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1. 发明申请

US20110297898A1 PREPARATION OF A PHOTOCHROMIC INK 失效
标题翻译：光敏墨水的制备
公开(公告)号：US20110297898A1
公开(公告)日：2011-12-08
申请号：US13141718
申请日：2009-12-23
申请人： Marc Maurer , Max Hügin , Thomas Raimann , Leonhard Feiler , Bruno Inderbitzin , André Fuchs
发明人： Marc Maurer , Max Hügin , Thomas Raimann , Leonhard Feiler , Bruno Inderbitzin , André Fuchs
IPC分类号： C09D11/02 , C09D11/10 , C07D491/107 , C09D5/00
CPC分类号： C09K9/02 , C07D491/107 , C09B57/00 , C09D11/037 , C09D11/50 , C09K2211/1029 , C09K2211/1088 , Y10T436/141111
摘要： The present invention relates to a photochromic ink, the process for its preparation which is based on a spiropyran powder obtainable by melting, cooling and crushing, and to a new form of a spiropyran obtainable thereby. Said process to prepare a photochromic ink comprises the steps of a) heating and melting the spiropyran at a temperature below 250 C, b) cooling the melt to obtain a solidified spiropyran, c) crushing the solidified spiropyran to obtain a powder, d) optionally adding the powder to a binder providing the basis for the photochromic ink.
摘要翻译：本发明涉及一种光致变色油墨，其制备方法是基于通过熔融，冷却和粉碎获得的螺吡喃粉末，以及由此获得的新形式的螺吡喃。所述制备光致变色油墨的方法包括以下步骤：a）在低于250℃的温度下加热和熔化螺吡喃，b）冷却熔体以获得固化的吡咯啉，c）粉碎固化的吡咯烷以获得粉末，d）任选地将粉末添加到粘合剂中，为光致变色墨水提供基础。

2. 发明授权

US08287776B2 Preparation of a photochromic ink 失效
标题翻译：光致变色油墨的制备
公开(公告)号：US08287776B2
公开(公告)日：2012-10-16
申请号：US13141718
申请日：2009-12-23
申请人： Marc Maurer , Max Hügin , Thomas Raimann , Leonhard Feiler , Bruno Inderbitzin , André Fuchs
发明人： Marc Maurer , Max Hügin , Thomas Raimann , Leonhard Feiler , Bruno Inderbitzin , André Fuchs
IPC分类号： G02B5/23 , G01N33/00
CPC分类号： C09K9/02 , C07D491/107 , C09B57/00 , C09D11/037 , C09D11/50 , C09K2211/1029 , C09K2211/1088 , Y10T436/141111
摘要： The present invention relates to a photochromic ink, the process for its preparation which is based on a spiropyran powder obtainable by melting, cooling and crushing, and to a new form of a spiropyran obtainable thereby. Said process to prepare a photochromic ink comprises the steps of a) heating and melting the spiropyran at a temperature below 250 C, b) cooling the melt to obtain a solidified spiropyran, c) crushing the solidified spiropyran to obtain a powder, d) optionally adding the powder to a binder providing the basis for the photochromic ink.
摘要翻译：本发明涉及一种光致变色油墨，其制备方法是基于通过熔融，冷却和粉碎获得的螺吡喃粉末，以及由此获得的新形式的螺吡喃。所述制备光致变色油墨的方法包括以下步骤：a）在低于250℃的温度下加热和熔化螺吡喃，b）冷却熔体以获得固化的吡咯啉，c）粉碎固化的吡咯烷以获得粉末，d）任选地将粉末添加到粘合剂中，为光致变色墨水提供基础。

3. 发明授权

US07217803B2 Benzimidazole-pyridone-based azo dyes 失效
标题翻译：苯并咪唑 - 吡啶酮基偶氮染料
公开(公告)号：US07217803B2
公开(公告)日：2007-05-15
申请号：US10537063
申请日：2003-11-26
申请人： Leonhard Feiler , Thomas Raimann , Thomas Eichenberger , Max Hügin
发明人： Leonhard Feiler , Thomas Raimann , Thomas Eichenberger , Max Hügin
IPC分类号： C09B31/14 , C09B29/36 , C09B69/04 , D06P3/60
CPC分类号： C09B69/045 , C09B29/3617 , C09B31/14 , Y10S8/922
摘要： The present invention relates to azo dyes of formula (1) which are soluble in organic solvents, wherein R1 is —CN, —COOR5, —CONR6R7 or a heterocyclic ring, R2 is unsubstituted or substituted alkyl, unsubstituted or substituted aryl, —CF3, —COOR5, —CONR6R7 or —COR5, R3 is hydrogen, —SO3M, alkyl, alkoxy, alkylcarbonyl, —NO2 or halogen, R4 is substituted aryl, substituted heteroaryl or an aryl-N═N-aryl radical, wherein one or both of the aryl radicals in aryl-N═N-aryl is/are unsubstituted or substituted, or a radical heteroaryl-N═N-heteroaryl, wherein one or both of the heteroaryl radicals in heteroaryl-N═N-heteroaryl is/are unsubstituted or substituted, R5 is hydrogen, alkyl or unsubstituted or substituted aryl, R6 is hydrogen, alkyl or unsubstituted or substituted aryl, R7 is hydrogen, alkyl or unsubstituted or substituted aryl, M+ is a cation, n is a number 1, 2 or 3 and m is a number 1, 2 or 3, to a process for the preparation thereof and to the use thereof in the production of colored plastics or polymeric color particles, and as printing inks, printing dyes, coating compositions and wood stains
摘要翻译：本发明涉及可溶于有机溶剂的式（1）的偶氮染料，其中R 1是-CN，-COOR 5，-CONR 6 R 7或杂环R 2是未取代或取代的烷基，未取代或取代的芳基，-CF 3 - ， - COOR 5，-CONR 6 R 7或-COR 5，R 3，是氢，-SO 3 M，烷基，烷氧基，烷基羰基，-NO 2或卤素，R 4是取代的芳基，取代的杂芳基或芳基-NH-芳基，其中芳基-NH-芳基中的一个或两个芳基是未被取代或取代的，或者是杂芳基-NH-杂芳基，其中杂芳基-NN中的一个或两个杂芳基 - 杂芳基是未取代或取代的，R 5是氢，烷基或未取代或取代的芳基，R 6是氢，烷基或未取代或取代的芳基，R SUB > 7是氢，烷基或未取代的取代或取代的芳基，M + +是一种阳离子，n是数字1,2或3，m是数字1,2或3，其制备方法及其用途在生产有色塑料或聚合彩色颗粒时，以及作为印刷油墨，印刷染料，涂料组合物和木材污渍

4. 发明申请

US20120100395A1 INDICATOR SYSTEM FOR MONITORING A STERILIZATION PROCESS 审中-公开
标题翻译：用于监测灭菌过程的指示器系统
公开(公告)号：US20120100395A1
公开(公告)日：2012-04-26
申请号：US13319460
申请日：2010-05-05
申请人： Leonhard Feiler , Hans Reichert , Véronique Hall-Goulle , Thomas Raimann
发明人： Leonhard Feiler , Hans Reichert , Véronique Hall-Goulle , Thomas Raimann
IPC分类号： A61L2/04 , B32B9/04 , G01N31/22 , G01N25/00
CPC分类号： G01N31/226 , C09B7/00 , C09B19/02 , C09B29/12 , C09B29/20 , C09B33/153 , C09B57/004 , C09B67/0063 , C09B68/443 , C09B68/48 , C09D11/50
摘要： The present invention relates to a device for monitoring integral value of time, temperature comprising at least one layer of polymer comprising a latent pigment capable of undergoing at least one colour change, and an organic acid; or comprising one layer of polymer comprising a latent pigment capable of undergoing at least one colour change, and one layer of polymer comprising an organic acid, wherein said latent pigment is converted to its pigmentary form which causes said colour change. The device can be used for monitoring sterilization of medical and kitchen supplies, canned foods and doneness of microwave foods.
摘要翻译：本发明涉及一种用于监测时间积分值的装置，包括至少一层包含能够发生至少一种颜色变化的潜颜料的聚合物层和一种有机酸; 或包含一层包含能够发生至少一种颜色变化的潜在颜料的聚合物层，以及包含有机酸的一层聚合物，其中所述潜在颜料转变为引起所述颜色变化的其颜料形式。该设备可用于监测医疗和厨房用品，罐装食品和微波食品的灭菌。

5. 发明申请

US20100034961A1 PHOTOSTABILIZED TIME TEMPERATURE INDICATOR 审中-公开
标题翻译：光照时间温度指示器
公开(公告)号：US20100034961A1
公开(公告)日：2010-02-11
申请号：US12522559
申请日：2007-12-28
申请人： Elena Tenetov , Husein Salman , Julien Assous , Leonhard Feiler , Thomas Raimann
发明人： Elena Tenetov , Husein Salman , Julien Assous , Leonhard Feiler , Thomas Raimann
IPC分类号： B05D3/10 , C07D209/96
CPC分类号： C09K9/02 , C09K2211/1029 , C09K2211/1088 , G01N31/229
摘要： The present invention relates to time-temperature indicator (TTI) systems comprising spiropyran indicator of formula (I) wherein R1 is hydrogen, —C1-C6 alkoxy, halogen, —C1-C6 alkyl or —NO2, R2 is hydrogen or —C1-C6 alkoxy; R3 is NO2 halogen; R4 is hydrogen, —C1-C6 alkoxy or halogen; R5 is hydrogen, halogen, —C1-C6 alkoxy, —COOH, —COO—C1-C6alkyl, —CF3 or phenyl; R11 hydrogen or R11 and R5 form together a phenyl ring; Y is phenyl, naphthyl, anthracen-9-yl, 9H-fluoren-9-yl or a residue Formula (A) wherein R6 is hydrogen, halogen, —C1-C6 alkoxy, —NO2, —CF3, —O—CF3, —CN, —COO—C1-C6alkyl, phenyl or biphenyl, 9H-fluoren-9-yl; R7 is hydrogen, halogen, —CN,—C1-C6 alkoxy or R7 and R6 form together a phenyl ring; R8 is hydrogen, halogen, —CN, or —C1-C6 alkoxy; R9 is hydrogen or halogen or CN. R10 is hydrogen or halogen or CN. Ra is —(CH2)n- with n=1-6 or —CH2—CH═CH—. With the proviso that Formula (B) and Formula (C) are excluded.
摘要翻译：本发明涉及包含式（I）的螺吡喃指示剂的时间 - 温度指示剂（TTI）系统，其中R 1是氢，-C 1 -C 6烷氧基，卤素，-C 1 -C 6烷基或-NO 2，R 2是氢或-C1- C6烷氧基 R3是NO2卤素; R4是氢，-C 1 -C 6烷氧基或卤素; R 5是氢，卤素，-C 1 -C 6烷氧基，-COOH，-COO-C 1 -C 6烷基，-CF 3或苯基; R11氢或R11和R5一起形成苯环; Y是苯基，萘基，蒽-9-基，9H-芴-9-基或其中R 6是氢，卤素，-C 1 -C 6烷氧基，-NO 2，-CF 3，-O-CF 3， -CN，-COO-C 1 -C 6烷基，苯基或联苯基，9H-芴-9-基; R7是氢，卤素，-CN，-C1-C6烷氧基或R7和R6一起形成苯环; R8是氢，卤素，-CN或-C1-C6烷氧基; R9是氢或卤素或CN。 R 10是氢或卤素或CN。 R a为 - （CH 2）n - ，其中n = 1-6或-CH 2 -CH-CH-。条件是排除式（B）和式（C）。

6. 发明申请

US20120022261A1 Colorant Compositions Containing an Oxonol Dye 审中-公开
标题翻译：含有Oxonol染料的着色剂组合物
公开(公告)号：US20120022261A1
公开(公告)日：2012-01-26
申请号：US13245329
申请日：2011-09-26
申请人： Leonhard Feiler , Thomas Raimann
发明人： Leonhard Feiler , Thomas Raimann
IPC分类号： C07D401/06
CPC分类号： C09D11/328 , C09B23/06 , C09B69/04 , Y10T428/24802
摘要： The present invention relates to an oxonol dye of formula (I) wherein R1 and R2 are each independently of the other linear or branched C2-C6alkyl residues; R3, R4 and R5 are each independently of the other hydrogen, a C2-C14alkyl residue which may be unsubstituted or hydroxy- or amino-substituted and optionally interrupted by an oxygen atom and R6 is a C2-C14alkyl residue, which may be unsubstituted or hydroxy- or amino-substituted and optionally interrupted by an oxygen atom.
摘要翻译：本发明涉及式（I）的氧杂菁染料，其中R 1和R 2各自独立地为其它直链或支链C 2 -C 6烷基残基; R 3，R 4和R 5各自独立地为氢，可以是未取代的或羟基或氨基取代的，任选地被氧原子中断的C 2 -C 14烷基残基，R 6是C 2 -C 14烷基残基，其可以是未取代的或羟基或氨基取代的，并且任选地被氧原子中断。

7. 发明申请

US20110139059A1 TIME TEMPERATURE INDICATOR COMPRISING INDOLENIN BASED SPIROPYRANS CONTAINING A N-ACETYLAMIDO OR N-ACETYLESTER SIDE CHAIN 审中-公开
公开(公告)号：US20110139059A1
公开(公告)日：2011-06-16
申请号：US12990893
申请日：2009-05-11
申请人： Leonhard Feiler , Thomas Raimann
发明人： Leonhard Feiler , Thomas Raimann
IPC分类号： G01D21/00 , C07D491/107 , H05B6/02 , B05D3/10 , B05D3/00
CPC分类号： C07D491/10
摘要： The present invention relates to time-temperature indicator (TTI) systems comprising indolenin based spiropyrans containing a N-acetylamido or N-acetylester side chain, especially to a time temperature indicator comprising at least one spiropyran indicator of formula (I) Wherein R1 is hydrogen, —C1-C18 alkoxy, —C1-C18 alkylthio, —C1-C18 alkyl-SO—, —C1-C18 alkyl-SO2—, phenylthio, phenyl, halogen, —C1-C18 alkylthio, —C1-C18 alkyl-SO—, —C1-C18 alkyl-SO2—, phenylthio, phenyl, halogen, —C1-C18 alkyl or —NO2; R2 is hydrogen or —C1-C18 alkoxy; R3 is NO2 or halogen; R4 is hydrogen, —C1-C18 alkoxy or halogen; R5 is hydrogen, halogen, —C1-C18 alkoxy, —COOH, —COO—C1-C18alkyl, —CF3 or phenyl; R6 is hydrogen or R6 and R7 form together a phenyl ring; R7 is hydrogen; Ra is hydrogen or —C1-C6 alkyl; Rb is hydrogen or —C1-C6 alkyl, or together with Ra form a 5-6 membered ring; Y is —CH2—COO—R8 or —CH2—CO—N(R10)—R9; or CH2—CO—N(R10)-L-N(R10) CO—CH2— or Y is —CH2—CO—O-L′-O—CO—CH2— wherein R8 is hydrogen, C3-C18alkyl or R8 is ethyl with the proviso that R6 and R7 form together a phenyl ring; R9 is phenyl, mesityl, phenyl-O-phenyl, phenyl-S-phenyl, phenyl once or more than once substituted by halogen, —CF3, C1-C6alkyl, —C1-C6 alkoxy, carboxy, —COO—C1-C6alkyl whereby in case of a more than once substitution, the substituent can be the same or different; R10 is hydrogen, C1-C18alkyl; L is 1,3 phenylene or 1,4 phenylene wherein the phenylene linker is optionally substituted by once or more than once by halogen, —CF3, C1-C18 alkoxy, carboxy, —COO—C1-C18alkyl, —CONH2, —CON(C1-C18alkyl)2, nitro; or L is naphthalene, biphenylene or phenylene-O-phenylene wherein the naphthalene, biphenylene or phenylene-O-phenylene linker is optionally substituted once or more than once by halogen, —CF3, C1-C18alkyl, —C1-C18 alkoxy, carboxy, —COO—C1-C18alkyl, —CONH2, —CON(C1-C18alkyl)2, nitro; L′ is 1,3 phenylene

8. 发明申请

US20110059545A1 TIME-TEMPERATURE INDICATOR BASED ON OLIGOMERIC SPIROAROMATICS 审中-公开
标题翻译：基于低压螺旋桨的时间温度指示器
公开(公告)号：US20110059545A1
公开(公告)日：2011-03-10
申请号：US12523110
申请日：2008-01-14
申请人： Husein Salman , Elena Tenetov , Leonhard Feiler , Thomas Raimann
发明人： Husein Salman , Elena Tenetov , Leonhard Feiler , Thomas Raimann
IPC分类号： G01N21/00 , C07D209/96
CPC分类号： C09K9/02 , C09K2211/1029 , C09K2211/1088 , G01D7/005 , G01N31/229
摘要： The present invention relates to a time temperature indicator for indicating a temperature change over time comprising one dimeric or trimeric spiropyran indicator of the formula I or II wherein R1-R4 independently of one another is hydrogen, —C1C6 alkoxy, halogen, CF3, —C1C6 alkyl or —NO2, R5 is hydrogen, halogen, —C1-C6 alkoxy, —COOH, —COO—C1-C6 alkyl, —CF3 or phenyl; R11 is hydrogen or R11 and R5 form together a phenyl ring; Ra is —C1-C6 alkyl Rb is —C1-C6 alkyl, or together with Ra form a 5-6 membered ring L is a divalent linker; L′ is a trivalent linker.
摘要翻译：本发明涉及用于指示随时间的温度变化的时间温度指示剂，包括一种式I或II的二聚或三聚螺吡喃指示剂，其中R 1 -R 4彼此独立地是氢，-C 1 -C 6烷氧基，卤素，CF 3，-C 1 C 6 烷基或-NO 2，R 5是氢，卤素，-C 1 -C 6烷氧基，-COOH，-COO-C 1 -C 6烷基，-CF 3或苯基; R 11是氢或R 11和R 5一起形成苯环; R a为-C 1 -C 6烷基，R b为-C 1 -C 6烷基，或与R a一起形成5-6元环L为二价连接基; L'是三价接头。

9. 发明申请

US20090130400A1 Colorant compositions containing an oxonol dye 审中-公开
标题翻译：含有氧杂菁染料的着色剂组合物
公开(公告)号：US20090130400A1
公开(公告)日：2009-05-21
申请号：US11990815
申请日：2006-08-16
申请人： Leonhard Feiler , Thomas Raimann
发明人： Leonhard Feiler , Thomas Raimann
IPC分类号： B32B5/00 , C09B23/06 , B05D3/00
CPC分类号： C09D11/328 , C09B23/06 , C09B69/04 , Y10T428/24802
摘要： The present invention relates to a colorant composition comprising (i) an oxonol dye of general formula (I) wherein R1 and R2 are each independently of the other linear or branched C2-C6alkyl residues; R3, R4 and R5 are each independently of the other hydrogen, a C2-C14alkyl residue which may be unsubstituted or hydroxy- or amino-substituted and optionally interrupted by an oxygen atom and R6 is a C2-C14alkyl residue, which may be unsubstituted or hydroxy- or amino-substituted and optionally interrupted by an oxygen atom; and (ii) at least one cellulose nitrate binder.
摘要翻译：本发明涉及一种着色剂组合物，其包含（i）通式（I）的氧杂醇菁染料，其中R 1和R 2各自独立于其它直链或支链C 2 -C 6烷基残基; R 3，R 4和R 5各自独立地为氢，可以是未取代的或羟基或氨基取代的，任选地被氧原子中断的C 2 -C 14烷基残基，R 6是C 2 -C 14烷基残基，其可以是未取代的或羟基或氨基取代的，并任选被氧原子中断; 和（ii）至少一种硝酸纤维素粘合剂。

10. 发明申请

US20060053571A1 Azo dyes soluble in organic solvents 失效
标题翻译：偶氮染料可溶于有机溶剂
公开(公告)号：US20060053571A1
公开(公告)日：2006-03-16
申请号：US10537063
申请日：2003-11-26
申请人： Leonhard Feiler , Thomas Raimann , Thomas Eichenberger , Max Hugin
发明人： Leonhard Feiler , Thomas Raimann , Thomas Eichenberger , Max Hugin
IPC分类号： D06P3/52
CPC分类号： C09B69/045 , C09B29/3617 , C09B31/14 , Y10S8/922
摘要： The present invention relates to azo dyes of formula (1) which are soluble in organic solvents, wherein R1 is —CN, —COOR5, —CONR6R7 or a heterocyclic ring, R2 is unsubstituted or substituted alkyl, unsubstituted or substituted aryl, —CF3, —COOR5, —CONR6R7 or —COR5, R3 is hydrogen, —SO3M, alkyl, alkoxy, alkylcarbonyl, —NO2 or halogen, R4 is substituted aryl, substituted heteroaryl or an aryl-N═N-aryl radical, wherein one or both of the aryl radicals in aryl-N═N-aryl is/are unsubstituted or substituted, or a radical heteroaryl-N═N-heteroaryl, wherein one or both of the heteroaryl radicals in heteroaryl-N═N-heteroaryl is/are unsubstituted or substituted, R5 is hydrogen, alkyl or unsubstituted or substituted aryl, R6 is hydrogen, alkyl or unsubstituted or substituted aryl, R7 is hydrogen, alkyl or unsubstituted or substituted aryl, M+ is a cation, n is a number 1, 2 or 3 and m is a number 1, 2 or 3, to a process for the preparation thereof and to the use thereof in the production of coloured plastics or polymeric colour particles, and as printing inks, printing dyes, coating compositions and wood stains.
摘要翻译：

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