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1. 发明申请

US20050214645A1 Process for producing positive electrode active material for lithium secondary battery 有权
标题翻译：锂二次电池用正极活性物质的制造方法
公开(公告)号：US20050214645A1
公开(公告)日：2005-09-29
申请号：US11136493
申请日：2005-05-25
申请人： Kazushige Horichi , Manabu Suhara , Naoshi Saito , Megumi Uchida
发明人： Kazushige Horichi , Manabu Suhara , Naoshi Saito , Megumi Uchida
IPC分类号： C01B11/24 , C01G51/00 , C01G51/04 , H01M4/02 , H01M4/131 , H01M4/1315 , H01M4/48 , H01M4/485 , H01M4/52 , H01M4/525 , H01M10/02 , H01M10/0525 , H01M10/36
CPC分类号： H01M10/0525 , C01G51/42 , C01P2002/52 , C01P2002/72 , C01P2004/51 , C01P2004/61 , C01P2006/11 , C01P2006/12 , C01P2006/40 , H01M4/131 , H01M4/1315 , H01M4/485 , H01M4/525 , H01M2004/021
摘要： To provide a process for producing a lithium-cobalt composite oxide for a positive electrode of a lithium secondary battery, which has a large volume capacity density, high safety, high charge and discharge cycle durability, high press density and high productivity. A process for producing a lithium-cobalt composite oxide represented by the formula LipCoxMyOzFa (wherein M is a transition metal element other than Co, or an alkaline earth metal element, O.9≦p≦1.1, 0.980≦x≦1.000, 0≦y≦0.02, 1.9≦z≦2.1, x+y=1, and 0≦a≦0.02), characterized in that as a cobalt source, a mixture is used which comprises cobalt hydroxide in the form of substantially spherical secondary particles with an average particle size of from 8 to 20 μm formed by agglomeration of primary particles and tricobalt tetroxide in the form of secondary particles with an average particle size of from 2 to 10 μm formed by agglomeration of primary particles, in a cobalt atomic ratio of from 5:1 to 1:5, and firing is carried out at from 700 to 1,050° C.
摘要翻译：为了提供具有大容量密度，高安全性，高充放电循环耐久性，高压力密度和高生产率的锂二次电池正极用锂钴复合氧化物的制造方法。一种由下式表示的锂 - 钴复合氧化物的制备方法：其中R 1，R 2，R 2，（其中M是除Co以外的过渡金属元素或碱土金属元素，O.9 <= p <= 1.1,0.980 <= x <=1.000,0≤y <= 0.02，1.9 <= z <= 2.1，x + y = 1，0 <= a <= 0.02），其特征在于，作为钴源，使用包含基本上为球形的氢氧化钴的混合物平均粒度为8〜20μm的二次粒子是通过一次粒子和四氧化四铁的结合而形成的，该二次粒子是以原子粒子聚集形成的平均粒径为2〜10μm的二次粒子，以钴原子比例为5：1至1：5，焙烧时间为700至1050℃。

2. 发明授权

US08287828B2 Process for producing lithium-containing composite oxide for positive electrode for lithium secondary battery 有权
标题翻译：锂二次电池用正极用锂复合氧化物的制造方法
公开(公告)号：US08287828B2
公开(公告)日：2012-10-16
申请号：US11372003
申请日：2006-03-10
申请人： Takeshi Kawasato , Naoshi Saito , Megumi Uchida , Kazushige Horichi , Koji Tatsumi , Kunihiko Terase , Manabu Suhara
发明人： Takeshi Kawasato , Naoshi Saito , Megumi Uchida , Kazushige Horichi , Koji Tatsumi , Kunihiko Terase , Manabu Suhara
IPC分类号： H01M4/58 , H01M4/50 , H01M4/52 , C01D15/00
CPC分类号： H01M4/505 , H01M4/485 , H01M4/525 , H01M10/0525 , H01M2004/021
摘要： A process for producing a lithium-containing composite oxide for a positive electrode active material for use in a lithium secondary battery, the oxide having the formula LipQqNxMyOzFa (wherein Q is at least one element selected from the group consisting of titanium, zirconium, niobium and tantalum, N is at least one element selected from the group consisting of Co, Mn and Ni, M is at least one element selected from the group consisting of Al, alkaline earth metal elements and transition metal elements other than Q and N, 0.9≦p≦1.1, 0≦q
摘要翻译：一种锂二次电池用正极活性物质的含锂复合氧化物的制造方法，其特征在于，具有式LipQqNxMyOzFa（其中，Q为选自钛，锆，铌和钽，N是选自Co，Mn和Ni中的至少一种元素，M是选自Al，碱土金属元素和Q和N以外的过渡金属元素中的至少一种元素，0.9＆nlE ; p＆nlE; 1.1,0和nlE; q <0.03,0.97和nlE; x和nlE; 1.00,0和nlE; y <0.03,1.9＆amp; nlE; z＆nlE; 2.1，q + x + y = 1和0＆lt; nlE; a＆nlE; 0.02）锂元素源和N元素源的混合物，当这些元素存在时，M元素源和/或氟源在含氧气氛中，其中Q元素源是具有 pH为0.5〜11。

3. 发明授权

US07981547B2 Process for positive electrode active substance for lithium secondary battery 失效
标题翻译：锂二次电池正极活性物质的工艺
公开(公告)号：US07981547B2
公开(公告)日：2011-07-19
申请号：US12849435
申请日：2010-08-03
申请人： Manabu Suhara , Naoshi Saito , Kazushige Horichi , Megumi Uchida
发明人： Manabu Suhara , Naoshi Saito , Kazushige Horichi , Megumi Uchida
IPC分类号： H01M4/58 , H01M4/00 , H01M4/88 , C01D1/02
CPC分类号： H01M4/1315 , C01G51/006 , C01G51/42 , C01P2002/52 , C01P2002/72 , C01P2002/74 , C01P2004/03 , C01P2004/32 , C01P2004/45 , C01P2004/51 , C01P2004/54 , C01P2006/11 , C01P2006/12 , C01P2006/40 , H01M4/131 , H01M4/485 , H01M4/525 , H01M10/052 , H01M10/0565 , H01M2004/021
摘要： A positive electrode active material for a lithium secondary battery containing a lithium-cobalt composite oxide is produced by firing, as a cobalt source, a mixture of substantially spherical cobalt hydroxide or tricobalt tetraoxide having such a sharp particle size distribution that the average particle size D50 is from 7 to 20 μm, and cobalt oxyhydroxide having an average particle size of secondary particles formed by agglomeration of primary particles of from 7 to 20 μm, in a proportion of from 5:1 to 1:5 as the cobalt atomic ratio, at a temperature of from 700° C. to 1050° C. in an oxygen-comprising atmosphere.
摘要翻译：含有锂钴复合氧化物的锂二次电池用正极活性物质是通过以钴原料烧成具有如此尖锐的粒度分布的基本上球形的氢氧化钴或四氧化四钴的混合物来生产的，该平均粒径为D50 为7〜20μm，钴原子比为5:1〜1:5，初级粒子为7〜20μm的平均粒径的二氧化硅氢氧化钴为钴原子比，在含氧气氛中的温度为700℃至1050℃。

4. 发明授权

US07824803B2 Positive electrode active substance for lithium secondary battery and process for producing the same 有权
标题翻译：锂二次电池用正极活性物质及其制造方法
公开(公告)号：US07824803B2
公开(公告)日：2010-11-02
申请号：US12175652
申请日：2008-07-18
申请人： Manabu Suhara , Naoshi Saito , Kazushige Horichi , Megumi Uchida
发明人： Manabu Suhara , Naoshi Saito , Kazushige Horichi , Megumi Uchida
IPC分类号： H01M4/58 , H01M4/00 , H01M4/88 , C01D1/02
CPC分类号： H01M4/1315 , C01G51/006 , C01G51/42 , C01P2002/52 , C01P2002/72 , C01P2002/74 , C01P2004/03 , C01P2004/32 , C01P2004/45 , C01P2004/51 , C01P2004/54 , C01P2006/11 , C01P2006/12 , C01P2006/40 , H01M4/131 , H01M4/485 , H01M4/525 , H01M10/052 , H01M10/0565 , H01M2004/021
摘要： A positive electrode active material is produced by firing, as a cobalt source, a mixture of a) substantially spherical large particle size cobalt hydroxide or tricobalt tetraoxide having a sharp particle size distribution, and b) small particle size cobalt hydroxide or tricobalt tetraoxide, in a proportion of from 9:1 to 1:2 as the cobalt atomic ratio, at a temperature of from 700° C. to 1050° C. in an oxygen-comprising atmosphere.
摘要翻译：正极活性物质是通过焙烧a）基本上球形的大粒径氢氧化钴或具有尖锐粒度分布的四氧化四钴的混合物，以及b）小粒度氢氧化钴或四氧化四钴，在作为钴原子比的9:1至1:2的比例下，在含氧气氛中在700℃至1050℃的温度下进行。

5. 发明申请

US20100294985A1 POSITIVE ELECTRODE ACTIVE SUBSTANCE FOR LITHIUM SECONDARY BATTERY AND PROCESS FOR PRODUCING THE SAME 失效
标题翻译：用于锂二次电池的正极电极活性物质及其制造方法
公开(公告)号：US20100294985A1
公开(公告)日：2010-11-25
申请号：US12849435
申请日：2010-08-03
申请人： Manabu Suhara , Naoshi Saito , Kazushige Horichi , Megumi Uchida
发明人： Manabu Suhara , Naoshi Saito , Kazushige Horichi , Megumi Uchida
IPC分类号： H01M4/525
CPC分类号： H01M4/1315 , C01G51/006 , C01G51/42 , C01P2002/52 , C01P2002/72 , C01P2002/74 , C01P2004/03 , C01P2004/32 , C01P2004/45 , C01P2004/51 , C01P2004/54 , C01P2006/11 , C01P2006/12 , C01P2006/40 , H01M4/131 , H01M4/485 , H01M4/525 , H01M10/052 , H01M10/0565 , H01M2004/021
摘要： A positive electrode active material for a lithium secondary battery containing a lithium-cobalt composite oxide, which has a large volume capacity density, has a high safety and is excellent in charge and discharge cyclic durability, and its production process, are provided.A lithium-cobalt composite oxide represented by the formula LipCoxMyOzFa (wherein M is a transition metal element other than Co or an alkaline earth metal element, 0.9≦p≦1.1, 0.980≦x≦1.000, 0≦y≦0.02, 1.9≦z≦2.1, x+y=1 and 0≦a≦0.02) and comprising a mixture containing substantially spherical hard first particles of lithium-cobalt composite oxide having such a sharp particle size distribution that the volume basis cumulative size D10 is at least 50% of the average particle size D50, and the volume basis cumulative size D90 is at most 150% of the average particle size D50, and second particles of lithium-cobalt composite oxide filling the space among the first particles, in a mass ratio of first particles/second particles of from 1/2 to 9/1, and process for producing the same.
摘要翻译：提供了具有大体积容量密度的含有锂钴复合氧化物的锂二次电池用正极活性物质，其安全性高，充放电循环耐久性优异，其制造方法。由式LipCoxMyOzFa表示的锂钴复合氧化物（其中M是除Co以外的过渡金属元素或碱土金属元素，0.9＆nlE; p＆nlE; 1.1,0.980＆nlE; x＆nlE; 1.000,0和nlE; y＆nlE; 0.02,1.9 并且包括含有基本上球形的硬质的第一第一颗粒的锂 - 钴复合氧化物的混合物，所述锂 - 钴复合氧化物具有这样的尖锐的粒度分布，其体积基础累积尺寸D10处于（例如，n + 1）平均粒径D50的至少50％，体积基础累积尺寸D90为平均粒径D50的150％以下，以及以第一粒子的质量比填充第一粒子之间的空间的第二粒子的锂钴复合氧化物的1/2至9/1的第一颗粒/第二颗粒及其制备方法。

6. 发明申请

US20060263690A1 Positive electrode active material for lithium secondary battery and process for producing the same 审中-公开
标题翻译：锂二次电池用正极活性物质及其制造方法
公开(公告)号：US20060263690A1
公开(公告)日：2006-11-23
申请号：US10529289
申请日：2003-09-25
申请人： Manabu Suhara , Naoshi Saito , Kazushige Horichi , Megumi Uchida
发明人： Manabu Suhara , Naoshi Saito , Kazushige Horichi , Megumi Uchida
IPC分类号： H01M4/58 , H01M4/52
CPC分类号： H01M4/1315 , C01G51/006 , C01G51/42 , C01P2002/52 , C01P2002/72 , C01P2002/74 , C01P2004/03 , C01P2004/32 , C01P2004/45 , C01P2004/51 , C01P2004/54 , C01P2006/11 , C01P2006/12 , C01P2006/40 , H01M4/131 , H01M4/485 , H01M4/525 , H01M10/052 , H01M10/0565 , H01M2004/021
摘要： A positive electrode active material for a lithium secondary battery containing a lithium-cobalt composite oxide, which has a large volume capacity density, has a high safety and is excellent in charge and discharge cyclic durability, and its production process, are provided. A lithium-cobalt composite oxide represented by the formula LipCoxMyOzFa (wherein M is a transition metal element other than Co or an alkaline earth metal element, 0.9≦p≦1.1, 0.980≦x≦1.000, 0≦y≦0.02, 1.9≦z≦2.1, x+y=1 and 0≦a≦0.02) and comprising a mixture containing substantially spherical hard first particles of lithium-cobalt composite oxide having such a sharp particle size distribution that the volume basis cumulative size D10 is at least 50% of the average particle size D50, and the volume basis cumulative size D90 is at most 150% of the average particle size D50, and second particles of lithium-cobalt composite oxide filling the space among the first particles, in a mass ratio of first particles/second particles of from 1/2 to 9/1, and process for producing the same.
摘要翻译：提供了具有大体积容量密度的含有锂钴复合氧化物的锂二次电池用正极活性物质，其安全性高，充放电循环耐久性优异，其制造方法。由下式表示的锂钴复合氧化物：由下式表示的锂 - 钴复合氧化物： a（其中M是除Co或碱土金属元素以外的过渡金属元素，0.9 <= p <= 1.1,0.980 <= x <= 1.000,0 <= y <= 0.02,1.9 < z <= 2.1，x + y = 1，0 <= a <= 0.02），并且包括含有基本上球形的硬质的第一个具有如此尖锐的粒度分布的锂 - 钴复合氧化物颗粒的混合物的混合物，体积基础累积尺寸D10为平均颗粒尺寸D50的至少50％，体积基础累积尺寸D90为平均粒径D50的至多150％，并且以质量计填充第一颗粒之间的空间的第二种锂 - 钴复合氧化物颗粒第一颗粒/第二颗粒的比率为1/2至9/1，及其制备方法。

7. 发明授权

US07501209B2 Process for producing a lithium-cobalt composite oxide for a positive electrode for a lithium secondary cell 失效
标题翻译：锂二次电池用正极用锂钴复合氧化物的制造方法
公开(公告)号：US07501209B2
公开(公告)日：2009-03-10
申请号：US10849856
申请日：2004-05-21
申请人： Manabu Suhara , Naoshi Saito , Kazushige Horichi , Megumi Uchida
发明人： Manabu Suhara , Naoshi Saito , Kazushige Horichi , Megumi Uchida
IPC分类号： H01M4/58
CPC分类号： H01M4/582 , C01G51/42 , C01P2002/52 , C01P2002/54 , C01P2002/72 , C01P2002/74 , C01P2004/10 , C01P2004/32 , C01P2004/45 , C01P2004/50 , C01P2004/51 , C01P2004/61 , C01P2006/11 , C01P2006/12 , H01M4/131 , H01M4/1315 , H01M4/485 , H01M4/525 , H01M10/052 , H01M2004/021 , H01M2004/028
摘要： The present invention provides a positive electrode, which has a large volume capacity density, high safety, and is excellent in the coating uniformity, the charge and discharge cyclic durability and the low-temperature properties.Further, the present invention provides a process for producing a lithium-cobalt composite oxide for a positive electrode for a lithium secondary cell, the lithium-cobalt composite oxide being represented by the formula LipCoxMyOzFa (wherein M is a transition metal element other than Co, aluminum or an alkaline earth metal element, 0.9≦p≦1.1, 0.980≦x≦1.000, 0≦y≦0.02, 1.9≦z≦2.1, x+y=1 and 0≦a≦0.02).
摘要翻译：本发明提供一种具有大体积容量密度，高安全性的正极，并且涂布均匀性，充放电循环耐久性和低温性能优异。此外，本发明提供一种锂二次电池用正极用锂钴复合氧化物的制造方法，所述锂钴复合氧化物由式LipCoxMyOzFa（其中，M为除Co以外的过渡金属元素）铝或碱土金属元素，0.9 <= p <= 1.1,0.980 <= x <= 1.000,0 <= y <= 0.02,1.9 <= z <= 2.1，x + y = 1和0 <= a <= 0.02）。

8. 发明授权

US07192672B2 Process for producing positive electrode active material for lithium secondary battery 有权
标题翻译：锂二次电池用正极活性物质的制造方法
公开(公告)号：US07192672B2
公开(公告)日：2007-03-20
申请号：US11136493
申请日：2005-05-25
申请人： Kazushige Horichi , Manabu Suhara , Naoshi Saito , Megumi Uchida
发明人： Kazushige Horichi , Manabu Suhara , Naoshi Saito , Megumi Uchida
IPC分类号： H01M4/00
CPC分类号： H01M10/0525 , C01G51/42 , C01P2002/52 , C01P2002/72 , C01P2004/51 , C01P2004/61 , C01P2006/11 , C01P2006/12 , C01P2006/40 , H01M4/131 , H01M4/1315 , H01M4/485 , H01M4/525 , H01M2004/021
摘要： To provide a process for producing a lithium-cobalt composite oxide for a positive electrode of a lithium secondary battery, which has a large volume capacity density, high safety, high charge and discharge cycle durability, high press density and high productivity.A process for producing a lithium-cobalt composite oxide represented by the formula LipCoxMyOzFa (wherein M is a transition metal element other than Co, or an alkaline earth metal element, 0.9≦p≦1.1, 0.980≦x≦1.000, 0≦y≦0.02, 1.9≦z≦2.1, x+y=1, and 0≦a≦0.02), characterized in that as a cobalt source, a mixture is used which comprises cobalt hydroxide in the form of substantially spherical secondary particles with an average particle size of from 8 to 20 μm formed by agglomeration of primary particles and tricobalt tetroxide in the form of secondary particles with an average particle size of from 2 to 10 μm formed by agglomeration of primary particles, in a cobalt atomic ratio of from 5:1 to 1:5, and firing is carried out at from 700 to 1,050° C.
摘要翻译：为了提供具有大容量密度，高安全性，高充放电循环耐久性，高压力密度和高生产率的锂二次电池正极用锂钴复合氧化物的制造方法。一种由下式表示的锂 - 钴复合氧化物的制备方法：其中R 1，R 2，R 2，（其中M是除Co以外的过渡金属元素或碱土金属元素，0.9 <= p <= 1.1,0.980 <= x <= 1.000,0 <= y < 0.02，1.9 <= z <= 2.1，x + y = 1，0 <= a <= 0.02），其特征在于，作为钴源，使用包含基本上球形二次粒子形式的氢氧化钴的混合物平均粒度为8〜20μm的原子粒子的原子比通过一次粒子的聚集而形成的平均粒径为2〜10μm的二次粒子的一次粒子和四氧化四铁的凝聚而形成的平均粒径为8〜从5:1至1:5，并且在700至1050℃进行烧制。

9. 发明申请

US20060154146A1 Process for producing lithium-containing composite oxide for positive electrode for lithium secondary battery 有权
标题翻译：锂二次电池用正极用锂复合氧化物的制造方法
公开(公告)号：US20060154146A1
公开(公告)日：2006-07-13
申请号：US11372003
申请日：2006-03-10
申请人： Takeshi Kawasato , Naoshi Saito , Megumi Uchida , Kazushige Horichi , Koji Tatsumi , Kunihiko Terase , Manabu Suhara
发明人： Takeshi Kawasato , Naoshi Saito , Megumi Uchida , Kazushige Horichi , Koji Tatsumi , Kunihiko Terase , Manabu Suhara
IPC分类号： H01M4/58 , H01M4/52 , H01M4/50 , C01B9/08 , C01F7/50 , H01B1/02 , C01G25/02 , C01G11/02 , C01F11/02 , C01G53/04 , C01D1/02 , C01G51/04 , C01G33/00 , C01G19/02 , C01G23/00 , C01G45/12 , C01F7/16
CPC分类号： H01M4/505 , H01M4/485 , H01M4/525 , H01M10/0525 , H01M2004/021
摘要： It is to provide a positive electrode active material for a lithium secondary battery, which has a large volume capacity density and high safety, is excellent in uniform coating properties and is excellent in the charge and discharge cyclic durability and low temperature characteristics even at a high charge voltage. A process for producing a lithium-containing composite oxide represented by the formula LipQqNxMyOzFa (wherein Q is at least one element selected from the group consisting of titanium, zirconium, niobium and tantalum, N is at least one element selected from the group consisting of Co, Mn and Ni, M is at least one element selected from the group consisting of Al, alkaline earth metal elements and transition metal elements other than the Q element and the N element, 0.9≦p≦1.1, 0
摘要翻译：本发明提供一种具有容量密度大，安全性高的锂二次电池用正极活性物质，均匀涂布性能优异，即使在高温下也具有优异的充放电循环耐久性和低温特性充电电压。一种由下式表示的含锂复合氧化物的制备方法：其中R 1，R 2，R 2，R 3，（其中Q是选自钛，锆，铌和钽中的至少一种元素，N是选自下组中的至少一种元素：其中Q是选自钛，锆，铌和钽中的至少一种元素，由Co，Mn和Ni组成，M是选自Al，碱土金属元素和Q元素和N元素以外的过渡金属元素中的至少一种元素，0.9 <= p <= 1.1,0 < 来自锂源的q <= 0.03,0.97 <= x <1.00,0 <= y <0.03,1.9 <= z <= 2.1，q + x + y = 1和0 <= a <= 0.02）元素源和N元素源，并且如果需要，选自由M元素源和氟源组成的组中的至少一种源，其特征在于将作为Q元素源的Q元素化合物水溶液用作pH值为 0.5至11。

10. 发明授权

US07270797B2 Process for producing positive electrode active material for lithium secondary battery 失效
标题翻译：锂二次电池用正极活性物质的制造方法
公开(公告)号：US07270797B2
公开(公告)日：2007-09-18
申请号：US11128198
申请日：2005-05-13
申请人： Manabu Suhara , Naoshi Saito , Kazushige Horichi , Koji Tatsumi
发明人： Manabu Suhara , Naoshi Saito , Kazushige Horichi , Koji Tatsumi
IPC分类号： C01D1/02 , C01B13/14 , H01M4/58
CPC分类号： H01M4/0471 , C01G51/42 , C01P2002/72 , C01P2002/74 , C01P2004/50 , C01P2004/51 , C01P2004/61 , C01P2006/11 , C01P2006/12 , C01P2006/40 , H01M4/02 , H01M4/364 , H01M4/525 , H01M4/582 , H01M4/60 , H01M4/62 , H01M6/164 , H01M10/052 , H01M2004/021 , H01M2004/028
摘要： To provide a process for producing a lithium-cobalt composite oxide for a positive electrode of a lithium secondary battery excellent in volume capacity density, safety, charge and discharge cyclic durability, press density and productivity, by using in expensive cobalt hydroxide and lithium carbonate. A mixture having a cobalt hydroxide powder and a lithium carbonate powder mixed so that the atomic ratio of lithium/cobalt would be from 0.98 to 1.01, is fired in an oxygen-containing atmosphere at from 250 to 700° C., and the fired product is further fired in an oxygen-containing atmosphere at from 850 to 1,050° C., or such a mixture is heated at a temperature-raising rate of at most 4° C./min in a range from 250 to 600° C. and fired in an oxygen-containing atmosphere at from 850 to 1,050° C.
摘要翻译：为了提供一种生产锂二次电池用正极中的锂钴复合氧化物的方法，该锂二次电池的正极通过在昂贵的氢氧化钴和碳酸锂中的使用而具有优异的体积容量密度，安全性，充放电循环耐久性，压力密度和生产率。将混合物以氢氧化钴粉末和碳酸锂粉末混合，使得锂/钴的原子比为0.98〜1.01，在250〜700℃的含氧气氛中烧成，烧成品在850〜1050℃的含氧气氛中进一步烧成，或将这种混合物以250℃〜600℃的升温速度加热至4℃/分钟以上，在含氧气氛中在850〜1050℃下烧成。

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