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1. 发明授权

US5585190A Methods for making thin metal matrix composite bodies and articles produced thereby 失效
标题翻译：制造薄金属基复合体及其制品的方法
公开(公告)号：US5585190A
公开(公告)日：1996-12-17
申请号：US186194
申请日：1994-01-24
申请人： Marc S. Newkirk , Michael K. Aghajanian , Gregory E. Hannon , Allyn L. McCormick , Gerhard H. Schiroky , Michael A. Rocazella , Robert C. Kantner
发明人： Marc S. Newkirk , Michael K. Aghajanian , Gregory E. Hannon , Allyn L. McCormick , Gerhard H. Schiroky , Michael A. Rocazella , Robert C. Kantner
IPC分类号： C22C47/08 , C04B41/51 , C04B41/88 , C22C1/10 , C22C47/20 , C22C29/16
CPC分类号： C04B41/009 , C04B41/5155 , C04B41/88 , C22C1/1036 , B22F2003/1014 , C04B2111/00931 , C22C2001/1063 , Y10T428/30
摘要： The present invention relates to a novel process for forming thin metal matrix composite bodies. Particularly, an infiltration enhancer and/or an infiltrating atmosphere are in communication with a filler material or preform, at least at some point during the process, which permits molten matrix metal to spontaneously infiltrate the filler material or preform. Such spontaneous infiltration occurs without the application of any pressure or vacuum. In an embodiment of the present invention, the filler material may be sprayed upon a thin sheet of matrix metal. Alternatively, the filler material may be shaped via tape casting, slip casting, etc. to provide a thin preform. In another embodiment of the present invention, a body of matrix metal may be coated with a filler material such that upon spontaneous infiltration a metal matrix composite body is produced which inversely replicates the configuration of the original body of matrix metal. In yet another embodiment of the present invention, a plurality of thin tape cast preforms which are segregated by a barrier material (e.g., graphite foil) may be infiltrated with a matrix metal during a single spontaneous infiltration process.
摘要翻译：本发明涉及一种形成薄金属基复合体的新方法。特别地，渗透增强剂和/或渗透气氛至少在该过程中的某一点处与填料或预型体连通，这允许熔融基质金属自发地渗入填料或预型体。这种自发渗透发生在没有施加任何压力或真空的情况下。在本发明的一个实施例中，填充材料可以喷涂在基体金属薄片上。或者，填充材料可以通过带铸造，滑移浇铸等形成，以提供薄的预成型件。在本发明的另一个实施例中，基体金属体可以用填充材料涂覆，使得当自发渗透时，产生金属基体复合体，其反向地复制基体金属原体的构型。在本发明的另一个实施方案中，在单次自发渗透过程中，通过阻挡材料（例如，石墨箔）隔离的多个薄带铸造预制件可以用基质金属渗透。

2. 发明授权

US5529108A Thin metal matrix composites and production methods 失效
标题翻译：薄金属基复合材料及其制备方法
公开(公告)号：US5529108A
公开(公告)日：1996-06-25
申请号：US971849
申请日：1993-01-08
申请人： Marc S. Newkirk , Michael K. Aghajanian , Gregory E. Hannon , Allyn L. McCormick , Gerhard H. Schiroky , Michael A. Rocazella , Robert C. Kantner
发明人： Marc S. Newkirk , Michael K. Aghajanian , Gregory E. Hannon , Allyn L. McCormick , Gerhard H. Schiroky , Michael A. Rocazella , Robert C. Kantner
IPC分类号： C22C47/08 , C04B41/51 , C04B41/88 , C22C1/10 , C22C47/20 , B22D19/14 , B22D19/02
CPC分类号： C04B41/009 , C04B41/5155 , C04B41/88 , C22C1/1036 , B22F2003/1014 , C04B2111/00931 , C22C2001/1063 , Y10T428/30
摘要： The present invention relates to a novel process for forming thin metal matrix composite bodies. Particularly, an infiltration enhancer and/or an infiltrating atmosphere are in communication with a filler material or preform, at least, at some point during the process, which permits molten matrix metal to spontaneously infiltrate the filler material or preform. Such spontaneous infiltration occurs without the application of any pressure or vacuum. In an embodiment of the present invention, the filler material may be sprayed upon a thin sheet of matrix metal. Alternatively, the filler material may be shaped via tape casting, slip casting, etc. to provide a thin preform. In another embodiment of the present invention, a body of matrix metal may be coated with a filler material such that upon spontaneous infiltration a metal matrix composite body is produced which inversely replicates the configuration of the original body of matrix metal.
摘要翻译： PCT No.PCT / US91 / 03114 Sec。 371日期：1993年1月8日 102（e）日期1993年1月8日PCT 1991年5月9日PCT PCT。出版物WO91 / 17280 日本1991年11月14日。本发明涉及一种形成薄金属基复合体的新方法。特别地，渗透增强剂和/或渗透气氛至少在该过程中的某一点处与填料或预型体连通，这允许熔融基质金属自发地渗入填料或预型体。这种自发渗透发生在没有施加任何压力或真空的情况下。在本发明的一个实施例中，填充材料可以喷涂在基体金属薄片上。或者，填充材料可以通过带铸造，滑移浇铸等形成，以提供薄的预成型件。在本发明的另一个实施例中，基体金属体可以用填充材料涂覆，使得当自发渗透时，产生金属基体复合体，其反向地复制基体金属原体的构型。

3. 发明授权

US5280819A Methods for making thin metal matrix composite bodies and articles produced thereby 失效
标题翻译：制造薄金属基复合体及其制品的方法
公开(公告)号：US5280819A
公开(公告)日：1994-01-25
申请号：US841902
申请日：1992-02-25
申请人： Marc S. Newkirk , Michael K. Aghajanian , Gregory E. Hannon , Allyn L. McCormick , Gerhard H. Schiroky , Michael A. Rocazella , Robert C. Kantner
发明人： Marc S. Newkirk , Michael K. Aghajanian , Gregory E. Hannon , Allyn L. McCormick , Gerhard H. Schiroky , Michael A. Rocazella , Robert C. Kantner
IPC分类号： C22C47/08 , C04B41/51 , C04B41/88 , C22C1/10 , C22C47/20 , B22D19/02
CPC分类号： C04B41/009 , C04B41/5155 , C04B41/88 , C22C1/1036 , B22F2003/1014 , C04B2111/00931 , C22C2001/1063 , Y10T428/30
摘要： The present invention relates to a novel process for forming a plurality of thin metal matrix composite bodies. Particularly, an infiltration enhancer and/or an infiltrating atmosphere are in communication with a filler material or preform, at least at some point during the process, which permits molten matrix metal to spontaneously infiltrate the plurality of filler materials or preforms. Such spontaneous infiltration occurs without the application of any pressure or vacuum and occurs in a single step. In an embodiment of the present invention, the filler material may be sprayed upon a thin sheet of matrix metal. Alternatively, the filler material may be shaped via tape casting, slip casting, etc. to provide a thin preform. In another embodiment of the present invention, a body of matrix metal may be coated with a filler material such that upon spontaneous infiltration a metal matrix composite body is produced which inversely replicates the configuration of the original body of matrix metal.
摘要翻译：本发明涉及一种用于形成多个薄金属基复合体的新方法。特别地，渗透增强剂和/或渗透气氛至少在该过程中的某一点处与填料或预型体连通，这允许熔融基质金属自发地渗入多种填料或预型体。这种自发渗透在没有施加任何压力或真空的情况下发生并且发生在单个步骤中。在本发明的一个实施例中，填充材料可以喷涂在基体金属薄片上。或者，填充材料可以通过带铸造，滑移浇铸等形成，以提供薄的预成型件。在本发明的另一个实施例中，基体金属体可以用填充材料涂覆，使得当自发渗透时，产生金属基体复合体，其反向地复制基体金属原体的构型。

4. 发明授权

US5633213A Method for in situ tailoring the component of ceramic articles 失效
标题翻译：原位裁剪陶瓷制品成分的方法
公开(公告)号：US5633213A
公开(公告)日：1997-05-27
申请号：US356335
申请日：1995-02-21
申请人： Michael K. Aghajanian , Marc S. Newkirk , Christopher R. Kennedy , Robert C. Kantner , Michael A. Rocazella , Jerry G. Weinstein , Danny R. White , Gerhard H. Schiroky , William B. Johnson
发明人： Michael K. Aghajanian , Marc S. Newkirk , Christopher R. Kennedy , Robert C. Kantner , Michael A. Rocazella , Jerry G. Weinstein , Danny R. White , Gerhard H. Schiroky , William B. Johnson
IPC分类号： C04B35/65
CPC分类号： C04B35/652
摘要： There is disclosed a method for producing a self-supporting ceramic body by oxidation of a molten precursor metal with a vapor-phase oxidant to form an oxidation reaction product and inducing a molten flux comprising said molten precursor metal through said oxidation reaction product. A second metal is incorporated into said molten flux during the oxidation reaction. The resulting ceramic body includes sufficient second metal such that one or more properties of said ceramic body are at least partially affected by the presence and properties of said second metal in the metallic constituent.
摘要翻译： PCT No.PCT / US93 / 06064 Sec。 371日期1995年2月21日 102（e）日期1995年2月21日PCT提交1993年6月25日PCT公布。第WO94 / 00399号公报日本1994年1月6日公开了一种通过用气相氧化剂氧化熔融前体金属来生产自支撑陶瓷体的方法，以形成氧化反应产物，并通过所述氧化物诱导包含所述熔融前体金属的熔融焊剂反应产物。在氧化反应期间将第二金属并入所述熔融焊剂中。所得到的陶瓷体包括足够的第二金属，使得所述陶瓷体的一个或多个特性至少部分地受到金属成分中所述第二金属的存在和性质的影响。

5. 发明授权

US5268339A Method for in situ tailoring the component of ceramic articles 失效
标题翻译：原位裁剪陶瓷制品成分的方法
公开(公告)号：US5268339A
公开(公告)日：1993-12-07
申请号：US904739
申请日：1992-06-26
申请人： Michael K. Aghajanian , Marc S. Newkirk , Christopher R. Kennedy , Robert C. Kantner , Michael A. Rocazella , Jerry G. Weinstein , Danny R. White
发明人： Michael K. Aghajanian , Marc S. Newkirk , Christopher R. Kennedy , Robert C. Kantner , Michael A. Rocazella , Jerry G. Weinstein , Danny R. White
IPC分类号： C04B35/65
CPC分类号： C04B35/652
摘要： There is disclosed a method for producing a self-supporting ceramic body by oxidation of a molten precursor metal with a vapor-phase oxidant to form an oxidation reaction product and inducing a molten flux comprising said molten precursor metal through said oxidation reaction product. A second metal is incorporated into said molten flux during the oxidation reaction. The resulting ceramic body includes sufficient second metal such that one or more properties of said ceramic body are at least partially affected by the presence and properties of said second metal in the metallic constituent.
摘要翻译：公开了一种通过用气相氧化剂氧化熔融前体金属以形成氧化反应产物并通过所述氧化反应产物诱导包含所述熔融前体金属的熔融焊剂来生产自支撑陶瓷体的方法。在氧化反应期间将第二金属并入所述熔融焊剂中。所得到的陶瓷体包括足够的第二金属，使得所述陶瓷体的一个或多个特性至少部分地受到金属成分中所述第二金属的存在和性质的影响。

6. 发明授权

US5163499A Method of forming electronic packages 失效
标题翻译：电子封装形成方法
公开(公告)号：US5163499A
公开(公告)日：1992-11-17
申请号：US520936
申请日：1990-05-09
申请人： Marc S. Newkirk , Danny R. White , Christopher R. Kennedy , Alan S. Nagelberg , Michael K. Aghajanian , Robert J. Wiener , Steven D. Keck , John T. Burke , Peter M. Engelgau , Cheng-Tsin Lee , Michael A. Rocazella
发明人： Marc S. Newkirk , Danny R. White , Christopher R. Kennedy , Alan S. Nagelberg , Michael K. Aghajanian , Robert J. Wiener , Steven D. Keck , John T. Burke , Peter M. Engelgau , Cheng-Tsin Lee , Michael A. Rocazella
IPC分类号： H01L23/02 , C04B35/65 , C04B37/02 , C22C1/10 , H01L21/48 , H01L23/14 , H01L23/373
CPC分类号： C04B35/652 , C22C1/1015 , C22C1/1036 , C22C47/06 , H01L21/4803 , H01L23/14 , H01L23/3733 , C22C2001/1063 , H01L2924/0002
摘要： The present invention relates to the formation of a macrocomposite body by spontaneously infiltrating a permeable mass of filler material or a preform with molten matrix metal and bonding the spontaneously infiltrated material to at least one second material such as a ceramic or ceramic containing body and/or a metal or metal containing body. Particularly, an infiltration enhancer and/or infiltration enhancer precursor and/or infiltrating atmosphere are in communication with a filler material or a preform, at least at some point during the process, which permits molten matrix metal to spontaneously infiltrate the filler material or preform. Moreover, prior to infiltration, the filler material or preform is placed into contact with at least a portion of a second material such that after infiltration of the filler material or preform, the infiltrated material is bonded to the second material, thereby forming a sealable electronic package.
摘要翻译：本发明涉及通过自发渗透填充材料的可渗透物质或具有熔融基质金属的预成型体并将自发渗透的材料结合到至少一种第二材料如陶瓷或含陶瓷的体和/或含金属或金属的物体。特别地，渗透增强剂和/或渗透增强剂前体和/或渗透气氛至少在该过程中的某一点处与填料或预型体连通，这允许熔融基质金属自发地渗入填料或预型体。此外，在渗透之前，将填料或预型体放置成与第二材料的至少一部分接触，使得在填充材料或预型体渗透之后，渗透的材料结合到第二材料，从而形成可密封的电子包。

7. 发明授权

US5618635A Macrocomposite bodies 失效
标题翻译：大复合体
公开(公告)号：US5618635A
公开(公告)日：1997-04-08
申请号：US411055
申请日：1995-03-27
申请人： Marc S. Newkirk , Danny R. White , Christopher R. Kennedy , Alan S. Nagelberg , Michael K. Aghajanian , Robert J. Wiener
发明人： Marc S. Newkirk , Danny R. White , Christopher R. Kennedy , Alan S. Nagelberg , Michael K. Aghajanian , Robert J. Wiener
IPC分类号： B22D19/14 , C22C1/10 , C22C21/00 , C22C47/08 , C22C1/09
CPC分类号： C22C1/1015 , C22C1/1036 , C22C47/06 , C22C2001/1063 , Y10T428/12007 , Y10T428/12486
摘要： The present invention relates to the formation of a macrocomposite body by spontaneously infiltrating a permeable mass of filler material or a preform with molten matrix metal and bonding the spontaneously infiltrated material to at least one second material such as a ceramic or ceramic containing body and/or a metal or metal containing body. Particularly, an infiltration enhancer and/or infiltration enhancer precursor and/or infiltrating atmosphere are in communication with a filler material or a preform, at least at some point during the process, which permits molten matrix metal to spontaneously infiltrate the filler material or preform. Moreover, prior to infiltration, the filler material or preform is placed into contact with at least a portion of a second material such that after infiltation of the filler material or preform, the infiltrated material is bonded to the second material, thereby forming a macrocomposite body.
摘要翻译：本发明涉及通过自发渗透填充材料的可渗透物质或具有熔融基质金属的预成型体并将自发渗透的材料结合到至少一种第二材料如陶瓷或含陶瓷的体和/或含金属或金属的物体。特别地，渗透增强剂和/或渗透增强剂前体和/或渗透气氛至少在该过程中的某一点处与填料或预型体连通，这允许熔融基质金属自发地渗入填料或预型体。此外，在渗透之前，将填料或预型体放置成与第二材料的至少一部分接触，使得在渗入填料或预型体之后，渗透的材料结合到第二材料，由此形成大复合体。

8. 发明授权

US5541004A Metal matrix composite bodies utilizing a crushed polycrystalline oxidation reaction product as a filler 失效
标题翻译：使用破碎的多晶氧化反应产物作为填料的金属基质复合体
公开(公告)号：US5541004A
公开(公告)日：1996-07-30
申请号：US303567
申请日：1994-09-09
申请人： Marc S. Newkirk , Michael K. Aghajanian
发明人： Marc S. Newkirk , Michael K. Aghajanian
IPC分类号： B22D19/14 , C22C1/10 , C22C21/00 , C22C47/08 , C22C1/09
CPC分类号： C22C1/1036 , C22C2001/1057 , C22C2001/1063 , Y10T428/12007 , Y10T428/12486
摘要： The present invention relates to a novel method for forming metal matrix composite bodies and novel metal matrix composite bodies produced thereby. Particularly, a polycrystalline oxidation reaction product of a parent metal and an oxidant is first formed. The polycrystalline oxidation reaction product is thereafter comminuted into an appropriately sized filler material which can be placed into a suitable container or formed into a preform. The filler material or preform of comminuted polycrystalline oxidation reaction product is thereafter placed into contact with a matrix metal alloy in the presence of an infiltration enhancer, and/or an infiltration enhancer precursor and/or an infiltrating atmosphere, at least at some point during the process, whereupon the matrix metal alloy spontaneously infiltrates the filler material or preform. As a result of utilizing comminuted or crushed polycrystalline oxidation reaction product, enhanced infiltration (e.g., enhanced rate or amount) is achieved. Moreover, novel metal matrix composite bodies are produced.
摘要翻译：本发明涉及一种形成金属基复合体的新颖方法和由其制造的新型金属基复合体。特别地，首先形成母体金属和氧化剂的多晶氧化反应产物。然后将多晶氧化反应产物粉碎成适当尺寸的填充材料，其可以放置在合适的容器中或形成预成型体。此后，在渗透增强剂和/或渗透增强剂前体和/或渗透气氛的存在下，将粉末状多晶氧化反应产物的填料或预成型体置于基质金属合金中，至少在因此基体金属合金自发地渗入填料或预成型体。作为利用粉碎或破碎的多晶氧化反应产物的结果，实现了增强的渗透（例如增强的速率或量）。此外，还生产出新颖的金属基复合体。

9. 发明授权

US5518061A Method of modifying the properties of a metal matrix composite body 失效
标题翻译：改性金属基复合体的性能的方法
公开(公告)号：US5518061A
公开(公告)日：1996-05-21
申请号：US199413
申请日：1994-02-22
申请人： Marc S. Newkirk , Andrew W. Urquhart , Michael K. Aghajanian , Mark G. Mortenson , Vilupanur A. Ravi , Alan S. Nagelberg
发明人： Marc S. Newkirk , Andrew W. Urquhart , Michael K. Aghajanian , Mark G. Mortenson , Vilupanur A. Ravi , Alan S. Nagelberg
IPC分类号： C04B41/52 , C04B41/89 , C22C1/10 , B22D19/14 , B22D19/00
CPC分类号： C04B41/89 , C04B41/52 , C22C1/1036 , C22C2001/1057 , C22C2001/1063
摘要： The present invention relates to modifying the properties of a metal matrix composite body by a post formation process treatment and/or a substantially contiguous modification treatment. The post formation process treatment may be applicable to a variety of metal matrix composite bodies produced by various techniques, and is particularly applicable to modifying the properties of a metal matrix composite body produced by a spontaneous infiltration technique. The substantially contiguous modification process may also be used primarily in conjunction with metal matrix composite bodies produced according to a spontaneous infiltration technique. Particularly, at least a portion of the matrix metal of the metal matrix composite body and/or the filler material of the metal matrix composite body is modified or altered during and/or after the formation process.
摘要翻译：本发明涉及通过后形成工艺处理和/或基本相邻的改性处理来改性金属基质复合体的性质。后形成处理可以适用于通过各种技术制造的各种金属基复合体，特别适用于通过自发渗透技术制造的金属基复合体的特性。基本相邻的改性方法也可以主要与根据自发渗透技术制备的金属基质复合体一起使用。特别地，金属基体复合体的基质金属和/或金属基体复合体的填充材料的至少一部分在形成过程中和/或之后被修饰或改变。

10. 发明授权

US5301738A Method of modifying the properties of a metal matrix composite body 失效
标题翻译：改性金属基复合体的性能的方法
公开(公告)号：US5301738A
公开(公告)日：1994-04-12
申请号：US841241
申请日：1992-02-24
申请人： Marc S. Newkirk , Andrew W. Urquhart , Michael K. Aghajanian , Mark G. Mortenson , Vilupanur A. Ravi , Alan S. Nagelberg
发明人： Marc S. Newkirk , Andrew W. Urquhart , Michael K. Aghajanian , Mark G. Mortenson , Vilupanur A. Ravi , Alan S. Nagelberg
IPC分类号： C04B41/52 , C04B41/89 , C22C1/10 , B22D19/14
CPC分类号： C04B41/52 , C04B41/89 , C22C1/1036
摘要： The present invention relates to modifying the properties of a metal matrix composite body by a post formation process modification treatment. The post formation process treatment may be applicable to a variety of metal matrix composite bodies produced by various techniques, and is particularly applicable to modifying the properties of a metal matrix composite body produced by a spontaneous infiltration technique. Particularly, at least a portion of the matrix metal of the metal matrix composite body and/or the filler material of the metal matrix composite body is modified or altered after the formation process. Preferably, the preform contains a second non-metal material, an infiltration enhancer of infiltration enhancer precursor, and an infiltration atmosphere.
摘要翻译：本发明涉及通过后形成工艺改性处理改性金属基复合体的性能。后形成处理可以适用于通过各种技术制造的各种金属基复合体，特别适用于通过自发渗透技术制造的金属基复合体的特性。特别地，金属基体复合体的基体金属的至少一部分和/或金属基复合体的填充材料在形成工序之后被修改或改变。优选地，预成型体包含第二非金属材料，渗透增强剂前体的渗透增强剂和渗透气氛。

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