sub.6 alkyl or C.sub.2 -C.sub.6 alkenyl group,R.sup.2 =a C.sub.2 -C.sub.6 alkenyl group if R.sup.2 SiHCl.sub.2 is reacted with the oligosilazanes by itself, orR.sup.2 =a C.sub.1 -C.sub.6 alkyl or C.sub.2 -C.sub.6 alkenyl group if R.sup.2 SiHCl.sub.2 is reacted with the oligosilazanes as a mixture with other chlorosilanes, andR.sup.3, R.sup.4, R.sup.5 =a C.sub.1 -C.sub.6 alkyl or C.sub.C.sub.2 -C.sub.6 alkenyl group,and where R.sup.3 SiCl.sub.3 is used only as a mixture with at least one of the other chlorosilanes (containing R.sup.2, R.sup.4 or R.sup.5).The polymeric hydridochlorosilazanes according to the invention can be converted into polysilazanes by reaction with ammonia, and these in turn can be pyrolyzed to form ceramic materials containing silicon nitride.
摘要翻译：本发明涉及新型的聚合氯化二氯硅氮烷，用于其制备，以形成含有氮化硅的陶瓷材料的加工，以及所述材料本身。通过使通式（R1SiHNH）n的低聚氢化有机硅氮烷（其中n为约3至约12）与至少一种氯代硅烷R 2 SiHCl 2，R 3 SiCl 3，Cl 2 R 4 Si-CH 2 CH 2 -SiR 4 Cl 2或Cl 3 Si-CH 2 CH 2 -SiR 5 Cl 2中的至少一种反应来制备聚合的氢氯硅氮烷， 30℃至300℃，其中彼此独立的基团具有以下含义：R 1 = C 1 -C 6烷基或C 2 -C 6烯基，如果R 2 SiHCl 2与C 2 -C 6烯基反应，则R 2 = C 2 -C 6烯基如果R2SiHCl2与低聚硅氮烷作为与其它氯硅烷的混合物反应，则R2 = C1-C6烷基或C2-C6烯基，R3，R4，R5 = C1-C6烷基或CC2-C6烯基，并且其中R 3 SiCl 3仅与至少一种其它氯硅烷（包含R 2，R 4或R 5）一起使用。根据本发明的聚合物氯化硅烷可以通过与氨的反应转化为聚硅氮烷，并且这些可以热解而形成含有氮化硅的陶瓷材料。

4. 发明授权

US5075266A Process for the production of ceramic material containing silicon nitride from polymeric hydridochlorosilazanes 失效
标题翻译：从聚合氯化石蜡生产含有硝酸硅的陶瓷材料的工艺
公开(公告)号：US5075266A
公开(公告)日：1991-12-24
申请号：US381501
申请日：1989-07-18
申请人： Thomas Gerdau , Hans-Jerg Kleiner , Martin Bruck , Marcellus Peuckert , Fritz Aldinger
发明人： Thomas Gerdau , Hans-Jerg Kleiner , Martin Bruck , Marcellus Peuckert , Fritz Aldinger
IPC分类号： C01B21/068 , C04B35/589 , C08G77/48 , C08G77/62 , C08L83/16 , D01F9/10
CPC分类号： C08L83/16 , C04B35/589
摘要： The invention relates to a process for the production of ceramic material containing silicon nitride, such as fibers, coatings or moldings. In this process, polymeric hydridochlorosilazanes are rendered infusible at a temperature below their softening point by treatment with gaseous NH.sub.3 and are then pyrolyzed in an atmosphere containing NH.sub.3 at 700.degree. to 1500.degree. C. Fibers, coatings or moldings containing silicon nitride are produced by first producing appropriate structures from a melt of the polymeric hydridochlorosilazane and then rendering them infusible and pyrolyzing them.
摘要翻译：本发明涉及生产含有氮化硅的陶瓷材料的方法，例如纤维，涂层或模制品。在此过程中，聚合氯化硅烷可以通过用气态NH 3处理而在低于其软化点的温度下熔化，然后在含有氮气的气氛中在700°至1500°C下热解。含有氮化硅的纤维，涂层或模制品首先通过从聚合氯代硅氮烷的熔体中产生适当的结构，然后使它们不熔融并热解。

5. 发明授权

US5066623A Polymeric hydridosilazanes and processes for their preparation, and their use 失效
标题翻译：聚合氢氧化物及其制备方法及其使用
公开(公告)号：US5066623A
公开(公告)日：1991-11-19
申请号：US491534
申请日：1990-03-12
申请人： Thomas Gerdau , Hans-Jerg Kleiner , Marcellus Peuckert , Martin Bruck , Fritz Aldinger
发明人： Thomas Gerdau , Hans-Jerg Kleiner , Marcellus Peuckert , Martin Bruck , Fritz Aldinger
IPC分类号： C04B35/589 , C08G77/48 , C08G77/62
CPC分类号： C04B35/589 , C08G77/62
摘要： The invention relates to novel polymeric hydridosilazanes, processes for their preparation and their use for the preparation of ceramic material containing silicon nitride. To prepare the polymeric hydridosilazanes, polymeric hydridochlorosilazanes are reacted with NH.sub.3. To prepare the ceramic material containing silicon nitride, the polymeric hydridosilazanes are then pyrolyzed.

6. 发明授权

US5008423A Polymeric hydridochlorosilazanes and processes for their preparation 失效
标题翻译：聚合氯乙基硅氮烷及其制备方法
公开(公告)号：US5008423A
公开(公告)日：1991-04-16
申请号：US248547
申请日：1988-09-22
申请人： Thomas Gerdau , Hans-Jerg Kleiner , Marcellus Peuckert , Martin Bruck , Fritz Aldinger
发明人： Thomas Gerdau , Hans-Jerg Kleiner , Marcellus Peuckert , Martin Bruck , Fritz Aldinger
IPC分类号： C04B35/589 , C07F7/10 , C08G77/48 , C08G77/62
CPC分类号： C07F7/10 , C04B35/589 , C08G77/62
摘要： The invention relates to novel polymeric hydridochlorosilazanes and a process for their preparation. The compounds according to the invention can be converted into polyhydridosilaznes by reaction with ammonia, and these can in turn be pyrolyzed to ceramic material containing silicon nitride. To prepare the polymeric hydridochlorosilazanes, oligohydridoalkylsilazanes (R.sup.1 SiHNH).sub.n are reacted with a dichlorohydridoalkylsilane R.sup.2 SiHCl.sub.2.
摘要翻译：本发明涉及新颖的聚合氯乙硅氮烷及其制备方法。根据本发明的化合物可以通过与氨的反应转化为多羟基硅氮烷，并且它们又可以热解成含有氮化硅的陶瓷材料。为了制备聚合氯化硅烷，将低聚氢化烷基硅氮烷（R1SiHNH）n与二氯代氢化烷基硅烷R2SiHCl2反应。

7. 发明授权

US4931513A Polymeric hydridosilazanes and processes for their preparation and their use 失效
标题翻译：聚合氢硅氮烷及其制备方法及其应用
公开(公告)号：US4931513A
公开(公告)日：1990-06-05
申请号：US247933
申请日：1988-09-22
申请人： Thomas Gerdau , Hans-Jerg Kleiner , Marcellus Peuckert , Martin Bruck , Fritz Aldinger
发明人： Thomas Gerdau , Hans-Jerg Kleiner , Marcellus Peuckert , Martin Bruck , Fritz Aldinger
IPC分类号： C04B35/589 , C08G77/48 , C08G77/62
CPC分类号： C04B35/589 , C08G77/62
摘要： The invention relates to novel polymeric hydridosilazanes, processes for their preparation and their use for the preparation of ceramic material containing silicon nitride. To prepare the polymeric hydridosilazanes, polymeric hydridochlorosilazanes are reacted with NH.sub.3. To prepare the ceramic material containing silicon nitride, the polymeric hydridosilazanes are then pyrolyzed.
摘要翻译：本发明涉及新的聚合物硅藻土，其制备方法及其用于制备含有氮化硅的陶瓷材料的用途。为了制备聚合的羟基硅氮烷，聚合的氯代硅氮烷与NH 3反应。为了制备含有氮化硅的陶瓷材料，聚合物氢硅氮烷然后被热解。

8. 发明授权

US5081080A Polymeric hydridosilazanes, processes for the preparation thereof, silicon nitride-containing ceramic materials which can be prepared therefrom, and the preparation thereof 失效
标题翻译：聚合氢硅氮烷，其制备方法，可由其制备的含氮化硅的陶瓷材料及其制备方法
公开(公告)号：US5081080A
公开(公告)日：1992-01-14
申请号：US512732
申请日：1990-04-20
申请人： Tilo Vaahs , Thomas Gerdau , Marcellus Peuckert , Martin Bruck
发明人： Tilo Vaahs , Thomas Gerdau , Marcellus Peuckert , Martin Bruck
IPC分类号： C04B35/589 , C08G77/62
CPC分类号： C08G77/62 , C04B35/589
摘要： The invention relates to novel polymeric hydridosilazanes, their preparation, their conversion into silicon nitride-containing ceramic material, and this material itself. To prepare the polymeric hydridosilazanes, polymeric hydridothiosilazanes are reacted with NH.sub.3. To prepare the silicon nitride-containing ceramic material, the polymeric hydridosilazanes are then pyrolyzed.
摘要翻译：本发明涉及新颖的聚合物硅藻土，其制备方法，其转化为含氮化硅的陶瓷材料，以及该材料本身。为了制备聚合物硅藻土，聚合的硫代氨基硅烷与NH 3反应。为了制备含氮化硅的陶瓷材料，聚合物氢硅氮烷然后被热解。

9. 发明授权

US4939225A Polymeric hydridosilazanes, processes for the preparation thereof, silicon nitride-containing ceramic materials which can be prepared therefrom, and the preparation thereof 失效
标题翻译：聚合氢硅氮烷，其制备方法，可由其制备的含氮化硅的陶瓷材料及其制备方法
公开(公告)号：US4939225A
公开(公告)日：1990-07-03
申请号：US289901
申请日：1988-12-23
申请人： Tilo Vaahs , Thomas Gerdau , Marcellus Peuckert , Martin Bruck
发明人： Tilo Vaahs , Thomas Gerdau , Marcellus Peuckert , Martin Bruck
IPC分类号： C04B35/589 , C08G77/48 , C08G77/62 , D01F9/10
CPC分类号： C08G77/62 , C04B35/589
摘要： Polymeric hydridosilazanes, processes for the preparation thereof, silicon nitride-containing ceramic materials which can be prepared therefrom, and the preparation thereof.The invention relates to novel polymeric hydridosilazanes, their preparation, their conversion into silicon nitride-containing ceramic material, and this material itself. To prepare the polymeric hydridosilazanes, polymeric hydridothiosilazanes are reacted with NH.sub.3. To prepare the silicon nitride-containing ceramic material, the polymeric hydridosilazanes are then pyrolyzed.
摘要翻译：聚合氢硅氮烷，其制备方法，可由其制备的含氮化硅的陶瓷材料及其制备方法。本发明涉及新颖的聚合物硅藻土，其制备方法，其转化为含氮化硅的陶瓷材料，以及该材料本身。为了制备聚合物硅藻土，聚合的硫代氨基硅烷与NH 3反应。为了制备含氮化硅的陶瓷材料，聚合物氢硅氮烷然后被热解。

10. 发明授权

US4859795A Ethylenically unsaturated phosphinic acid and thiophosphinic acid isocyanates and isothiocyanates, and a process for their preparation 失效
标题翻译：烯键式不饱和次膦酸和硫代次膦酸异氰酸酯和异硫氰酸酯及其制备方法
公开(公告)号：US4859795A
公开(公告)日：1989-08-22
申请号：US047102
申请日：1987-05-08
申请人： Thomas Gerdau , Hans-Jerg Kleiner , Georg Pawlowski
发明人： Thomas Gerdau , Hans-Jerg Kleiner , Georg Pawlowski
IPC分类号： C07F9/02 , C07F9/22 , C07F9/36 , C08F30/02
CPC分类号： C07F9/36
摘要： Compounds of the general formula ##STR1## wherein X and Y are the same or different and denote oxygen or sulfur,R.sub.1 is an ethylenically unsaturated aliphatic radical containing from 2 to 6 carbon atoms, andR.sub.2 is a saturated aliphatic radical containing from 1 to 6 carbon atoms or an aryl radical containing from 6 to 10 carbon atoms,are intermediate products used for the preparation of photocrosslinkable polymers with lateral (thio)phosphinyl(thio)urethane groups or (thio)phosphinyl(thio)urea groups, which polymers are useful in photosensitive mixtures and recording material.
摘要翻译：通式（I）的化合物，其中X和Y相同或不同，表示氧或硫，R 1是含有2-6个碳原子的烯属不饱和脂族基团，R 2是含有 1至6个碳原子或含有6至10个碳原子的芳基是用于制备具有侧面（硫代）氧膦基（硫代）氨基甲酸酯基或（硫代）氧膦基（硫））脲基的光可交联聚合物的中间产物，其中聚合物可用于光敏混合物和记录材料。

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