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1. 发明授权

US5215618A A process for bonding substrates with an ester group-containing hot melt adhesive 失效
标题翻译：使用含钙组合热熔胶粘合基材的方法
公开(公告)号：US5215618A
公开(公告)日：1993-06-01
申请号：US742251
申请日：1991-08-08
申请人： Lutz Schmalstieg , Eduard Haensel , Klaus Nachtkamp , Heinrich Konigshofen , Otto Ganster
发明人： Lutz Schmalstieg , Eduard Haensel , Klaus Nachtkamp , Heinrich Konigshofen , Otto Ganster
IPC分类号： C08G18/10 , C08G18/30 , C08G18/42 , C08G18/77 , C09J5/06 , C09J175/00 , C09J175/04
CPC分类号： C08G18/302 , C08G18/307 , C08G18/771 , C08G2170/20
摘要： Disclosed herein is a process for bonding substrates comprising applying a hot-melt adhesive to the surface of at least one of the substrates and contacting the surface of said substrate with the surface of the other substrate, said adhesive containing an ester group-containing polyisocyanate which is a solid below 30.degree. C. and liquid above 100.degree. C., corresponding to formula (I)A(OCO-B-NCO).sub.n (I)in whichn stands for a whole number or a fraction (statistical average) of from 2 to 6,A stands for an n-valent organic group such as is obtained by removal of hydroxyl groups from an n-valent polyhydroxyl compound in the molecular weight (Mn) range of from 800 to 6000 containing ester and/or carbonate groups andB stands for an aliphatic, cycloaliphatic or aromatic hydrocarbon group having up to 18 carbon atoms.
摘要翻译：本文公开了一种用于粘合基材的方法，包括将热熔粘合剂施加到至少一个基材的表面并使所述基材的表面与另一个基材的表面接触，所述粘合剂含有含酯基的多异氰酸酯，是低于30℃的固体和高于100℃的液体，对应于式（I）A（OCO-B-NCO）n（I），其中n代表整数或分数（统计平均值） 2〜6中，A表示通过从含有酯和/或碳酸酯基的800〜6000的分子量（Mn）范围的n价多羟基化合物除去羟基而得到的n价有机基团 B代表具有至多18个碳原子的脂族，脂环族或芳族烃基。

2. 发明授权

US5219975A Process for the preparation of amines, the amines thus obtained and the use thereof as hardeners for epoxide resins 失效
标题翻译：制备氨基酸的方法，获得的氨基酸及其作为环氧化物树脂硬化剂的用途
公开(公告)号：US5219975A
公开(公告)日：1993-06-15
申请号：US696901
申请日：1991-05-07
申请人： Lutz Schmalstieg , Karl-Heinz Hentschel , Josef Pedain , Klaus Nachtkamp
发明人： Lutz Schmalstieg , Karl-Heinz Hentschel , Josef Pedain , Klaus Nachtkamp
IPC分类号： C08G18/10 , C08G18/32 , C08G18/80 , C08G59/00 , C08G59/50 , C08L63/00
CPC分类号： C08G18/10 , C08L63/00
摘要： The present invention is directed to a process for the preparation of amines containing urethane and urea groups. The amines are produced by reacting A) isocyanate prepolymers containing urethane groups and in which the isocyanate groups are reversibly blocked with secondary monoamines with B) amines having molecular weights of from 60 to 500, which are at least difunctional and which have a total of at least two primary or secondary amino groups, with splitting off of the secondary monoamine. The invention is also directed to the amines so produced and to the use as a hardener for an epoxide resin.
摘要翻译：本发明涉及一种制备含氨基甲酸酯和脲基的胺的方法。胺是通过使A）含有氨基甲酸酯基团的异氰酸酯预聚物与其中异氰酸酯基团与二级单胺可逆地封端的B）制备的，B）分子量为60至500的胺，其至少是双官能的，并且总共在至少两个伯或仲氨基，分离出次级单胺。本发明还涉及如此制备的胺和用作环氧树脂的硬化剂的用途。

3. 发明授权

US5747628A Polyisocyanates containing ether and urethane groups, a process for their preparation and their use in the production of polyurethane lacquers 失效
标题翻译：含有醚和氨基甲酸酯基团的聚异氰酸酯，其制备方法及其在生产聚氨酯漆中的应用
公开(公告)号：US5747628A
公开(公告)日：1998-05-05
申请号：US984596
申请日：1992-12-02
申请人： Lutz Schmalstieg , Hermann Gruber , Bernd Riberi , Klaus Nachtkamp
发明人： Lutz Schmalstieg , Hermann Gruber , Bernd Riberi , Klaus Nachtkamp
IPC分类号： C08G18/32 , C07C271/28 , C08G18/10 , C08G18/73 , C08G18/80 , C09D175/00 , C09D175/04 , C09D175/06 , C09D175/08 , C07C269/02 , C07C271/26 , C08G18/76
CPC分类号： C07C271/28 , C08G18/10 , C08G18/8029 , C09D175/06
摘要： Polyisocyanates based on polyhydroxy polyethers and tolylene diisocyanate containing ether and urethane groups and having an isocyanate group content of from 11.8 to 14.4% by weight, an average isocyanate functionality of from 3.1 to 4.0 and a free tolylene diisocyanate content of less than 0.1% by weight are produced by reacting a polyhydroxy polyether having a molecular weight in the range of from about 350 to about 500 with excess quantities of tolylene diisocyanate and subsequently distilling the mixture to remove unreacted excess of the starting diisocyanate. These polyisocyanates are particularly useful in the production of polyurethane lacquers.
摘要翻译：基于多羟基聚醚的多异氰酸酯和含有醚和氨基甲酸酯基团的甲苯二异氰酸酯，异氰酸酯基含量为11.8至14.4重量％，平均异氰酸酯官能度为3.1至4.0，游离甲苯二异氰酸酯含量小于0.1重量％通过使分子量为约350至约500的多羟基聚醚与过量的甲苯二异氰酸酯反应制备，随后蒸馏混合物以除去未反应的过量的起始二异氰酸酯。这些多异氰酸酯特别可用于生产聚氨酯漆。

4. 发明授权

US5096994A Polyisocyanates containing ester groups, a process for the production of these polyisocyanates and their use in polyurethane coating compositions 失效
标题翻译：含有酯基的聚异氰酸酯，生产这些聚异氰酸酯的方法及其在聚氨酯涂料组合物中的用途
公开(公告)号：US5096994A
公开(公告)日：1992-03-17
申请号：US561770
申请日：1990-08-02
申请人： Lutz Schmalstieg , Josef Pedain , Klaus Nachtkamp , Lothar Kahl , Manfred Schonfelder
发明人： Lutz Schmalstieg , Josef Pedain , Klaus Nachtkamp , Lothar Kahl , Manfred Schonfelder
IPC分类号： C07C263/16 , C07C265/04 , C07H13/04 , C08G18/73 , C08G18/77 , C09D175/00 , C09D175/04
CPC分类号： C07H13/04 , C07C265/04 , C08G18/771
摘要： The present invention relates to polyisocyanates which contain ester groups and havea) a content of aliphatically bound isocyanate groups of 18 to 33% by weight,b) an average NCO functionality of 4.1 to 10, preferably from 4.5 to 10, andc) a viscosity of 200 to 2,5000 mPa.s at 22.degree. C.The present invention also relates to preferred polyisocyanates which contain ester groups and havea) a content of aliphatically bound isocyanate groups of 20 to 33% by weight,b) an average NCO functionality of 5 to 8 andc) a viscosity of 500 to 1,000 mPa.s at 22.degree. C.The present invention further relates to a process for the preparation of these preferred polyisocyanates by reacting isocyanatocarboxylic acid chlorides with O-silylated, polyhydric alcohols at a temperature of about 50.degree. to 150.degree. C. Finally, the present invention relates to the use of the polyisocyanates as the isocyanate component for two-component polyurethane coating compositions.
摘要翻译：本发明涉及含有酯基并且具有以下特征的多异氰酸酯：a）脂肪族结合的异氰酸酯基团的含量为18〜33重量％，b）平均NCO官能度为4.1〜10，优选为4.5〜10，以及c） 22℃下的粘度为200〜25000mPa.s。本发明还涉及优选的含有酯基的多异氰酸酯，其具有a）含有20〜33重量％的脂肪族结合的异氰酸酯基的含量，b）平均 NCO官能度为5至8，和c）在22℃下的粘度为500至1,000mPa.s。本发明还涉及通过使异氰酸酯基羧酸与O-甲硅烷基化的多元醇反应来制备这些优选的多异氰酸酯的方法在约50℃至150℃的温度下进行。最后，本发明涉及多异氰酸酯作为双组分聚氨酯涂料组合物的异氰酸酯组分的用途。

5. 发明授权

US5061775A Heat curable mixtures and their use for the formation of coatings on heat resistant substrates 失效
标题翻译：可热固化的混合物及其在耐热基材上形成涂层的用途
公开(公告)号：US5061775A
公开(公告)日：1991-10-29
申请号：US549508
申请日：1990-07-06
申请人： Lutz Schmalstieg , Klaus Nachtkamp , Karl-Ludwig Noble
发明人： Lutz Schmalstieg , Klaus Nachtkamp , Karl-Ludwig Noble
IPC分类号： C08G18/10 , C08G18/78 , C08G18/79 , C08G18/80 , C09D175/00
CPC分类号： C08G18/808 , C08G18/10 , C08G18/7831 , C08G18/792
摘要： The present invention relates to a coating composition which may be cured at elevated temperature and is based onA) a polyisocyanate component containing at least one organic polyisocyanate having reversibly blocked isocyanate groups and a molecular weight of 398 to 25,000, excluding the weight of the blocking agent, the isocyanate groups being reversibly blocked with a secondary monoamine andB) an isocyanate reactive component containing at least one organic polyamine having a molecular weight of 60 to 499 and at least two primary amino groups.The present invention also relates to the use of these coating compositions for the formation of coatings on heat resistant substrates.
摘要翻译：本发明涉及一种涂料组合物，其可以在升高的温度下固化，并且基于A）含有至少一种具有可逆封闭的异氰酸酯基团并且分子量为398至25,000的有机聚异氰酸酯的多异氰酸酯组分，不包括嵌段的重量异氰酸酯基团可以用二级单胺可逆地封闭，以及B）含有至少一种分子量为60-499和至少两个伯氨基的有机多胺的异氰酸酯反应性组分。本发明还涉及这些涂料组合物在耐热基材上形成涂层的用途。

6. 发明授权

US5142081A Process for the preparation of O-silylated hydroxyl compounds and their use for the preparation of isocyanates containing ester groups 失效
标题翻译：制备O-硅氧烷化合物的方法及其用于制备含有酯基团的异氰酸酯的方法
公开(公告)号：US5142081A
公开(公告)日：1992-08-25
申请号：US596173
申请日：1990-10-10
申请人： Lutz Schmalstieg , Josef Pedain , Klaus Nachtkamp
发明人： Lutz Schmalstieg , Josef Pedain , Klaus Nachtkamp
IPC分类号： C07F7/18
CPC分类号： C07F7/188
摘要： This present invention relates to a process for the preparation of O-silylated aliphatic hydroxyl, compounds by the reaction of aliphatic hydroxyl compounds with triorganochlorosilanes and removal of the resulting gaseous hydrogen chloride from the reaction mixture, characterized in that the reaction is carried out in the presence of phase transfer catalysts in the absence of solvent.The invention also relates to the use of the O-silylated hydroxyl compounds obtained by this process as starting materials for the preparation of isocyanates containing ester groups by a reaction with isocyanato carboxylic acid chlorides.
摘要翻译：本发明涉及通过脂族羟基化合物与三有机氯硅烷的反应和从反应混合物中除去所得到的气态氯化氢来制备O-甲硅烷基化的脂族羟基化合物的方法，其特征在于反应在在不存在溶剂的情况下存在相转移催化剂。本发明还涉及通过该方法获得的O-甲硅烷基化羟基化合物作为通过与异氰酸根合羧酸氯化物反应制备含酯基的异氰酸酯的起始原料的用途。

7. 发明授权

US5306740A Process for the production of brominated chlorine-substituted poly-1,3-butadiene 失效
标题翻译：生产溴化氯取代聚-1,3-丁二烯的方法
公开(公告)号：US5306740A
公开(公告)日：1994-04-26
申请号：US44732
申请日：1993-04-12
申请人： Hans J. Laas , Heinz W. Lucas , Klaus Nachtkamp , Heinrich Konigshofen
发明人： Hans J. Laas , Heinz W. Lucas , Klaus Nachtkamp , Heinrich Konigshofen
IPC分类号： B32B7/12 , B32B15/06 , C08C19/14 , C08F4/28 , C08F8/20 , C08F136/00 , C08F136/18 , C09J115/02 , C09J121/00 , C08F8/22
CPC分类号： C09J115/02 , C08C19/14 , Y02P20/582
摘要： Brominated chlorine-substituted poly-1,3-butadiene is produced by a process in which an aqueous chlorine-substituted poly-1,3-butadiene latex is reacted in aqueous phase with a brominating agent in the presence of a radical-forming catalyst and/or in the presence of light at a pH value below 7 and at a temperature of 20.degree. to 95.degree. C., the brominated reaction product is optionally precipitated from the aqueous dispersion obtained and then separated from the aqueous liquid.
摘要翻译：溴化氯取代的聚-1,3-丁二烯通过以下方法制备：其中氯取代的聚-1,3-丁二烯胶乳在水性相中与溴化剂在自由基形成催化剂存在下反应， /或在pH值低于7且温度为20摄氏度至95摄氏度的光的存在下，溴化反应产物任选地从所获得的水分散体中沉淀，然后与水性液体分离。

8. 发明授权

US07071326B2 Anionic cellulose nitrate derivatives and aqueous dispersions thereof 失效
标题翻译：阴离子硝酸纤维素衍生物及其水分散体
公开(公告)号：US07071326B2
公开(公告)日：2006-07-04
申请号：US11290193
申请日：2005-11-30
申请人： Carsten Hüttermann , Thomas Wagner , Klaus Nachtkamp
发明人： Carsten Hüttermann , Thomas Wagner , Klaus Nachtkamp
IPC分类号： C08B7/00 , C09D101/20
CPC分类号： C08J3/05 , C08B7/00 , C08J2301/18 , C08L1/20
摘要： An anionic cellulose nitrate derivative is described, which has: (i) a degree of acid group substitution (DS (acid)) in the range of 0.01 to 0.2; and (ii) a nitrogen content of 10.7 wt. % to 12.3 wt. %, based on the weight of cellulose nitrate derivative. The anionic cellulose nitrate derivative is prepared by a process which includes esterifying cellulose nitrate feed material with at least one dicarboxylic acid anhydride (e.g., maleic anhydride). Aqueous dispersions according to the present invention include: (a) at least on anionic cellulose nitrate derivative according to the present invention; and (b) at least one base.
摘要翻译：描述了一种阴离子硝酸纤维素衍生物，其具有：（i）酸基置换度（DS（酸））在0.01至0.2的范围内; 和（ii）10.7重量％的氮含量。％〜12.3重量％％，基于硝酸纤维素衍生物的重量。通过包括用至少一种二羧酸酐（例如马来酸酐）将硝酸纤维素原料酯化的方法制备阴离子硝酸纤维素衍生物。根据本发明的水分散体包括：（a）至少一种根据本发明的阴离子硝酸纤维素衍生物; 和（b）至少一个碱基。

9. 发明申请

US20060041117A1 Process for the preparation of cellulose derivatives containing amino groups 审中-公开
标题翻译：制备含氨基的纤维素衍生物的方法
公开(公告)号：US20060041117A1
公开(公告)日：2006-02-23
申请号：US11184093
申请日：2005-07-19
申请人： Jurgen Engelhardt , Meinolf Brackhagen , Klaus Nachtkamp , Wolfgang Koch , Thomas Schulze , Frank Meister
发明人： Jurgen Engelhardt , Meinolf Brackhagen , Klaus Nachtkamp , Wolfgang Koch , Thomas Schulze , Frank Meister
IPC分类号： C08B11/00
CPC分类号： C08B11/145 , A61K8/731 , A61Q19/00 , C02F1/56 , D21H17/07 , D21H17/25
摘要： A process is described for the preparation of cellulose derivatives containing amino groups that involves reacting, in the presents of water as a reaction medium, alkali cellulose or alkali cellulose derivatives with reagents represented by the following formula, X—(CH2)n—NR1R2 in which: X is selected from the group consisting of chlorine, bromine, iodine and a sulfonic acid radical R′SO3, in which R′ is an aromatic radical or an aliphatic radical; n is at least 2; and R1 and R2 independently of each other are selected from the group consisting of aliphatic substituents, branched alkyl substituents, cyclic alkyl substituents, aryl substituents, aryl substituents substituted by heteroatoms, H, and R1 and R2 together form a ring with the nitrogen. In the process, the mole ratio of cellulose to water, of said reaction medium, is 1:5 to 1:40 mol water per mol of anhydroglucose unit (AGU). Amino functional cellulose derivatives prepared in accordance with the method of the present invention are useful in cosmetic formulations and aqueous paper treatment compositions.
摘要翻译：描述了制备含有氨基的纤维素衍生物的方法，该方法包括在作为反应介质的水的存在下，将碱纤维素或碱性纤维素衍生物与下式表示的试剂反应：<？在线配方说明= “In-line Formulas”end =“lead”？> X-（CH 2）n - NR 1 R 2 - 其中：X选自氯，溴，碘和磺酸基R'SO 2，其中：X选自氯，溴，碘，磺酸根R' 其中R'是芳族基团或脂族基团; n至少为2; R 1和R 2彼此独立地选自脂族取代基，支链烷基取代基，环烷基取代基，芳基取代基，被杂原子取代的芳基取代基，H和R 1和R 2一起与氮一起形成环。在该过程中，所述反应介质的纤维素与水的摩尔比为每摩尔脱水葡萄糖单元（AGU）为1:5至1:40摩尔水。根据本发明的方法制备的氨基官能纤维素衍生物可用于化妆品制剂和水性纸处理组合物中。

10. 发明授权

US5981653A Process for the production of aqueous stoving coating compositions 失效
标题翻译：用于生产水性烘烤涂料组合物的方法
公开(公告)号：US5981653A
公开(公告)日：1999-11-09
申请号：US844815
申请日：1997-04-22
申请人： Oswald Wilmes , Lothar Kahl , Bernd Klinksiek , Christian Wamprecht , Manfred Bock , Klaus Nachtkamp
发明人： Oswald Wilmes , Lothar Kahl , Bernd Klinksiek , Christian Wamprecht , Manfred Bock , Klaus Nachtkamp
IPC分类号： C08J3/02 , B01J13/04 , C08G18/08 , C08G18/63 , C08G18/79 , C08G18/80 , C08J3/03 , C08J3/12 , C09D5/46 , C09D175/04 , C08G18/40 , C08L75/04
CPC分类号： C08J3/03 , C08G18/0866 , C08G18/631 , C08G18/792 , C08G18/8061 , C08G2150/20 , C08J2375/04
摘要： The present invention relates to a process for the production of aqueous dispersions which form powder coatings at room temperature, have an average particle size of 0.1 to 10 .mu.m, contain polyols and blocked polyisocyanate crosslinking agents, and, after stoving, yield coatings with improved water and solvent resistance, in particular on metallic substrates.
摘要翻译：本发明涉及一种在室温下形成粉末涂料的水性分散体的制备方法，平均粒径为0.1-10μm，含有多元醇和封端的多异氰酸酯交联剂，并且在烘烤后，产率增加了耐水和耐溶剂性，特别是在金属基材上。

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