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1. 发明授权

US06303092B1 Process for operating equilibrium controlled reactions 失效
标题翻译：操作平衡控制反应的方法
公开(公告)号：US06303092B1
公开(公告)日：2001-10-16
申请号：US08419317
申请日：1995-04-10
申请人： Madhu Anand , Shivaji Sircar , Brian Thomas Carvill
发明人： Madhu Anand , Shivaji Sircar , Brian Thomas Carvill
IPC分类号： C01B3118
CPC分类号： C01B3/56 , B01D53/02 , B01D2257/504 , B01D2259/402 , B01J8/0005 , B01J8/008 , B01J8/04 , B01J19/0006 , B01J20/02 , B01J20/0211 , B01J20/0225 , B01J20/0233 , B01J20/0237 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/103 , B01J20/18 , B01J20/3204 , B01J20/3236 , B01J2208/00132 , B01J2208/00141 , B01J2208/00274 , B01J2208/00309 , B01J2208/0053 , B01J2208/00539 , B01J2208/0061 , C01B3/38 , C01B32/40 , C01B2203/02 , C01B2203/0233 , C01B2203/0238 , C01B2203/0283 , C01B2203/0405 , C01B2203/042 , C01B2203/043 , C01B2203/047 , C01B2203/0475 , C01B2203/0495 , C01B2203/0883 , C01B2203/1058 , C01B2203/1064 , C01B2203/1082 , C01B2203/1241 , C01B2203/147 , C01B2203/148 , C01B2203/80 , Y02C10/08 , Y02P20/152 , Y02P20/52
摘要： The present invention is a process for operating equilibrium controlled reactions in continuous mode wherein a feedstock is reacted in a plurality of reactors containing an admixture of a desired process catalyst and an adsorbent to form a product which is selectively adsorbed by the adsorbent and an admixture containing a product which is withdrawn from the reactor. A series of separation steps is used to desorb the product which is selectively adsorbed by the adsorbent and to prepare the reactor for a subsequent process cycle. The process utilizes a novel series of adsorption and desorption steps to collect the less selectively adsorbed product in substantially pure form under relatively constant flow rate at feedstock pressure.
摘要翻译：本发明是一种在连续模式下操作平衡控制反应的方法，其中原料在含有所需工艺催化剂和吸附剂的混合物的多个反应器中反应以形成被吸附剂选择性吸附的产物和含有从反应器中取出的产物。一系列分离步骤用于解吸吸附剂选择性吸附的产物，并为随后的工艺循环制备反应器。该方法利用新的一系列吸附和解吸步骤，以在原料压力下以相对恒定的流速收集基本上纯的形式的较少选择性吸附的产物。

2. 发明授权

US06312658B1 Integrated steam methane reforming process for producing carbon monoxide and hydrogen 失效
标题翻译：用于生产一氧化碳和氢气的综合蒸汽甲烷重整方法
公开(公告)号：US06312658B1
公开(公告)日：2001-11-06
申请号：US08624149
申请日：1996-04-08
申请人： Jeffrey Raymond Hufton , Shivaji Sircar , William Frederick Baade , Joseph Michael Abrardo , Madhu Anand
发明人： Jeffrey Raymond Hufton , Shivaji Sircar , William Frederick Baade , Joseph Michael Abrardo , Madhu Anand
IPC分类号： C01B3118
CPC分类号： C01B3/56 , B01D53/02 , B01D2257/504 , B01D2259/402 , B01J8/0005 , B01J8/008 , B01J8/04 , B01J19/0006 , B01J20/02 , B01J20/0211 , B01J20/0225 , B01J20/0233 , B01J20/0237 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/103 , B01J20/18 , B01J20/3204 , B01J20/3236 , B01J2208/00132 , B01J2208/00141 , B01J2208/00274 , B01J2208/00309 , B01J2208/0053 , B01J2208/00539 , B01J2208/0061 , C01B3/38 , C01B32/40 , C01B2203/02 , C01B2203/0233 , C01B2203/0238 , C01B2203/0283 , C01B2203/0405 , C01B2203/042 , C01B2203/043 , C01B2203/047 , C01B2203/0475 , C01B2203/0495 , C01B2203/0883 , C01B2203/1058 , C01B2203/1064 , C01B2203/1082 , C01B2203/1241 , C01B2203/147 , C01B2203/148 , C01B2203/80 , Y02C10/08 , Y02P20/152 , Y02P20/52
摘要： The present invention is a process for producing an essentially pure carbon monoxide (CO) product and an essentially pure hydrogen product by reforming a hydrocarbon such as methane and steam in the presence of a reforming catalyst to produce a reformate product enriched in CO, carbon dioxide and hydrogen. The reformate is subjected to an integrated series of separation steps and carbon dioxide present in a portion of the waste effluent recovered from such series of spearation steps is shifted to CO in an integrated sorption enhanced reaction (SER) process.
摘要翻译：本发明是通过在重整催化剂存在下重整烃如甲烷和蒸汽来生产基本上纯的一氧化碳（CO）产物和基本上纯的氢产物的方法，以产生富含CO，二氧化碳的重整产品和氢气。重整产物经受一系列分离步骤，存在于从这种串联步骤中回收的废液中的一部分二氧化碳在一体化吸附增强反应（SER）方法中转移到CO。

3. 发明授权

US5753010A Hydrogen recovery by pressure swing adsorption integrated with adsorbent membranes 失效
标题翻译：通过与吸附膜结合的变压吸附氢回收
公开(公告)号：US5753010A
公开(公告)日：1998-05-19
申请号：US736846
申请日：1996-10-28
申请人： Shivaji Sircar , William Emil Waldron , Madhu Anand , Madhukar Bhaskara Rao
发明人： Shivaji Sircar , William Emil Waldron , Madhu Anand , Madhukar Bhaskara Rao
IPC分类号： B01D53/047 , B01D53/22
CPC分类号： B01D53/047 , B01D2256/16 , B01D2257/50 , B01D2257/7022 , B01D2259/4006 , B01D53/0446
摘要： A method for increasing product recovery or reducing the size of steam methane reformer and pressure swing adsorption systems utilized for hydrogen production. A significant portion of the hydrogen in the PSA depressurization and purge effluent gas, which is otherwise burned as fuel in the reformer, is recovered and recycled to the PSA system to provide additional high purity hydrogen product. This is accomplished by processing selected portions of the depressurization and purge effluent gas in adsorbent membrane separators to increase hydrogen content for recycle to the PSA system. Remaining portions of the depressurization and purge effluent gas which contain lower concentrations of hydrogen are utilized for fuel value in the reformer.
摘要翻译：一种用于提高产品回收率或减小用于氢气生产的蒸汽甲烷重整器和变压吸附系统的尺寸的方法。回收再循环到PSA系统中的PSA减压和吹扫废气中的大部分氢，否则这些氢气作为燃料被燃烧，以提供额外的高纯度氢产物。这是通过在吸附膜分离器中处理选定部分的减压和吹扫流出气体来实现的，以增加用于再循环到PSA系统中的氢含量。含有较低浓度氢的减压和吹扫废气的剩余部分用于重整器中的燃料价值。

4. 发明授权

US5435836A Hydrogen recovery by adsorbent membranes 失效
标题翻译：通过吸附膜回收氢气
公开(公告)号：US5435836A
公开(公告)日：1995-07-25
申请号：US173457
申请日：1993-12-23
申请人： Madhu Anand , Madhukar B. Rao , Shivaji Sircar
发明人： Madhu Anand , Madhukar B. Rao , Shivaji Sircar
IPC分类号： B01D53/22 , C01B3/50 , C01B3/56 , B01D53/047
CPC分类号： B01D53/229 , C01B3/501 , C01B3/56 , C01B2203/0405 , C01B2203/043 , C01B2203/047 , C01B2203/0475 , C01B2203/048
摘要： Recovery of hydrogen from hydrogen-containing gas mixtures by pressure swing adsorption is increased by utilizing an adsorbent membrane to concentrate hydrogen in the pressure swing adsorption reject gas and recycling the resulting hydrogen-enriched stream to the feed of the pressure swing adsorption system. Lower compression requirements are realized compared with the use of polymeric membranes for the same service because the hydrogen-enriched stream is recovered from the adsorbent membrane as nonpermeate at essentially the membrane feed pressure. Simultaneous permeation of carbon dioxide and methane occur in the adsorbent membrane, which can be operated at feed pressures as low as 5 psig when hydrogen is used as a sweep gas.
摘要翻译：通过利用吸附剂膜将氢气在变压吸附废气中浓缩并将所得富氢物流再循环到变压吸附系统的进料中，通过变压吸附从含氢气体混合物中回收氢。与使用相同服务的聚合物膜相比，实现了较低的压缩要求，因为在基本上膜进料压力下，富集的流从吸附膜回收为非渗透性。在吸附剂膜中同时渗透二氧化碳和甲烷，当氢气用作吹扫气体时，其可以在低至5psig的进料压力下操作。

5. 发明授权

US06328945B1 Integrated steam methane reforming process for producing carbon monoxide 失效
标题翻译：用于生产一氧化碳的综合蒸汽甲烷重整方法
公开(公告)号：US06328945B1
公开(公告)日：2001-12-11
申请号：US08624148
申请日：1996-04-08
申请人： Jeffrey Raymond Hufton , Shivaji Sircar , William Frederick Baade , Joseph Michael Abrardo , Madhu Anand
发明人： Jeffrey Raymond Hufton , Shivaji Sircar , William Frederick Baade , Joseph Michael Abrardo , Madhu Anand
IPC分类号： C01B3118
CPC分类号： C01B3/56 , B01D53/02 , B01D2257/504 , B01D2259/402 , B01J8/0005 , B01J8/008 , B01J8/04 , B01J19/0006 , B01J20/02 , B01J20/0211 , B01J20/0225 , B01J20/0233 , B01J20/0237 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/103 , B01J20/18 , B01J20/3204 , B01J20/3236 , B01J2208/00132 , B01J2208/00141 , B01J2208/00274 , B01J2208/00309 , B01J2208/0053 , B01J2208/00539 , B01J2208/0061 , C01B3/38 , C01B32/40 , C01B2203/02 , C01B2203/0233 , C01B2203/0238 , C01B2203/0283 , C01B2203/0405 , C01B2203/042 , C01B2203/043 , C01B2203/047 , C01B2203/0475 , C01B2203/0495 , C01B2203/0883 , C01B2203/1058 , C01B2203/1064 , C01B2203/1082 , C01B2203/1241 , C01B2203/147 , C01B2203/148 , C01B2203/80 , Y02C10/08 , Y02P20/152 , Y02P20/52
摘要： A process for producing carbon monoxide (CO) by reforming methane and steam in the presence of a reforming catalyst to produce a reformate product enriched in CO, carbon dioxide (CO2) and hydrogen. CO2 in the enriched reformate is shifted to CO in an integrated sorption enhanced reaction (SER) cycle which employs a series of cyclic steps to facilitate reaction of CO2 and hydrogen at high conversion and to produce a CO-enriched product obtained at reactor feed pressure and at essentially constant flow rate. A series of adsorbent regeneration step including depressurization, purging and product pressurization are used to desorb water which is selectively adsorbed by the adsorbent during the shift reaction and to prepare the reactor for a subsequent process cycle.
摘要翻译：一种通过在重整催化剂存在下重整甲烷和蒸汽来生产一氧化碳（CO）的方法，以生产富含CO，二氧化碳（CO 2）和氢的重整产物。富集的重整产物中的CO 2在集成吸附增强反应（SER）循环中转移到CO，其采用一系列循环步骤以促进CO 2和氢在高转化率下的反应并产生在反应器进料压力下获得的富含CO的产物，基本上恒定的流速。一系列吸附剂再生步骤包括减压，净化和产物加压，用于解吸在转化反应期间被吸附剂选择性吸附的水，并为后续的工艺循环制备反应器。

6. 发明授权

US5779768A Recovery of volatile organic compounds from gas streams 失效
标题翻译：从气流中回收挥发性有机化合物
公开(公告)号：US5779768A
公开(公告)日：1998-07-14
申请号：US619846
申请日：1996-03-19
申请人： Madhu Anand , Shivaji Sircar , Augustine Ivanhoe Dalton
发明人： Madhu Anand , Shivaji Sircar , Augustine Ivanhoe Dalton
IPC分类号： B01D53/00 , B01D53/04 , B01D53/047
CPC分类号： B01D53/0462 , B01D53/002 , B01D2253/102 , B01D2253/104 , B01D2253/106 , B01D2253/108 , B01D2256/10 , B01D2256/16 , B01D2256/18 , B01D2257/708 , B01D2259/40047 , B01D2259/40056 , B01D2259/40081 , B01D2259/4009 , B01D2259/402
摘要： A condensable component present at low concentration in a feed gas mixture containing the condensable component and a noncondensable component is recovered by selective adsorption from the feed gas mixture in an adsorption step, the resulting adsorbed condensable component is desorbed by a heated purge gas in a regeneration step to yield a purge gas effluent enriched in desorbed condensable component, and the purge gas effluent is cooled to condense and recover the condensable component as a liquid. An improvement comprises, during a time period of the regeneration step in which the concentration of the condensable component in the purge gas effluent reaches a maximum value, (a) dividing the purge gas effluent into a first and a second portion, (b) cooling the first portion of the purge gas effluent to a temperature sufficient to condense substantially all of the condensable component present therein and recovering the resulting condensate therefrom, and (c) cooling a second portion of the purge gas effluent and combining the resulting cooled gas stream with the feed gas mixture to yield a total feed mixture for the adsorption step.
摘要翻译：通过在吸附步骤中从进料气体混合物中选择性吸附来回收在含有可冷凝组分和不可冷凝组分的进料气体混合物中低浓度存在的可冷凝组分，所得吸附的可冷凝组分在再生中被加热的吹扫气体解吸逐步产生富集解吸的可冷凝组分的吹扫气体流出物，并将吹扫气体流出物冷却以冷凝并回收可冷凝组分作为液体。改进包括在再生步骤的时间段内，其中净化气体流出物中的可冷凝组分的浓度达到最大值，（a）将净化气体流出物分成第一和第二部分，（b）冷却净化气体流出物的第一部分达到足以冷凝基本上所有可冷凝组分的温度并从其中回收所得的冷凝物，和（c）冷却第二部分吹扫气流出物并将所得到的冷却气流与进料气体混合物以产生用于吸附步骤的总进料混合物。

7. 发明授权

US09656865B2 Use of storage-stable aqueous solutions of chlorine dioxide to generate pure chlorine dioxide gas for decontamination 有权
公开(公告)号：US09656865B2
公开(公告)日：2017-05-23
申请号：US12296051
申请日：2007-04-05
申请人： Thomas Ellsworth McWhorter , Aaron Rosenblatt , Madhu Anand , John Peter Hobbs
发明人： Thomas Ellsworth McWhorter , Aaron Rosenblatt , Madhu Anand , John Peter Hobbs
IPC分类号： A61L2/20 , C01B11/02 , A61L2/22
CPC分类号： C01B11/022 , A61L2/20 , A61L2/22
摘要： New methods are disclosed for decontaminating surfaces and enclosures that avoid problems such as salt deposits, corrosion and condensation that accompany the use of known methods. The methods involve the use of chlorine dioxide solutions prepared by passing dilute chlorine gas over solid granular sodium chlorite to produce chlorine dioxide gas which is then collected to form a solution with very low levels of impurities. The chlorine dioxide gas can be introduced into an enclosure and used to disinfect a portion of the contents of the enclosure.

8. 发明授权

US09045340B2 Storage-stable aqueous solutions of chlorine dioxide and methods for preparing and using them 有权
公开(公告)号：US09045340B2
公开(公告)日：2015-06-02
申请号：US13365902
申请日：2012-02-03
申请人： Thomas Ellsworth McWhorter , Peter Kazlas , Madhu Anand , John Peter Hobbs , Aaron A. Rosenblatt , Robert H. Shay , Barzin Keramati
发明人： Thomas Ellsworth McWhorter , Peter Kazlas , Madhu Anand , John Peter Hobbs , Aaron A. Rosenblatt , Robert H. Shay , Barzin Keramati
IPC分类号： A61L2/18 , C01B11/02
CPC分类号： C01B11/024 , A01N59/00 , A61K33/00 , B65B63/00 , C01B11/022 , C01B11/028 , Y10T428/13 , Y10T428/131 , Y10T428/1334 , Y10T428/1352
摘要： The present invention is for extremely pure solutions of chlorine dioxide, methods for making such solutions and to compositions and methods for storing, shipping and using such solutions. Generally, the chlorine dioxide solutions of the invention are aqueous solutions containing about 2500 ppm or less of total impurities. The chlorine dioxide solution can be prepare by passing dilute highly pure chlorine gas through a bed of substantially solid sodium chlorite and contacting the resulting chlorine dioxide gas with a liquid.

9. 发明授权

US07955588B2 Metal sulfide catalysts and methods of making same 有权
标题翻译：金属硫化物催化剂及其制备方法
公开(公告)号：US07955588B2
公开(公告)日：2011-06-07
申请号：US12783663
申请日：2010-05-20
申请人： Madhu Anand , Brian C. Dunn , Glenn W. Dodwell
发明人： Madhu Anand , Brian C. Dunn , Glenn W. Dodwell
IPC分类号： B01J27/04 , B01J27/047 , B01J27/051 , B01J37/20 , C07C9/04
CPC分类号： C01G39/06 , B01J27/04 , B01J27/047 , B01J27/051 , B01J37/031 , C01G31/00 , C01G41/00
摘要： Methods and apparatus relate to catalysts and preparation of the catalysts, which are defined by sulfides of a transition metal, such as one of molybdenum, tungsten, and vanadium. Precursors for the catalysts include a metal ion source compound, such as molybdenum trioxide, and a sulfide ion source compound, such as thioacetamide. Once the precursors are dissolved if solid and combined in a mixture, homogenous precipitation from the mixture forms the catalysts. Exemplary uses of the catalysts include packing for a methanation reactor that converts carbon monoxide and hydrogen into methane.
摘要翻译：方法和装置涉及催化剂和制备催化剂，其由过渡金属的硫化物如钼，钨和钒中的一种所定义。催化剂的前体包括金属离子源化合物，例如三氧化钼，以及硫化物离子源化合物，例如硫代乙酰胺。一旦前体溶解如果固体并在混合物中组合，则从混合物中均匀沉淀形成催化剂。催化剂的示例性用途包括将一氧化碳和氢气转化为甲烷的甲烷化反应器的填料。

10. 发明申请

US20070243716A1 Selection and deposition of nanoparticles using CO2-expanded liquids 有权
标题翻译：使用二氧化碳膨胀液体选择和沉积纳米颗粒
公开(公告)号：US20070243716A1
公开(公告)日：2007-10-18
申请号：US11237601
申请日：2005-09-27
申请人： Christopher Roberts , Marshall McLeod , Madhu Anand
发明人： Christopher Roberts , Marshall McLeod , Madhu Anand
IPC分类号： H01L21/31
CPC分类号： C30B7/00 , B05D1/18 , B05D2401/32 , B05D2401/90 , B82Y30/00 , C30B7/005 , C30B29/605 , Y10S977/70 , Y10S977/773
摘要： A method for size selection of nanostructures comprising utilizing a gas-expanded liquids (GEL) and controlled pressure to precipitate desired size populations of nanostructures, e.g., monodisperse. The GEL can comprise CO2 antisolvent and an organic solvent. The method can be carried out in an apparatus comprising a first open vessel configured to allow movement of a liquid/particle solution to specific desired locations within the vessel, a second pressure vessel, a location controller for controlling location of the particles and solution within the first vessel, a inlet for addition of antisolvent to the first vessel, and a device for measuring the amount of antisolvent added. Also disclosed is a method for forming nanoparticle thin films comprising utilizing a GEL containing a substrate, pressurizing the solution to precipitate and deposit nanoparticles onto the substrate, removing the solvent thereby leaving a thin nanoparticle film, removing the solvent and antisolvent, and drying the film.
摘要翻译：纳米结构尺寸选择的方法包括利用气体膨胀液体（GEL）和受控压力来沉淀所需尺寸的纳米结构体，例如单分散。 GEL可以包含CO 2反溶剂和有机溶剂。该方法可以在包括构造成允许液体/颗粒溶液移动到容器内的特定所需位置的第一开放容器的设备中进行，第二压力容器，位置控制器，用于控制颗粒和溶液的位置第一容器，用于向第一容器添加抗溶剂的入口，以及用于测量加入的抗溶剂量的装置。还公开了一种用于形成纳米颗粒薄膜的方法，其包括使用含有底物的GEL，将溶液加压沉淀并将纳米颗粒沉积到基底上，除去溶剂从而留下薄的纳米颗粒膜，除去溶剂和反溶剂，并干燥该膜。

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